5-IODO-1H-BENZIMIDAZOLE

Product Name: 5-IODO-1H-BENZIMIDAZOLE
CAS No.: 78597-27-0
Chemical Name: 5-IODO-1H-BENZIMIDAZOLE
Synonyms: 6-Iodobenzimidazole;5-Iodobenzimidazole;5(6)-iodobenziMidazole;6-iodo-1H-benzimidazole;5-IODO-1H-BENZIMIDAZOLE;1H-BenziMidazole,6-iodo;5-Iodo-1H-benzoimidazole;5-Iodo-1H-benzimidazole97%;5-iodo-1H-1,3-benzodiazole;5(6)-IODO-1H-BENZIMIDAZOLE
CBNumber: CB3476015
Molecular Formula: C7H5IN2
Formula Weight: 244.03
MOL File: 78597-27-0.mol

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5-IODO-1H-BENZIMIDAZOLE Property

Melting point:: 144-145 °C
Boiling point:: 438.5±18.0 °C(Predicted)
Density: 2.082±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder
pka: 11.39±0.30(Predicted)
color: Faint lemon

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR16685
Product name: 5-Iodo-1H-benzimidazole
Purity: 97%
Packaging: 250mg
Price: $95
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-H-19
Product name: 5-Iodo-1H-benzimidazole
Packaging: 250mg
Price: $104
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-H-19
Product name: 5-Iodo-1H-benzimidazole
Packaging: 1g
Price: $240
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0142683
Product name: 5-IODO-1H-BENZIMIDAZOLE
Purity: 95.00%
Packaging: 250MG
Price: $252
Updated: 2021/12/16

Matrix Scientific

Product number: 130817
Product name: 5-Iodo-1H-benzimidazole
Packaging: 1g
Price: $504
Updated: 2021/12/16

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5-IODO-1H-BENZIMIDAZOLE Chemical Properties,Usage,Production

Synthesis

64-18-6

20691-72-9

78597-27-0

The general procedure for the synthesis of 5-iodobenzimidazole from formic acid and 4-iodo-2-nitroaniline is as follows: intermediate Example 12.Synthesis of 5-iodo-1H-benzo[d]imidazole from 5-((trimethylsilyl)ethynyl)-1H-benzo[d]imidazole). 4-Methyl-2-nitroaniline (1 g, 3.7 mmol) was dissolved in formic acid (10 ml), iron powder (2.1 g, 37 mmol) was added, and the reaction mixture was heated and refluxed for 12 h at 90 °C. After completion of the reaction, formic acid was removed by distillation. The crude product was dissolved in ethyl acetate, and the organic layer was washed sequentially with water and saturated brine, and then dried with anhydrous sodium sulfate. The solvent was removed by distillation under reduced pressure to afford the target product 5-iodo-1H-benzo[d]imidazole in 68% yield (0.85 g). Product characterization by LC-MS (ES): calculated mass: 243.95; observed mass: 244.8 [M + H]+ (retention time: 0.173 min).

References

[1] Synlett, 2010, # 18, p. 2759 - 2764
[2] Patent: WO2014/162039, 2014, A1. Location in patent: Page/Page column 39

5-IODO-1H-BENZIMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-IODO-1H-BENZIMIDAZOLE Suppliers

China 67 France 1 India 2 United Kingdom 1 United States 8 Global 79

Accela ChemBio Co.,Ltd.

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View Lastest Price from 5-IODO-1H-BENZIMIDAZOLE manufacturers

Career Henan Chemica Co

Product: 5-IODO-1H-BENZIMIDAZOLE 78597-27-0
Price: US $9.80-8.00/KG
Min. Order: 1KG
Purity: 95%~99.99%
Supply Ability: 10 MT/ Month
Release date: 2020-10-28

78597-27-0, 5-IODO-1H-BENZIMIDAZOLERelated Search:

6-IODO-1-(2-METHYL-PROPANE-2-SULFONYL)-1H-BENZOIMIDAZOL-2-YLAMINE 1H-BENZIMIDAZOLE, 2-CHLORO-5-IODO- 5-IODO-2-METHYLBENZIMIDAZOLE 2-AMINO-6-IODO-BENZOIMIDAZOLE-1-SULFONIC ACID DIMETHYLAMIDE 5-IODO-1H-BENZIMIDAZOLE 1H-BENZIMIDAZOLE, 5-IODO-2-(TRIFLUOROMETHYL)- 5-IODO-1H-BENZIMIDAZOLE-2-AMINE 1H-BENZIMIDAZOLE-2-CARBOXALDEHYDE, 5-IODO- 6-IODO-1-(PROPANE-2-SULFONYL)-1H-BENZO-IMIDAZOL-2-YLAMINE

5-IODO-1H-BENZIMIDAZOLE

6-iodo-1H-benzimidazole

6-Iodobenzimidazole

5-Iodo-1H-benzimidazole97%

5-Iodo-1H-benzoimidazole

1H-BenziMidazole,6-iodo

5-iodo-1H-1,3-benzodiazole

5(6)-iodobenziMidazole

5-iodo-1H-benzo[d]iMidazole

6-Iodo-1H-benzo[d]iMidazole

5-Iodo-1H-benzimidazole 97%

5-Iodobenzimidazole

5(6)-IODO-1H-BENZIMIDAZOLE

78597-27-0