6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE
- Product Name
- 6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE
- CAS No.
- 116081-18-6
- Chemical Name
- 6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE
- Synonyms
- 6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE;Oxazolo[5,4-b]pyridine, 6-bromo-2-methyl-
- CBNumber
- CB3816028
- Molecular Formula
- C7H5BrN2O
- Formula Weight
- 213.03
- MOL File
- Mol file
6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to light brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- HCH0353573
- Product name
- 6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.35
- Updated
- 2021/12/16
- Product number
- 2649AA
- Product name
- 6-Bromo-2-methyloxazolo[5,4-b]pyridine
- Packaging
- 250mg
- Price
- $447
- Updated
- 2021/12/16
- Product number
- AA10-4005
- Product name
- 6-Bromo-2-methyl-oxazolo[5,4-b]pyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $450
- Updated
- 2021/12/16
- Product number
- A192130
- Product name
- 6-Bromo-2-methyloxazolo[5,4-b]pyridine
- Purity
- 95%
- Packaging
- 100mg
- Price
- $151
- Updated
- 2021/12/16
- Product number
- A192130
- Product name
- 6-Bromo-2-methyloxazolo[5,4-b]pyridine
- Purity
- 95%
- Packaging
- 250mg
- Price
- $277
- Updated
- 2021/12/16
6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE Chemical Properties,Usage,Production
Synthesis
1445-45-0
98786-86-8
116081-18-6
Step 1: Synthesis of 6-bromo-2-methyloxazolo[5,4-b]pyridine 3-Amino-5-bromopyridin-2-ol (1.00 g, 5.29 mmol) was mixed with trimethyl orthoacetate (5 mL) and placed in a microwave reactor and the reaction was stirred at 120 °C for 2 hours. After completion of the reaction, the reaction mixture was concentrated and purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate = 5:1 to 1:1) to afford 550 mg (49% yield) of 6-bromo-2-methyloxazolo[5,4-b]pyridine as a white solid. LC-MS: m/z 212.8 [M + H]+. 1H NMR (400 MHz, CDCl3) δ [ppm]: 8.36 (d, J = 2.1 Hz, 1H), 8.08 (d, J = 2.1 Hz, 1H), 2.69 (s, 3H).
References
[1] Patent: US2015/225367, 2015, A1. Location in patent: Paragraph 0626
6-BROMO-2-METHYL-OXAZOLO[5,4-B]PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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