3,6-Diiodopyridazine
- Product Name
- 3,6-Diiodopyridazine
- CAS No.
- 20698-04-8
- Chemical Name
- 3,6-Diiodopyridazine
- Synonyms
- 3,6-DIIDOPYRIDAZINE;3,6-Diiodopyridazine;Pyridazine, 3,6-diiodo-;3,6-Diiodopyridazine 97%;3,6-Diiodopyridazine ISO 9001:2015 REACH
- CBNumber
- CB3511950
- Molecular Formula
- C4H2I2N2
- Formula Weight
- 331.88
- MOL File
- 20698-04-8.mol
3,6-Diiodopyridazine Property
- Melting point:
- 155-160 °C
- Boiling point:
- 382.2±22.0 °C(Predicted)
- Density
- 2.765±0.06 g/cm3(Predicted)
- Flash point:
- >110℃
- storage temp.
- 2-8°C
- pka
- -0.80±0.10(Predicted)
- form
- solid
- Appearance
- Off-white to yellow Solid
- InChI
- InChI=1S/C4H2I2N2/c5-3-1-2-4(6)8-7-3/h1-2H
- InChIKey
- GCLHXKPPHRIJOE-UHFFFAOYSA-N
- SMILES
- C1(I)=NN=C(I)C=C1
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-37/38-41
- Safety Statements
- 26-36/37/39
- WGK Germany
- 3
- HazardClass
- IRRITANT
- HS Code
- 2933998090
- Storage Class
- 11 - Combustible Solids
- Hazard Classifications
- Acute Tox. 4 Oral
Eye Dam. 1
Skin Irrit. 2
STOT SE 3
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 708364
- Product name
- 3,6-Diiodopyridazine
- Purity
- 97%
- Packaging
- 1g
- Price
- $176
- Updated
- 2023/06/20
- Product number
- 708364
- Product name
- 3,6-Diiodopyridazine
- Purity
- 97%
- Packaging
- 5g
- Price
- $416
- Updated
- 2023/06/20
- Product number
- D481890
- Product name
- 3,6-Diiodopyridazine
- Packaging
- 50g
- Price
- $1260
- Updated
- 2021/12/16
- Product number
- 3H32-H-52
- Product name
- 3,6-Diiodopyridazine
- Packaging
- 1g
- Price
- $88
- Updated
- 2021/12/16
- Product number
- 047829
- Product name
- 3,6-Diiodopyridazine
- Purity
- >95%
- Packaging
- 500mg
- Price
- $118
- Updated
- 2021/12/16
3,6-Diiodopyridazine Chemical Properties,Usage,Production
Uses
3,6-Diiodopyridazine is used as a reactant in the preparation of conjugated ethynyl and vinylpyridazines as rod-like conjugated molecules with light-emitting properties.
Synthesis
141-30-0
20698-04-8
Example 12 Synthesis of compound 12: To 2 g of 3,6-dichloropyridazine was added 60 ml of acetone and 20.12 g (268.4 mmol) of sodium iodide, and the mixture was stirred under reflux conditions (bath temperature: 70 °C) for 2 hours. After completion of the reaction, water was added to the reaction mixture and extracted with ethyl acetate. The organic layer was washed sequentially with saturated aqueous sodium thiosulfate and saturated aqueous sodium chloride, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 2.73 g (8.23 mmol) of 3,6-diiodopyridazine in 61% yield.
References
[1] Tetrahedron, 2015, vol. 71, # 40, p. 7670 - 7675
[2] Patent: WO2007/48802, 2007, A1. Location in patent: Page/Page column 91
[3] Journal of Heterocyclic Chemistry, 1999, vol. 36, # 5, p. 1135 - 1142
[4] Journal of Medicinal Chemistry, 1999, vol. 42, # 4, p. 669 - 676
[5] Patent: US5670492, 1997, A
3,6-Diiodopyridazine Preparation Products And Raw materials
Raw materials
Preparation Products
3,6-Diiodopyridazine Suppliers
- Tel
- 19713077352; 19713077352
- 1038096457@qq.com
- Country
- China
- ProdList
- 2802
- Advantage
- 58
- Tel
- 0838-5675166 15883665058
- Fax
- 0838-5675535
- nbcxkj@126.com
- Country
- China
- ProdList
- 937
- Advantage
- 55
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44802
- Advantage
- 61
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14101
- Advantage
- 59
- Tel
- 0571-82693216
- Fax
- +86-571-82880190
- info@yuhaochemical.com
- Country
- China
- ProdList
- 6387
- Advantage
- 52
- Tel
- 0531-81313138 13066006660
- Fax
- QQ: 3366077777
- chibapharm@foxmail.com
- Country
- China
- ProdList
- 3966
- Advantage
- 55
- Tel
- 0512-65617459 18915409046
- Fax
- 0512-65617459
- sales@sibian-chem.com
- Country
- China
- ProdList
- 1922
- Advantage
- 55
- Tel
- 027-86697669 13986148687
- Fax
- 86-027-86697669
- sales@tcaschem.com
- Country
- China
- ProdList
- 4036
- Advantage
- 55
View Lastest Price from 3,6-Diiodopyridazine manufacturers
- Product
- 3,6-Diiodopyridazine 20698-04-8
- Price
- US $3.00-9.00/KG
- Min. Order
- 0.1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2025-06-26
- Product
- 3,6-Diiodopyridazine 20698-04-8
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-11-02
- Product
- 3,6-Diiodopyridazine 20698-04-8
- Price
- US $5.00/KG
- Min. Order
- 5KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2019-08-02