2 4 6-TRICHLOROBENZYL ALCOHOL 97
- Product Name
- 2 4 6-TRICHLOROBENZYL ALCOHOL 97
- CAS No.
- 217479-60-2
- Chemical Name
- 2 4 6-TRICHLOROBENZYL ALCOHOL 97
- Synonyms
- (2,4,6-Trichlorophenyl)Methanol;BenzeneMethanol, 2,4,6-trichloro-;2 4 6-TRICHLOROBENZYL ALCOHOL 97;2,4,6-
Trichlorobenzyl alcohol - CBNumber
- CB3504529
- Molecular Formula
- C7H5Cl3O
- Formula Weight
- 211.47
- MOL File
- 217479-60-2.mol
2 4 6-TRICHLOROBENZYL ALCOHOL 97 Property
- Melting point:
- 98-101 °C (lit.)
- Boiling point:
- 299.4±35.0 °C(Predicted)
- Density
- 1.520±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 13.18±0.10(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 526436
- Product name
- 2,4,6-Trichlorobenzyl alcohol
- Purity
- 97%
- Packaging
- 5g
- Price
- $152.5
- Updated
- 2025/07/31
- Product number
- T774740
- Product name
- 2,4,6-Trichlorobenzyl alcohol
- Packaging
- 2.5g
- Price
- $220
- Updated
- 2021/12/16
- Product number
- W4505
- Product name
- 2,4,6-Trichlorobenzyl alcohol
- Packaging
- 250mg
- Price
- $80
- Updated
- 2021/12/16
- Product number
- 076292
- Product name
- 2,4,6-Trichlorobenzyl alcohol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $116
- Updated
- 2021/12/16
- Product number
- 076292
- Product name
- 2,4,6-Trichlorobenzyl alcohol
- Purity
- 95+%
- Packaging
- 5g
- Price
- $360
- Updated
- 2021/12/16
2 4 6-TRICHLOROBENZYL ALCOHOL 97 Chemical Properties,Usage,Production
Uses
2,4,6-Trichlorobenzyl Alcohol is an intermediate in the synthesis of 1,3,5-Trichloro-2-methylbenzene (T774363). 1,3,5-Trichloro-2-methylbenzene can be used as reactant/reagent in hydrodechlorination process and catalysts for the production of 2,?6-?dichlorotoluene from polychlorotoluene-?containing mixtures. Also, it is derived from 2,4,6-Trichlorobenzoic Acid (T774715), which is a possible degradation intermediate of Polychlorinated Biphenyls (PCBs) in contaminated soil, suggesting the occurrence of microbial transformation processes over time.
Synthesis
50-43-1
217479-60-2
Step 1) Commercially available 2,4,6-trichlorobenzoic acid (22.5 g, 0.1 mol) was dissolved in tetrahydrofuran (200 mL) under nitrogen protection and cooled in an ice bath. Borane-dimethyl sulfide complex (10 M, 20 mL, 0.2 mol) was added slowly. The reaction mixture was gradually warmed to 22 °C and stirred overnight under reflux conditions. Subsequently, methanol (100 mL) was added slowly and stirring was continued for 16 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure to afford 2,4,6-trichlorobenzyl alcohol (22.7 g, 100% yield) as a white solid.1H NMR (CDCl3, 400 MHz) δ: 7.37 (s, 2H), 4.93 (d, 2H, J = 6.8 Hz).
References
[1] Patent: WO2013/72300, 2013, A1. Location in patent: Page/Page column 123-124
[2] Angewandte Chemie - International Edition, 2015, vol. 54, # 36, p. 10596 - 10599
[3] Angew. Chem., 2015, vol. 127, p. 10742 - 10745,4
[4] Patent: US6348474, 2002, B1. Location in patent: Page column 126
2 4 6-TRICHLOROBENZYL ALCOHOL 97 Preparation Products And Raw materials
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View Lastest Price from 2 4 6-TRICHLOROBENZYL ALCOHOL 97 manufacturers
- Product
- 2 4 6-TRICHLOROBENZYL ALCOHOL 97 217479-60-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kgs
- Release date
- 2020-01-29