N-DECYLBORONIC ACID
- Product Name
- N-DECYLBORONIC ACID
- CAS No.
- 24464-63-9
- Chemical Name
- N-DECYLBORONIC ACID
- Synonyms
- ecylboronicaci;Decylboronic acid;N-DECYLBORONIC ACI;N-DECYLBORONIC ACID;RARECHEM AH PB 0104;Boronic acid, B-decyl-;Decylboronic acid, 98.8%;1-Decylboronic acid, 98%;1-Decaneboronicacid (6CI);1-DECANEBORONICACID (6CI);
- CBNumber
- CB3755024
- Molecular Formula
- C10H23BO2
- Formula Weight
- 186.1
- MOL File
- 24464-63-9.mol
N-DECYLBORONIC ACID Property
- Melting point:
- 76-78°C
- Boiling point:
- 297.1±23.0 °C(Predicted)
- Density
- 0.883±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- pka
- 10.35±0.43(Predicted)
- Appearance
- White to off-white Solid
- Sensitive
- Air Sensitive
- BRN
- 1743934
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- D226938
- Product name
- N-Decylboronicacid
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- D226938
- Product name
- N-Decylboronicacid
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- BOR0000761
- Product name
- N-DECYLBORONIC ACID
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $143.64
- Updated
- 2021/12/16
- Product number
- OR360123
- Product name
- N-Decylboronicacid
- Packaging
- 5g
- Price
- $145
- Updated
- 2021/12/16
- Product number
- 090740
- Product name
- Decylboronic acid
- Purity
- 98%
- Packaging
- 1g
- Price
- $152
- Updated
- 2021/12/16
N-DECYLBORONIC ACID Chemical Properties,Usage,Production
Uses
suzuki reaction
Synthesis
55671-55-1
872-05-9
7732-18-5
24464-63-9
GENERAL STEPS: To a 100 mL round-bottomed flask was added a 2.1 M dichloromethane solution of dibromoborane-dimethyl sulfide complex (HBBr2-SMe2) (26.2 mL, ~55.0 mmol) and 1-decene (9.5 mL, 50.0 mmol) was added slowly and dropwise at 20 °C to the stirring solution. Subsequently, a dichloromethane solution (2.5 mL, 2.5 mmol) of 1 M boron tribromide (BBr3) was added dropwise at 0 °C. The reaction mixture was stirred at 0 °C for 15 min and then naturally warmed to 20 °C and continued stirring for 30 min. The reaction solution was slowly transferred to a flask containing a stirred mixture of ether (Et2O, 100 mL) and water (H2O, 20 mL) at 0 °C for hydrolysis, which was completed with stirring for 20 min. The mixture was transferred to a separatory funnel to minimize contact with air, and the aqueous layer was separated and discarded. The organic phase was washed sequentially with water (2 x 30 mL) and saturated brine (2 x 30 mL), dried with anhydrous magnesium sulfate, filtered and concentrated on a rotary evaporator. A free-flowing white powder product, n-decylboronic acid, was obtained in a yield of 8.71 g in 93% yield. The product was characterized by the following data: 1H NMR δ 6.50 (s, 2H), 1.41 (p, J = 7.8, 7.2 Hz, 2H), 1.28 (s, 14H), 0.92-0.84 (m, 3H), 0.71 (t, J = 7.8 Hz, 2H); 13C NMR δ 32.55, 32.07, 29.79, 29.73, 29.62, 29.50, 24.53, 23.50, 22.85, 14.28; 11B NMR δ 32.32.
References
[1] Journal of Organometallic Chemistry, 2018, vol. 865, p. 159 - 165
N-DECYLBORONIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-DECYLBORONIC ACID manufacturers
- Product
- N-DECYLBORONIC ACID 24463-63-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- MIn98%HPLC/LC
- Supply Ability
- 100KGS
- Release date
- 2020-10-29
- Product
- N-DECYLBORONIC ACID 24464-63-9
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08
- Product
- N-DECYLBORONIC ACI 24464-63-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg;5kg;100kg
- Release date
- 2019-07-04