ChemicalBook > CAS DataBase List > N-BENZYLHYDROXYLAMINE HYDROCHLORIDE

N-BENZYLHYDROXYLAMINE HYDROCHLORIDE

Product Name
N-BENZYLHYDROXYLAMINE HYDROCHLORIDE
CAS No.
622-30-0
Chemical Name
N-BENZYLHYDROXYLAMINE HYDROCHLORIDE
Synonyms
N-Hydroxybenzylamine;N-Benzylhydroxylamine;N-benzyl hydroxylalmine;N-Hydroxybenzenemethanamine;N-Benzylhydroxylamine, 98+%;N-Hydroxy-1-phenylmethanamine;Benzenemethanamine, N-hydroxy-
CBNumber
CB3502459
Molecular Formula
C7H9NO
Formula Weight
123.15
MOL File
622-30-0.mol
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N-BENZYLHYDROXYLAMINE HYDROCHLORIDE Property

Melting point:
~105 °C
Boiling point:
253.9±33.0 °C(Predicted)
Density 
1.098±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Store in freezer, under -20°C
pka
13.19±0.30(Predicted)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3
F 
3-10
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
B297055
Product name
N-Benzylhydroxylamine
Packaging
10mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
9353AB
Product name
N-Benzylhydroxylamine
Packaging
10g
Price
$324
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0145636
Product name
N-BENZYLHYDROXYLAMINE
Purity
95.00%
Packaging
5MG
Price
$503.47
Updated
2021/12/16
Ark Pharm
Product number
AK110567
Product name
N-Benzylhydroxylamine
Purity
95%
Packaging
1g
Price
$28
Updated
2021/12/16
J&W Pharmlab
Product number
20R1551
Product name
N-Benzyl-hydroxylamine
Purity
96%
Packaging
5g
Price
$30
Updated
2021/12/16
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N-BENZYLHYDROXYLAMINE HYDROCHLORIDE Chemical Properties,Usage,Production

Preparation

(a) Preparation of a-phenyl-N-benzylnitrone. To a flask equipped with a stirrer and condenser and containing 17.6 gm (0.0827 mole) of N,N-dibenzylhydroxylamine is added 36.8 gm (0.17 mole) of yellow mer­curic oxide and 100 ml of ether. The mixture is stirred and the resulting exothermic reaction causes the ether to reflux for 1 hr. After a total of 3 hr reaction time the reaction mixture is filtered and concentrated to afford 15.7 gm (90%), m.p. 81.5-83.5°C (recrystallized from acetone-ligroin). Jones and Sneed [12a] earlier reported that air-KOH can also be used to effect this oxidation.
(b) Hydrolysis of a-phenyl-N-benzylnitrone to N-benzylhydroxylamine [12a]. To a flask containing 17.0 gm (0.0806 mole) of the above nitrone is added 34 ml of concentrated hydrochloric acid solution. Then the mixture is steam-distilled to remove the formed benzaldehyde. After the benzal­dehyde is removed the hydrochloric acid is removed by heating over a low flame. To the cool residue is added a cold solution of sodium carbonate to neutralize the mixture. The mixture is filtered, and the filtrate, after being cooled to 0°C, is made alkaline. After 1 hr N-benzylhydroxylamine pre­cipitates from the cold filtrate and is filtered to afford 6.0 gm (61%), m.p. 57°C (recrystallized from benzene-petroleum ether). Yields as high as 88% have been reported for this preparation.

N-BENZYLHYDROXYLAMINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Benzaldoxime

Preparation Products

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N-BENZYLHYDROXYLAMINE HYDROCHLORIDE Suppliers

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View Lastest Price from N-BENZYLHYDROXYLAMINE HYDROCHLORIDE manufacturers

Honest Joy Holdings Limited
Product
N-Benzylhydroxylamine 622-30-0
Price
US $0.00/KG
Min. Order
1KG
Purity
98.5%
Supply Ability
100 tons
Release date
2022-02-21
Nanjing jinheyou Trading Co., Ltd.
Product
N-BENZYLHYDROXYLAMINE HYDROCHLORIDE 622-30-0
Price
US $0.00/g
Min. Order
1g
Purity
95%min
Supply Ability
20kgs/month
Release date
2019-11-18
Nanjing jinheyou Trading Co., Ltd.
Product
N-BENZYLHYDROXYLAMINE HYDROCHLORIDE 622-30-0
Price
US $0.00/g
Min. Order
1g
Purity
95%min
Supply Ability
30kgs/month
Release date
2019-11-14

622-30-0, N-BENZYLHYDROXYLAMINE HYDROCHLORIDERelated Search:

HYDROXYLAMINE N-Benzylhydroxylamine hydrochloride

  • N-benzyl hydroxylalmine
  • N-Benzylhydroxylamine
  • N-Hydroxybenzenemethanamine
  • N-Hydroxybenzylamine
  • Benzenemethanamine, N-hydroxy-
  • N-Hydroxy-1-phenylmethanamine
  • N-Benzylhydroxylamine, 98+%
  • 622-30-0
  • Polyamines