ChemicalBook > CAS DataBase List > 3,5-BIS(TRIFLUOROMETHYL)ANISOLE

3,5-BIS(TRIFLUOROMETHYL)ANISOLE

Product Name: 3,5-BIS(TRIFLUOROMETHYL)ANISOLE
CAS No.: 349-60-0
Chemical Name: 3,5-BIS(TRIFLUOROMETHYL)ANISOLE
Synonyms: 3,5-Bis-trifluormethyl-aniso;3,5-BIS(TRIFLUOROMETHYL)ANISOLE;1-Methoxy-3,5-bis(trifluoromethyl)benzene;Benzene, 1-methoxy-3,5-bis(trifluoromethyl)-;1,3-Bis(trifluoromethyl)-5-methoxybenzene, 3,5-Bis(trifluoromethyl)phenyl methyl ether
CBNumber: CB3705645
Molecular Formula: C9H6F6O
Formula Weight: 244.13
MOL File: 349-60-0.mol

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3,5-BIS(TRIFLUOROMETHYL)ANISOLE Property

Boiling point:: 158-160°C
Density: 1.352
refractive index: 1.4075
Flash point:: 158-160°C
storage temp.: 2-8°C
Appearance: Colorless to light yellow Liquid
BRN: 2533238
CAS DataBase Reference: 349-60-0(CAS DataBase Reference)

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Safety

Hazard Codes: F
Risk Statements: 10
Safety Statements: 16
RIDADR: 3271
Hazard Note: Flammable
HazardClass: 3
PackingGroup: III
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H226Flammable liquid and vapour

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0020795
Product name: 3,5-BIS(TRIFLUOROMETHYL)ANISOLE
Purity: 95.00%
Packaging: 1G
Price: $149.1
Updated: 2021/12/16

AK Scientific

Product number: Z0532
Product name: 3,5-Bis(trifluoromethyl)anisole
Packaging: 25g
Price: $171
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2807-3-X5
Product name: 3,5-Bis(trifluoromethyl)anisole
Packaging: 25g
Price: $397
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0020795
Product name: 3,5-BIS(TRIFLUOROMETHYL)ANISOLE
Purity: 95.00%
Packaging: 25G
Price: $1170.48
Updated: 2021/12/16

Matrix Scientific

Product number: 005854
Product name: 3,5-Bis(trifluoromethyl)anisole
Packaging: 5g
Price: $44
Updated: 2021/12/16

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3,5-BIS(TRIFLUOROMETHYL)ANISOLE Chemical Properties,Usage,Production

Synthesis

328-70-1

124-41-4

349-60-0

The general procedure for the synthesis of 3,5-bis(trifluoromethyl)anisole from 3,5-bis(trifluoromethyl)bromobenzene and sodium methanol was as follows: 25 g of 1-bromo-3,5-bis(trifluoromethyl)benzene (85 mmol) was mixed with 366 mg of copper(I) bromide (CuBr, 3 mol%), 1.57 g of 18-crown-6 (7 mol%), and 92.3 g of sodium methanol in methanol ( 30% concentration, 21% precursor concentration) were mixed and heated to 105 °C. The reaction conversion was >97% as determined by GC (total reaction time 22 h). Subsequently, the reaction mixture was poured into 175 g of water and the pH was adjusted to 5-6 by dropwise addition of hydrochloric acid and then filtered through diatomaceous earth. The aqueous phase was extracted twice with 150 g of dichloromethane. The organic phases were combined and purified by vacuum fractional distillation to afford 16.5 g of 3,5-bis(trifluoromethyl)anisole (68 mmol, 79.4% yield) with a GC purity of >98.5%.

References

[1] Patent: US2008/71084, 2008, A1. Location in patent: Page/Page column 4

3,5-BIS(TRIFLUOROMETHYL)ANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,5-BIS(TRIFLUOROMETHYL)ANISOLE manufacturers

Honest Joy Holdings Limited

Product: 1-methoxy-3,5-bis(trifluoromethyl)benzene 349-60-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99.2%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: 3,5-BIS(TRIFLUOROMETHYL)ANISOLE 349-60-0
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2020-01-31

349-60-0, 3,5-BIS(TRIFLUOROMETHYL)ANISOLERelated Search:

3,5-BIS(TRIFLUOROMETHYL)ANISOLE

1-Methoxy-3,5-bis(trifluoromethyl)benzene

1,3-Bis(trifluoromethyl)-5-methoxybenzene, 3,5-Bis(trifluoromethyl)phenyl methyl ether

3,5-Bis-trifluormethyl-aniso

Benzene, 1-methoxy-3,5-bis(trifluoromethyl)-

349-60-0