2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER
- Product Name
- 2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER
- CAS No.
- 1128-00-3
- Chemical Name
- 2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER
- Synonyms
- Ethyl 2-aMinocyclohex-1-enecarboxylate;ethyl 2-aminocyclohexene-1-carboxylate;ETHYL 2-AMINO-1-CYCLOHEXENE-1-CARBOXYLATE;ETHYL 2-AMINOCYCLOHEX-1-ENE-1-CARBOXYLATE;ETHYL-(2-AMINOCYCLOHEX-1-EN-1-CARBOXYLAT);Ethyl 2-amino-1-cyclohexene-1-carboxylate,98%;2-Amino-1-cyclohexenecarboxylic acid ethyl ester;2-aminocyclohexene-1-carboxylic acid ethyl ester;2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER;1-Cyclohexene-1-carboxylicacid, 2-aMino-, ethyl ester
- CBNumber
- CB3666676
- Molecular Formula
- C9H15NO2
- Formula Weight
- 169.22
- MOL File
- 1128-00-3.mol
2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER Property
- Melting point:
- 70-74 °C
- Boiling point:
- 298.52°C (rough estimate)
- Density
- 1.0873 (rough estimate)
- refractive index
- 1.4580 (estimate)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- Crystals or Crystalline Powder
- pka
- 6.97±0.20(Predicted)
- color
- White to light yellow
Safety
- Safety Statements
- 24/25
- HS Code
- 29224999
N-Bromosuccinimide Price
- Product number
- E937155
- Product name
- Ethyl2-Amino-1-cyclohexene-1-carboxylate
- Packaging
- 500mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 2221AA
- Product name
- Ethyl2-aminocyclohex-1-enecarboxylate
- Packaging
- 1g
- Price
- $137
- Updated
- 2021/12/16
- Product number
- 118768
- Product name
- Ethyl 2-aminocyclohex-1-ene-1-carboxylate
- Purity
- >95%
- Packaging
- 500mg
- Price
- $138
- Updated
- 2021/12/16
- Product number
- OR322410
- Product name
- Ethyl 2-amino-1-cyclohexene-1-carboxylate
- Packaging
- 1g
- Price
- $156
- Updated
- 2021/12/16
- Product number
- 4458-1-08
- Product name
- Ethyl 2-amino-1-cyclohexene-1-carboxylate
- Packaging
- 1g
- Price
- $184
- Updated
- 2021/12/16
2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER Chemical Properties,Usage,Production
Chemical Properties
white to light yellow crystals or
Definition
ChEBI: Ethyl-2-amino-1-cyclohexene-1-carboxylate is an enamine and an enone.
Synthesis
1655-07-8
1128-00-3
a) To a solution of ethyl 2-cyclohexanone carboxylate (18.9 mL, 118 mmol) in methanol (120 mL) was added ammonium carbamate (9.20 g, 118 mmol). The reaction mixture was stirred at room temperature for 1 hour until the ammonium carbamate was completely dissolved. After continuing to stir the reaction mixture for 1 h, the volatile solvent was removed by distillation under reduced pressure to afford ethyl 2-amino-1-cyclohexene-1-carboxylate as a white to pale yellow solid (19.9 g, quantitative yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 1.28 (t, J = 7.2 Hz, 3H), 1.57-1.71 (m, 4H), 2.21 (t, J = 6.1 Hz, 2H), 2.26 (t, J = 6.1 Hz, 2H), 4.15 (q, J = 7.2 Hz, 2H), 6.06 (br s, 2H) .
References
[1] Patent: WO2013/26900, 2013, A1. Location in patent: Page/Page column 60
[2] New Journal of Chemistry, 2005, vol. 29, # 6, p. 769 - 772
[3] Tetrahedron Letters, 2013, vol. 54, # 9, p. 1133 - 1136
[4] Bioorganic and Medicinal Chemistry, 2014, vol. 22, # 14, p. 3654 - 3669
[5] Chemistry of Heterocyclic Compounds, 2006, vol. 42, # 6, p. 765 - 775
2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER manufacturers
- Product
- 2-AMINO-CYCLOHEX-1-ENECARBOXYLIC ACID ETHYL ESTER 1128-00-3
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000KG
- Release date
- 2024-07-16