METHYL (2-NITRO-PHENYL)-ACETATE
- Product Name
- METHYL (2-NITRO-PHENYL)-ACETATE
- CAS No.
- 30095-98-8
- Chemical Name
- METHYL (2-NITRO-PHENYL)-ACETATE
- Synonyms
- Benzocaine Impurity 12;Methyl o-nitrophenylacetate;METHYL (NITRO-PHENYL)-ACETATE;METHYL (2-NITRO-PHENYL)-ACETATE;METHYL 2-(2-NITROPHENYL)ACETATE;METHYL2-(2-NITHROPHENYL)-ACETATE;2-Nitrobenzeneacetic acid methyl;2-(2-Nitrophenyl)acetic acid methyl;o-Nitrophenylacetic acid methyl ester;(2-Nitrophenyl)acetic acid, methyl ester
- CBNumber
- CB4115520
- Molecular Formula
- C9H9NO4
- Formula Weight
- 195.17
- MOL File
- 30095-98-8.mol
METHYL (2-NITRO-PHENYL)-ACETATE Property
- Boiling point:
- 112-115°/2mm
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to brown Solid-Liquid Mixture
Safety
- HS Code
- 2915390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- PH004629
- Product name
- methyl (2-nitrophenyl)acetate
- Purity
- AldrichCPR
- Packaging
- 1MG
- Price
- $134
- Updated
- 2023/06/20
- Product number
- B495365
- Product name
- Methyl2-(2-Nitrophenyl)acetate
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 113936
- Product name
- Methyl (2-nitrophenyl)acetate
- Purity
- 97%
- Packaging
- 1g
- Price
- $197
- Updated
- 2021/12/16
- Product number
- CHM1043039
- Product name
- (2-NITRO-PHENYL)-ACETIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $501.57
- Updated
- 2021/12/16
- Product number
- 05R0121
- Product name
- Methyl(2-nitro-phenyl)-acetate
- Purity
- 97%
- Packaging
- 100g
- Price
- $680
- Updated
- 2021/12/16
METHYL (2-NITRO-PHENYL)-ACETATE Chemical Properties,Usage,Production
Synthesis
3740-52-1
30095-98-8
General procedure for the synthesis of methyl (2-nitrophenyl)acetate from o-nitrophenylacetic acid: (A) Preparation of methyl 2-(2-nitrophenyl)acetate 2-(2-Nitrophenyl)acetic acid (5.06 g, 27.9 mmol) was dissolved in methanol (100 mL) and concentrated sulfuric acid (5 mL) was added slowly and dropwise. The reaction mixture was heated under reflux conditions for 16 hours. Upon completion of the reaction, the solvent was removed by evaporation and water was added to the residue, which was subsequently extracted with ethyl acetate. The organic layer was washed sequentially with saturated aqueous sodium bicarbonate and saturated brine and dried over anhydrous sodium sulfate. Evaporation of the solvent gave the title compound as a light orange oil (5.37 g, 99.0% yield). 1H-NMR (CDCl3) δ: 3.72 (3H, s), 4.03 (2H, s), 7.36 (1H, d, J = 7.3 Hz), 7.44-7.51 (1H, m), 7.57-7.63 (1H, m), 8.12 (1H, d, J = 7.8 Hz).
References
[1] Patent: EP1227084, 2002, A1
[2] Patent: CN106831436, 2017, A. Location in patent: Paragraph 0016; 0017; 0019
[3] Patent: US5240938, 1993, A
[4] Patent: US2005/101587, 2005, A9
[5] Angewandte Chemie - International Edition, 2012, vol. 51, # 2, p. 548 - 551
METHYL (2-NITRO-PHENYL)-ACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
METHYL (2-NITRO-PHENYL)-ACETATE Suppliers
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11035
- Advantage
- 64
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- 010-59484199 18611897322
- sales@eternalchem.com
- Country
- China
- ProdList
- 4383
- Advantage
- 60
- Tel
- 18270980682
- Fax
- 021 51613951
- mlcheng@sunwaypharm.cn
- Country
- China
- ProdList
- 8669
- Advantage
- 57
- Tel
- 021-58170097
- info@topbiochem.com
- Country
- China
- ProdList
- 9510
- Advantage
- 58
- Tel
- +86-21-60341587
- Fax
- +86-21-61294319
- sales@topbiochem.com
- Country
- China
- ProdList
- 6175
- Advantage
- 58
- Tel
- 18652989687
- Fax
- +86-25-52131256
- sales@norris-pharm.com
- Country
- China
- ProdList
- 8878
- Advantage
- 55
- Tel
- 025-66113011 17798518460
- Fax
- (1)02557626880
- cfzhang@aikonchem.com
- Country
- China
- ProdList
- 19913
- Advantage
- 55
- Tel
- 021-57171705 13817537615
- Fax
- QQ3095748324
- sales@run-biotech.com
- Country
- China
- ProdList
- 2334
- Advantage
- 58
View Lastest Price from METHYL (2-NITRO-PHENYL)-ACETATE manufacturers
- Product
- METHYL (2-NITRO-PHENYL)-ACETATE 30095-98-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-07-18