ChemicalBook > CAS DataBase List > 4-IODO-3-NITROPHENOL

4-IODO-3-NITROPHENOL

Product Name: 4-IODO-3-NITROPHENOL
CAS No.: 50590-07-3
Chemical Name: 4-IODO-3-NITROPHENOL
Synonyms: 3-Iodo-4-nitrophenol.;Phenol, 3-iodo-4-nitro-;4-IODO-3-NITROPHENOL 97%
CBNumber: CB3434549
Molecular Formula: C6H4INO3
Formula Weight: 265.01
MOL File: 50590-07-3.mol

Less

4-IODO-3-NITROPHENOL Property

Melting point:: 153-159 °C
Boiling point:: 382.5±37.0 °C(Predicted)
Density: 2.176
storage temp.: 2-8°C(protect from light)
pka: 6.39±0.10(Predicted)
Appearance: Light yellow to yellow Solid

Less

Safety

Hazard Codes: Xn
Risk Statements: 36/37/38-20/21/22
Safety Statements: 36/37/39-26
HS Code: 2908990000

Less

Hazard and Precautionary Statements (GHS)

Less

N-Bromosuccinimide Price

TRC

Product number: I715733
Product name: 3-Iodo-4-nitrophenol
Packaging: 500mg
Price: $175
Updated: 2021/12/16

AK Scientific

Product number: J55270
Product name: 3-Iodo-4-nitrophenol
Packaging: 1g
Price: $49
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-17
Product name: 3-Iodo-4-nitrophenol
Packaging: 1g
Price: $240
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-17
Product name: 3-Iodo-4-nitrophenol
Packaging: 5G
Price: $768
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0036018
Product name: 3-IODO-4-NITROPHENOL
Purity: 95.00%
Packaging: 10G
Price: $1963.5
Updated: 2021/12/16

Less

4-IODO-3-NITROPHENOL Chemical Properties,Usage,Production

Synthesis

626-02-8

27783-55-7

50590-07-3

General procedure for the synthesis of 5-iodo-2-nitrophenol and 3-iodo-4-nitrophenol from 3-iodophenol: 3.0 mL of fuming nitric acid (75 mmol) in 12 mL of glacial acetic acid was slowly added dropwise to 15.03 g (68.3 mmol) of 3-iodophenol dissolved in 60 mL of glacial acetic acid over a 25-minute period and the reaction flask was placed in an ice bath to cool. After the dropwise addition was completed, the reaction mixture was continued to be stirred at room temperature for 30 min. Subsequently, the reaction solution was poured into ice water and concentrated under vacuum to remove most of the solvent. The residue was dissolved in 150 mL of water and then extracted with dichloromethane (2 x 300 mL). The organic phases were combined, dried with anhydrous magnesium sulfate, and the solvent was evaporated under reduced pressure to give 17 g of crude product. Separation by silica gel medium-pressure chromatography (eluent ratio 1:2 ethyl acetate:hexane) afforded 3-iodo-4-nitrophenol (6.93 g, 26.1 mmol, 38% yield), melting point 121-123 °C; 1H NMR (CDCl3, 300 MHz) δ 7.98 (d, 1H, J = 9 Hz), 7.54 (d, 1H, J = 3 Hz) 6.92 (dd, 1H, J = 9, 3 Hz), 5.54 (bs, 1H); IR (KBr) 3150 (wide), 1600, 1580, 1512, 1404, 1336, 1298, 1212, 1121, 1023, 870 cm?1; and 3-iodo-6-nitrophenol (3.07 g, 11.6 mmol, yield 17%), melting point 92-94 °C after recrystallization from dichloromethane/hexane (literature value 96 °C; Hodgson, H.H. et al., 1927); 1H NMR (CDCl3, 300 MHz) δ 10.53 (s, 1H), 7.76 (d, 1H, J = 9.0 Hz), 7.59 (d, 1H, J = 2.0 Hz), 7.33 ( dd, 1H, J = 9.0, 2.0 Hz); 13C NMR (CDCl3; assisted attribution by HMQC) δ 105.2 (C-3), 125.6 (C-5), 129.2 (C-2), 129.7 (C-4), 133.4 (C-6), 154.6 (C-1); IR (KBr) 3430 (broad), 1604, 1671, 1518, 1463 1571, 1518, 1463, 1317, 1225, 1172, 1055, 888 cm?1; Calculated elemental analysis (C6H4INO3): C, 27.19; H, 1.52; N, 5.29. Measured values: C, 27.36; H, 1.57; N, 5.15.

