2,3-DIBROMO-4-PICOLINE

Product Name: 2,3-DIBROMO-4-PICOLINE
CAS No.: 871483-22-6
Chemical Name: 2,3-DIBROMO-4-PICOLINE
Synonyms: 2,3-DIBROMO-4-PICOLINE;Pyridine, 2,3-dibromo-4-methyl-
CBNumber: CB41075988
Molecular Formula: C6H5Br2N
Formula Weight: 250.92
MOL File: Mol file

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2,3-DIBROMO-4-PICOLINE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Off-white to light brown Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FD140902
Product name: 2,3-Dibromo-4-methylpyridine
Packaging: 250mg
Price: $150
Updated: 2021/12/16

AK Scientific

Product number: 3761AC
Product name: 2,3-Dibromo-4-methylpyridine
Packaging: 1g
Price: $284
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD140902
Product name: 2,3-Dibromo-4-methylpyridine
Packaging: 500mg
Price: $260
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0295499
Product name: 2,3-DIBROMO-4-METHYLPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $500.61
Updated: 2021/12/16

Chemenu

Product number: CM128389
Product name: 2,3-dibromo-4-methylpyridine
Purity: 97%
Packaging: 5g
Price: $1061
Updated: 2021/12/16

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2,3-DIBROMO-4-PICOLINE Chemical Properties,Usage,Production

Synthesis

40073-38-9

871483-22-6

General procedure for the synthesis of 2,3-dibromo-4-methylpyridine from 2-amino-3-bromo-4-methylpyridine: Bromine (0.35 mL, 6.8 mmol) was slowly added dropwise to a solution of 3-bromo-4-methylpyridin-2-amine (0.44 g, 2.4 mmol) dissolved in 48% hydrobromic acid (3 mL) to form an orange slurry at -10 °C. 5 minutes later, sodium nitrite (0.47 g, 6.8 mmol) dissolved in water (1.5 mL) was added dropwise over 5 minutes. The reaction mixture was slowly warmed to 10 °C, held for 3.5 h, then cooled to 0 °C and the reaction was quenched with 10 N sodium hydroxide solution until the pH reached about 12. The resulting orange slurry was extracted with dichloromethane (3 x 50 mL), the organic phase was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give an orange to brown solid. Purification by silica gel column chromatography (eluent: hexane/ether, 7:3, v/v) afforded 2,3-dibromo-4-methylpyridine (0.28 g, 47% yield) as a light yellow solid.1H NMR (CDCl3) δ 2.48 (s, 3H), 7.11 (d, 1H, J = 6.0 Hz), 8.16 (d, 1H, J = 6.0 Hz).

References

[1] Patent: US2005/277668, 2005, A1. Location in patent: Page/Page column 28

2,3-DIBROMO-4-PICOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3-DIBROMO-4-PICOLINE Suppliers

China 49 India 4 United Kingdom 2 United States 9 Global 64

Capot Chemical Co., Ltd

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Nanijing m&m biotechnology Co. ,Ltd.

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View Lastest Price from 2,3-DIBROMO-4-PICOLINE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2,3-DIBROMO-4-PICOLINE 871483-22-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-12

Shaanxi Dideu Medichem Co. Ltd

Product: 2,3-Dibromo-4-picoline 871483-22-6
Price: US $0.10/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000 tons
Release date: 2019-12-27

Career Henan Chemical Co

Product: 2,3-Dibromo-4-picoline 871483-22-6
Price: US $1.00/KG
Min. Order: 1g
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-09

871483-22-6, 2,3-DIBROMO-4-PICOLINERelated Search:

2,3-DIBROMO-4-PICOLINE

Pyridine, 2,3-dibromo-4-methyl-

871483-22-6