2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE

Product Name: 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE
CAS No.: 55860-22-5
Chemical Name: 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE
Synonyms: SKL827;NSC 8284;AKOS B015640;ASISCHEM U00018;AKOS USSH-4110470;AKOS BBS-00003901;ART-CHEM-BB B015640;CHEMBRDG-BB 3015640;2-chloroacetanisidide;2-chloro-o-acetanisidid
CBNumber: CB4113102
Molecular Formula: C9H10ClNO2
Formula Weight: 199.63
MOL File: 55860-22-5.mol

More

Less

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Property

Melting point:: 51 °C(Solv: ethanol (64-17-5))
Boiling point:: 339.0±22.0 °C(Predicted)
Density: 1.264±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 12.27±0.70(Predicted)
Appearance: Light brown to brown Solid
CAS DataBase Reference: 55860-22-5(CAS DataBase Reference)

More

Less

Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2924297099

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S854948
Product name: 2-CHLORO-2'-METHOXYACETANILIDE
Purity: Aldrich
Packaging: 50mg
Price: $28.6
Updated: 2023/06/20

TRC

Product number: C376863
Product name: 2-chloro-N-(2-methoxyphenyl)acetamide
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C376863
Product name: 2-chloro-N-(2-methoxyphenyl)acetamide
Packaging: 250mg
Price: $110
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC58981
Product name: 2-chloro-n-(2-methoxyphenyl)acetamide
Packaging: 500mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 029474
Product name: 2-Chloro-N-(2-methoxyphenyl)acetamide
Packaging: 500mg
Price: $95
Updated: 2021/12/16

More

Less

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Chemical Properties,Usage,Production

Synthesis

90-04-0

79-04-9

55860-22-5

The general procedure for the synthesis of 2-chloro-N-(2-methoxyphenyl)acetamide from o-methoxyaniline (0.5 g, 4.05 mmol) and chloroacetyl chloride (0.387 mL, 4.87 mmol) was as follows: to a solution of acetonitrile (10.0 mL) of o-methoxyaniline under argon gas protection was added N,N-diisopropyl ethylamine (DIPEA, 1.56 mL 8.93 mmol), followed by slow dropwise addition of chloroacetyl chloride. After the dropwise addition, the reaction mixture was stirred at room temperature for 1 hour. The reaction process was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was concentrated and purified by column chromatography (eluent: 20% ethyl acetate/hexane) to afford the target compound 2-chloro-N-(2-methoxyphenyl)acetamide as a brown solid (0.72 g, 89.05% yield). The structure of the product was confirmed by 1H NMR (CDCl3, 400 MHz): δ 8.96 (s, 1H), 8.35 (dd, J = 1.6, 8.0 Hz, 1H), 7.14-7.10 (m, 1H), 7.02-6.97 (m, 1H), 6.94-6.91 (m, 1H), 4.21 (s, 2H), 3.93 (s, 3H).

References

[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 14, p. 6289 - 6304
[2] Bioorganic and Medicinal Chemistry, 2014, vol. 22, # 24, p. 6885 - 6892
[3] Farmaco, 2002, vol. 57, # 3, p. 201 - 206
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006, vol. 45, # 8, p. 1871 - 1879
[5] Bioorganic and Medicinal Chemistry, 2004, vol. 12, # 13, p. 3471 - 3483

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Suppliers

China 47 Germany 3 India 2 Russia 1 Ukraine 2 United Kingdom 4 United States 10 Global 69

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
Fax: 86-027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 35896
Advantage: 56

Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd

Tel: 18210788515
Fax: 18210788515
Email: zhuzixin999@163.c0m
Country: China
ProdList: 2998
Advantage: 55

Wuhan Chemwish Technology Co.， Ltd

Tel: 027-67849912
Fax: 027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 9148
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Yantai ShengKailun Chemical Technology Co., Ltd.

Tel: 13356901049
Fax: QQ：1025383091
Email: 3119594100@qq.com
Country: China
ProdList: 7964
Advantage: 55

Dalian lichuang Chemical Co., Ltd

Tel: 0411-0411-00000000 13644282108
Fax: -
Email: 3500508746@qq.com
Country: China
ProdList: 2896
Advantage: 55

Aikon International Limited

Tel: 025-58851090 15955137747
Fax: (6)02557626880
Email: sales01@aikonchem.com
Country: China
ProdList: 15949
Advantage: 58

Shanghai Thunder Biological Technology Co., Ltd.

Tel: 18621609968
Email: 1162686636@qq.com
Country: China
ProdList: 874
Advantage: 58

More

Less

View Lastest Price from 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE manufacturers

Career Henan Chemical Co

Product: 2-Chloro-N-(2-methoxyphenyl)acetamide 55860-22-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

55860-22-5, 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDERelated Search:

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE N1-(2,4-DIMETHOXYPHENYL)-2-CHLOROACETAMIDE N-(2-Methoxyphenyl)acetamide 2-CHLORO-N-(2,5-DIMETHOXYPHENYL)ACETAMIDE 2-Chloro-N-(2-methoxy-4-nitro-phenyl)-acetamide 2-CHLORO-N-(2-PHENOXY-PHENYL)-ACETAMIDE 2-CHLORO-N-(5-CHLORO-2,4-DIMETHOXYPHENYL)ACETAMIDE 2-CHLORO-N-(2-ETHOXYPHENYL)ACETAMIDE 3-(2-CHLORO-ACETYL)-3H-BENZOOXAZOL-2-ONE 2-CHLORO-N-(5-CHLORO-2-METHOXYPHENYL)ACETAMIDE 2-CHLORO-N-(2-METHOXY-5-METHYLPHENYL)ACETAMIDE 2-CHLORO-N-(4-CHLORO-2,5-DIMETHOXYPHENYL)ACETAMIDE N1-[2-(2,4-DICHLOROPHENOXY)PHENYL]-2-CHLOROACETAMIDE N1-[2-(4-CHLORO-3,5-DIMETHYLPHENOXY)-5-(TRIFLUOROMETHYL)PHENYL]-2,3,3-TRICHLOROACRYLAMIDE AURORA KA-4065 AKOS BBS-00005468 N1-[2-(4-CYANOPHENOXY)-5-(TRIFLUOROMETHYL)PHENYL]-2-CHLOROACETAMIDE N1-[2-(4-CHLORO-3,5-DIMETHYLPHENOXY)-5-(TRIFLUOROMETHYL)PHENYL]-2-CHLOROACETAMIDE

ART-CHEM-BB B015640

ASISCHEM U00018

CHEMBRDG-BB 3015640

ACETAMIDE, 2-CHLORO-N-(2-METHOXYPHENYL)-

AKOS B015640

AKOS BBS-00003901

AKOS USSH-4110470

2-chloro-2’-methoxyacetanilide

2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE

2-chloroacetanisidide

2-chloro-o-acetanisidid

2-chloro-N-(2-methoxyphenyl)acetamide(SALTDATA: FREE)

2-Chloro-2'-methoxyacetanlide

2-Chloro-o-acetanisidide

N-(2-Anisyl)chloroacetamide

N-Chloroacetyl-2-methoxyaniline

NSC 8284

o-Acetanisidide,2-chloro-(6CI)

2-chloro-N-(2-methoxyphenyl)ethanamide

o-ACETANISIDIDE, 2-CHLORO-

SKL827

2-CHLORO-2'-METHOXYACETANILIDE

55860-22-5