References

[1] Tetrahedron, 2010, vol. 66, # 47, p. 9252 - 9262
[2] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 16, p. 4960 - 4971
[3] Patent: WO2005/95347, 2005, A1. Location in patent: Page/Page column 41
[4] Journal of the Chemical Society, 1927, p. 634
[5] Journal of the Chemical Society, 1925, vol. 127, p. 1602

4-IODO-3-NITROPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

Less

4-IODO-3-NITROPHENOL Suppliers

China 50 Germany 1 India 2 Japan 1 Switzerland 1 United Kingdom 8 United States 9 Global 72

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Chemsky（shanghai）International Co.,Ltd.

Tel: 021-50135380
Email: shchemsky@sina.com
Country: China
ProdList: 32321
Advantage: 50

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 86(512)5235 8471 17715136450
Fax: 86(512)5235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 4169
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Xinyanhe Pharmatech Co.,Ltd

Tel: 0519-85252752 15366845260
Fax: 86-0519-85683352
Email: taihuaren@vip.163.com
Country: China
ProdList: 1124
Advantage: 58

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Zhengzhou Huiju Chemical Co., Ltd.

Tel: 0371-55900031 18137872243
Fax: QQ：2853979815
Email: 2853979815@qq.com
Country: China
ProdList: 9996
Advantage: 55

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9754
Advantage: 58

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

DILICHEM

Tel: 0519-0519-81238123 18014346496
Email: shichaojun@126.com
Country: China
ProdList: 394
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9853
Advantage: 58

Cool Pharm, Ltd

Tel: 021-58581007 18019463053
Fax: 021-50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12878
Advantage: 58

Xinyi Kaiwu Chemical Technology Co., Ltd.

Tel: 0516-0516-88997009 18651776937
Email: 4164357@qq.com
Country: China
ProdList: 3204
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

Hefei Hirisun Pharmatech Co., Ltd

Tel: +8615056975894
Fax: 86-0551-62678551
Email: shawn@hirisunpharm.com
Country: CHINA
ProdList: 9911
Advantage: 58

Accela ChemBio Co.,Ltd.

Tel: 021-50795510 4000665055
Email: sales@accelachem.com
Country: China
ProdList: 10467
Advantage: 58

CONIER CHEM AND PHARMA LIMITED

Tel: +8618523575427
Email: sales@conier.com
Country: China
ProdList: 49975
Advantage: 58

Shanghai Kaiwei Chemical Technology Co., Ltd.

Tel: 021-58461859 15821823057
Email: service@aiviche.com
Country: China
ProdList: 49312
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing@energy-chemical.com
Country: China
ProdList: 44918
Advantage: 58

Shanghai Sunway Pharmaceutical Technology Co.,Ltd.

Tel: 021-51816796-820 13611835272
Fax: 021-5161 3951
Email: sales2@sunwaypharm.com
Country: China
ProdList: 44119
Advantage: 58

Shanghai UCHEM Inc.

Tel: 18939844854
Fax: QQ3004479448
Email: sales6@myuchem.com
Country: China
ProdList: 4997
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Qi Qi hang Biotechnology Co., Ltd.

