2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE

Product Name: 2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE
CAS No.: 7471-05-8
Chemical Name: 2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE
Synonyms: 4,5-Dihydro-2-(pyridin-2-yl)-1H-imidazole;NSC 403538;2-(4,5-Dihydro-2-imidazolyl)pyridine;2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE;Pyridine, 2-(4,5-dihydro-1H-imidazol-2-yl)-;2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE ISO 9001：2015 REACH
CBNumber: CB41013355
Molecular Formula: C8H9N3
Formula Weight: 147.18
MOL File: Mol file

More

Less

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE Property

Melting point:: 104-105℃
Boiling point:: 172-173℃ (6 Torr)
Density: 1.24±0.1 g/cm3 (20 ºC 760 Torr)
Flash point:: 121.8±25.1℃
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
pka: 8.92±0.40(Predicted)
color: Pale Yellow to Light Beige

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H319Causes serious eye irritation
Precautionary statements: P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

ChemScene

Product number: CS-W018360
Product name: 2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine
Packaging: 250mg
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD140106
Product name: 2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine
Packaging: 1g
Price: $197
Updated: 2021/12/16

AK Scientific

Product number: 1614AC
Product name: 2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine
Packaging: 250mg
Price: $204
Updated: 2021/12/16

AK Scientific

Product number: 1614AC
Product name: 2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine
Packaging: 1g
Price: $235
Updated: 2021/12/16

ChemScene

Product number: CS-W018360
Product name: 2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine
Packaging: 1g
Price: $300
Updated: 2021/12/16

More

Less

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE Chemical Properties,Usage,Production

Uses

2-(4,5-Dihydro-1H-imidazol-2-yl)pyridine is used in preparation of γ-lactam and δ-lactam by C-H amination.

Synthesis

100-70-9

107-15-3

7471-05-8

Typical reactions were carried out under microwave radiation conditions. A mixture of 2-cyanopyridine (10 mmol), ethylenediamine (40 mmol) and Cu(II)-(IAA)2 (2.0 mmol) was placed in a microwave reactor and irradiated with pulses at a power of 1000 W for 5-20 min. The reaction process was monitored by thin layer chromatography (TLC) with an eluent ratio of ethyl acetate/methanol (3:1). Upon completion of the reaction, the mixture was cooled to room temperature and diluted by addition of dichloromethane (CH2Cl2), followed by filtration to remove the catalyst. The solvent was removed by rotary evaporation to give almost pure 2-(4,5-dihydro-1H-imidazol-2-yl)pyridine. For further purification, the standard method for the synthesis of imidazolines under reflux conditions can be used. The structure of the product was confirmed by melting point (mp), nuclear magnetic resonance hydrogen spectroscopy (1H NMR), mass spectrometry (MS) and infrared spectroscopy (IR) data.

References

[1] Journal of the Serbian Chemical Society, 2012, vol. 77, # 9, p. 1181 - 1189,9
[2] Canadian Journal of Chemistry, 2010, vol. 88, # 2, p. 135 - 141
[3] Monatshefte fur Chemie, 2007, vol. 138, # 6, p. 579 - 583
[4] Tetrahedron Letters, 2011, vol. 52, # 14, p. 1578 - 1582
[5] Tetrahedron Letters, 2006, vol. 47, # 13, p. 2129 - 2132

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE Suppliers

China 30 United Kingdom 2 United States 2 Global 34

Synyoo New Materials Co., Ltd.

Tel: 0757-82582588
Fax: 0757-82582503
Email: sales@synyoo.com
Country: China
ProdList: 75
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Struchem Co., Ltd.

Tel: 0512-63009836 18994340901
Fax: 0512-63006936
Email: helen@struchem.com
Country: China
ProdList: 3981
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

9ding chemical ( Shanghai) Limited

Tel: 021-021-52271985 17721149837
Fax: +86 (21) 52271987
Email: sales@9dingchem.com
Country: China
ProdList: 19800
Advantage: 60

Biokitchen

Tel: 021-021-021-31663258 13795219287
Fax: 021-31663258
Email: donghuanwen@126.com
Country: China
ProdList: 8816
Advantage: 58

Suzhou Nuoouman Biological Technology Co., Ltd.

Tel: 15026866316
Email: 180642609@qq.com
Country: China
ProdList: 4967
Advantage: 58

Zhengzhou Ruke Biological Co., Ltd.

Tel: 15981811963
Fax: QQ：1410472904
Email: 1410472904@qq.com
Country: China
ProdList: 5825
Advantage: 58

More

Less

View Lastest Price from 2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE manufacturers

Dideu Industries Group Limited

Product: 2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE 7471-05-8
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-21

7471-05-8, 2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINERelated Search:

Aluminum hydroxide

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE

4,5-Dihydro-2-(pyridin-2-yl)-1H-imidazole

NSC 403538

Pyridine, 2-(4,5-dihydro-1H-imidazol-2-yl)-

2-(4,5-DIHYDRO-1H-IMIDAZOL-2-YL)PYRIDINE ISO 9001：2015 REACH

2-(4,5-Dihydro-2-imidazolyl)pyridine

7471-05-8

7174-05-8