Cyclohexanol, 4-amino-1-methyl- (9CI)
- Product Name
- Cyclohexanol, 4-amino-1-methyl- (9CI)
- CAS No.
- 233764-32-4
- Chemical Name
- Cyclohexanol, 4-amino-1-methyl- (9CI)
- Synonyms
- 4-AMino-1-Methylcyclohexanol;4-aMino-1-Methylcyclohexan-1-ol;Cyclohexanol, 4-amino-1-methyl- (9CI)
- CBNumber
- CB41045893
- Molecular Formula
- C7H15NO
- Formula Weight
- 129.2
- MOL File
- 233764-32-4.mol
Cyclohexanol, 4-amino-1-methyl- (9CI) Property
- storage temp.
- Store at Room Tem.
N-Bromosuccinimide Price
- Product number
- CHM0960409
- Product name
- 4-AMINO-1-METHYLCYCLOHEXAN-1-OL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.61
- Updated
- 2021/12/16
- Product number
- 4256-1-67
- Product name
- 4-Amino-1-methylcyclohexan-1-ol
- Purity
- 97.0%
- Packaging
- 250mg
- Price
- $638
- Updated
- 2021/12/16
- Product number
- 113466
- Product name
- 4-Amino-1-methylcyclohexanol
- Packaging
- 1g
- Price
- $1131
- Updated
- 2021/12/16
- Product number
- 4256-1-67
- Product name
- 4-Amino-1-methylcyclohexan-1-ol
- Purity
- 97.0%
- Packaging
- 1g
- Price
- $1790
- Updated
- 2021/12/16
- Product number
- CM107589
- Product name
- 4-amino-1-methylcyclohexan-1-ol
- Purity
- 97%
- Packaging
- 1g
- Price
- $658
- Updated
- 2021/12/16
Cyclohexanol, 4-amino-1-methyl- (9CI) Chemical Properties,Usage,Production
Synthesis
952745-69-6
233764-32-4
Step 4: Synthesis of 4-amino-1-methylcyclohexanol 4-(Benzylamino)-1-methylcyclohexanol (4.9 g, 22.3 mmol) was dissolved in methanol (150 mL) and 7% Pd/C (700 mg) was added at 7 °C. The reaction was carried out overnight under hydrogen atmosphere. Upon completion of the reaction, the mixture was filtered to remove the Pd/C catalyst, and the filtrate was concentrated under vacuum to give a white solid product, 4-amino-1-methylcyclohexanol (2.9 g, quantitative yield), which could be used directly in the subsequent steps without further purification.
References
[1] Patent: WO2014/9302, 2014, A1. Location in patent: Page/Page column 90; 91
[2] Patent: US2015/158879, 2015, A1. Location in patent: Paragraph 0443; 0444
[3] Patent: US2016/200741, 2016, A1. Location in patent: Paragraph 0444-0445
[4] Patent: WO2011/139107, 2011, A2. Location in patent: Page/Page column 108-109
Cyclohexanol, 4-amino-1-methyl- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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