Tel: 15870833005
Email: 2232044025@qq.com
Country: China
ProdList: 8206
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Jiaxing Zhejia Biotechnology Co., LTD

Tel: 0573-85609002 18367600069;
Email: zhejia01@163.com
Country: China
ProdList: 8887
Advantage: 58

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 18621169109
Email: market03@meryer.com
Country: China
ProdList: 27987
Advantage: 58

Shandong Bourne Pharmaceutical Co. , Ltd.

Tel: 15865694623
Email: 1825792389@qq.com
Country: China
ProdList: 370
Advantage: 58

Shaanxi Xihua Chemical Industry Co., Ltd

Tel: 029-029-81123119 17391733320
Email: 1021@dideu.com
Country: China
ProdList: 10001
Advantage: 58

Beijing Solarbio Science & Tecnology Co., Ltd.

Tel: 010-50973130 17801761073
Email: Gsiyu@solarbio.com
Country: China
ProdList: 50464
Advantage: 58

Shanghai Jieshikai Biotechnology Co. , Ltd.

Tel: 021-57520305 13795461237
Email: zhuruyan@jskchem.com
Country: China
ProdList: 49234
Advantage: 58

Hangzhou Bingochem Co., Ltd.

Tel: 0571-8512-5372
Email: sales@bingochem.com
Country: China
ProdList: 21669
Advantage: 58

Shanghai Aladdin Biochemical Technology Co.,Ltd.

Tel: 400-6206333 13167063860
Email: anhua.mao@aladdin-e.com
Country: China
ProdList: 48457
Advantage: 58

Hubei Shanlexing Biotechnology Co., Ltd

Tel: 15972496547
Email: 15972496547@163.com
Country: China
ProdList: 2087
Advantage: 58

Shanghai Ken chemical Technology Co.,ltd

Tel: 02152215958
Email: 47697177@qq.com
Country: China
ProdList: 10011
Advantage: 58

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 17715136450
Email: 2439673774@qq.com
Country: China
ProdList: 15647
Advantage: 58

Santa Cruz Biotechnology Inc

Tel: 021-60936350
Email: scbt@scbt.com
Country: China
ProdList: 6594
Advantage: 58

Shanghai Fengluan Biotechnology Co., LTD

Tel: 13357659136
Email: jing.z@fengluanbiotech.com
Country: China
ProdList: 500
Advantage: 58

DAYANG CHEM (HANGZHOU) CO.,LTD

Tel: +86-88938639 +86-17705817739
Email: info@dycnchem.com
Country: China
ProdList: 53899
Advantage: 58

HANGZHOU LEAP CHEM CO., LTD.

Tel: +86-571-87711850
Email: market18@leapchem.com
Country: China
ProdList: 24727
Advantage: 58

Beijing Boning Biotechnology Co., Ltd.

Tel: 13269979963
Email: 1565439254@qq.com
Country: CHINA
ProdList: 195
Advantage: 58

Shanghai Machine Pure Industrial Co., Ltd.

Tel: --
Fax: --
Email: 3245176082@qq.com
Country: CHINA
ProdList: 6800
Advantage: 58

Shanghai Wowu Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: shhebio@126.com
Country: CHINA
ProdList: 6137
Advantage: 58

Shanghai Cheerchem Co., Ltd.

Tel: --
Fax: --
Email: qiyuehuagong@163.com
Country: China
ProdList: 34
Advantage: 50

Shanghai TBBMed Co.,Ltd.

Tel: --
Fax: --
Email: products@tbbmed.com
Country: China
ProdList: 216
Advantage: 0

Carbosynth China Ltd.

Tel: --
Fax: --
Email: sales@carbosynth.com
Country: China
ProdList: 6532
Advantage: 50

Less

View Lastest Price from 4-IODO-3-NITROPHENOL manufacturers

Career Henan Chemical Co

Product: 4-IODO-3-NITROPHENOL 50590-07-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-11

50590-07-3, 4-IODO-3-NITROPHENOLRelated Search:

3-Iodo-4-nitrophenol.

4-IODO-3-NITROPHENOL 97%

Phenol, 3-iodo-4-nitro-

50590-07-3

Aromatic Phenols