ChemicalBook > CAS DataBase List > 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE

Product Name
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
CAS No.
24422-15-9
Chemical Name
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
Synonyms
Rivaroxaban Impurity 166;trichlorothiophene-2-carbonyl chloride;3,4,5-trichloro-2-thiophenecarbonyl chloride;3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE;2-Thiophenecarbonyl chloride, 3,4,5-trichloro-;3,4,5-Trichlorothien-2-carboxylic acid chloride
CBNumber
CB3482535
Molecular Formula
C5Cl4OS
Formula Weight
249.93
MOL File
24422-15-9.mol
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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Property

Melting point:
38-40°C
Boiling point:
124-125°C 10mm
Flash point:
124-125°C/10mm
Sensitive 
Moisture Sensitive
BRN 
1427060
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Safety

Risk Statements 
34
Safety Statements 
26-36/37/39-45
RIDADR 
3261
HazardClass 
8
PackingGroup 
II
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Alfa Aesar
Product number
L17704
Product name
3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
Packaging
1g
Price
$38.9
Updated
2021/12/16
Alfa Aesar
Product number
L17704
Product name
3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
Packaging
5g
Price
$118
Updated
2021/12/16
AHH
Product number
MT-36791
Product name
3,4,5-Trichlorothiophene-2-carbonylchloride
Purity
97%
Packaging
25g
Price
$300
Updated
2021/12/16
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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Chemical Properties,Usage,Production

Preparation

3,4,5-Trichlorothiophene-2-carbonyl chloride synthesis: A mixture of 3,4,5-trichloro-2-thiophenecarboxylic acid (20.4 g, 0.088 mol), SOCl2 (7.3 mL, 0.1 mol), and DMF (0.2 mL) in 80 mL of 1,2-dichloroethane was heated at reflux temperature for 3 h. The reaction mixture became homogeneous after 1 h of heating. The solution was cooled to 25℃, concentrated and placed under high vacuum to remove residual solvent, giving 22.0 g (98% wt.) of 3,4,5-trichloro-2-thiophenecarbonyl chloride as an oil which solidified on standing to an off-white powder; m.p. 37-41℃, having a GC area % purity > 99%.

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Suppliers

Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006608290; 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40241
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30132
Advantage
84
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44751
Advantage
61
Shanghai Nuohey Chemical Co., Ltd.
Tel
021-52212593 13761626812
Fax
+86 (21) 51062076
Email
sales@nuohey.com
Country
China
ProdList
10690
Advantage
60
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131981
Advantage
58
Aikon International Limited
Tel
025-58851090 13611564524
Fax
(6)02557626880
Email
lwan@aikonchem.com
Country
China
ProdList
15952
Advantage
58
CONIER CHEM AND PHARMA LIMITED
Tel
+8618523575427
Email
sales@conier.com
Country
China
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Hubei Qingbei Yunyan Pharmaceutical Technology Co., Ltd
Tel
18162595016
Email
3287908757@qq.com
Country
China
ProdList
9514
Advantage
58
LEAPCHEM CO., LTD.
Tel
+86-852-30606658
Email
market18@leapchem.com
Country
China
ProdList
43348
Advantage
58

24422-15-9, 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDERelated Search:


  • 3,4,5-Trichlorothien-2-carboxylic acid chloride
  • 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
  • 3,4,5-trichloro-2-thiophenecarbonyl chloride
  • 2-Thiophenecarbonyl chloride, 3,4,5-trichloro-
  • Rivaroxaban Impurity 166
  • trichlorothiophene-2-carbonyl chloride
  • 24422-15-9
  • C5Cl4OS