ChemicalBook > CAS DataBase List > 2,3-dihydro-5,6-dimethylpyrazine

2,3-dihydro-5,6-dimethylpyrazine

Product Name
2,3-dihydro-5,6-dimethylpyrazine
CAS No.
15986-92-2
Chemical Name
2,3-dihydro-5,6-dimethylpyrazine
Synonyms
DHP-1;DHDMP;Einecs 240-122-3;5,6-Dimethyl-2,3-dihydropyrazine;5,6-Dihydro-2,3-dimethylpyrazine;2,3-Dimethyl-5,6-dihydropyrazine;2,3-dihydro-5,6-dimethylpyrazine;Pyrazine, 2,3-dihydro-5,6-dimethyl-
CBNumber
CB3924723
Molecular Formula
C6H10N2
Formula Weight
110.16
MOL File
15986-92-2.mol
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2,3-dihydro-5,6-dimethylpyrazine Property

Boiling point:
60-63 °C(Press: 18 Torr)
Density 
1.02±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
6.73±0.20(Predicted)
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AccelPharmtech
Product number
E0019
Product name
2,3-dihydro-5,6-dimethyl-Pyrazine
Purity
97.00%
Packaging
1G
Price
$290
Updated
2021/12/16
Ambeed
Product number
A129782
Product name
5,6-Dimethyl-2,3-dihydropyrazine
Purity
95%
Packaging
1g
Price
$335
Updated
2021/12/16
Chemenu
Product number
CM168915
Product name
5,6-Dimethyl-2,3-dihydropyrazine
Purity
95%
Packaging
1g
Price
$468
Updated
2021/12/16
Crysdot
Product number
CD11245192
Product name
5,6-Dimethyl-2,3-dihydropyrazine
Purity
95+%
Packaging
1g
Price
$495
Updated
2021/12/16
Alichem
Product number
15986922
Product name
5,6-Dimethyl-2,3-dihydropyrazine
Packaging
1g
Price
$545
Updated
2021/12/16
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2,3-dihydro-5,6-dimethylpyrazine Chemical Properties,Usage,Production

Uses

5,?6-?Dimethyl-?2,?3-?dihydropyrazine can be used in studies of perfume composition comprising fragrance modulator compounds and silicic acid esters for increasing and prolonging the intensity of fragrance.

Synthesis

107-15-3

431-03-8

15986-92-2

Over a period of 2 hours, 2,3-butanedione (18.6 g, 216 mmol, dissolved in 200 mL of anhydrous ether) was added slowly and dropwise to a solution of ethylenediamine (13 g, 216 mmol) in anhydrous ether (600 mL). The reaction mixture was stirred continuously for 3 hours at room temperature. Subsequently, the clarified reaction solution was concentrated under reduced pressure to give a brown oily crude product. Purification of the crude product by reduced pressure distillation resulted in 16.6 g (70% yield) of the target compound 5,6-dimethyl-2,3-dihydropyrazine (Formula F) as a clarified yellow oil. The boiling point was 60 °C/16 mm Hg. Nuclear magnetic resonance hydrogen spectroscopy (NMR, CD3) data were as follows: δ 3.3 (broad single peak, 4H), 2.1 (single peak, 6H) ppm.

References

[1] Transition Metal Chemistry, 2013, vol. 38, # 1, p. 31 - 36
[2] Chemical and Pharmaceutical Bulletin, 2010, vol. 58, # 6, p. 825 - 828
[3] Patent: WO2005/79769, 2005, A2. Location in patent: Page/Page column 91
[4] Synthesis (Germany), 2013, vol. 45, # 11, p. 1546 - 1552
[5] Patent: EP1254899, 2002, A2. Location in patent: Page 46

2,3-dihydro-5,6-dimethylpyrazine Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3-dihydro-5,6-dimethylpyrazine Suppliers

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View Lastest Price from 2,3-dihydro-5,6-dimethylpyrazine manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
5,6-Dimethyl-2,3-dihydropyrazine 15986-92-2
Price
US $1.10/g
Min. Order
1g
Purity
99.0% min
Supply Ability
100 tons min
Release date
2025-09-24
Shaanxi Dideu New Materials Co. Ltd
Product
2,3-dihydro-5,6-dimethylpyrazine 15986-92-2
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
95.0%
Supply Ability
10000KGS
Release date
2025-03-13
Shaanxi Dideu Medichem Co. Ltd
Product
2,3-dihydro-5,6-dimethylpyrazine 15986-92-2
Price
US $0.10/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10
Release date
2024-08-04

15986-92-2, 2,3-dihydro-5,6-dimethylpyrazineRelated Search:


  • 2,3-dihydro-5,6-dimethylpyrazine
  • 2,3-Dimethyl-5,6-dihydropyrazine
  • 5,6-Dihydro-2,3-dimethylpyrazine
  • 5,6-Dimethyl-2,3-dihydropyrazine
  • DHDMP
  • DHP-1
  • Einecs 240-122-3
  • Pyrazine, 2,3-dihydro-5,6-dimethyl-
  • 15986-92-2