1H-Benzimidazol-6-amine,1-methyl-(9CI)

Product Name: 1H-Benzimidazol-6-amine,1-methyl-(9CI)
CAS No.: 26530-93-8
Chemical Name: 1H-Benzimidazol-6-amine,1-methyl-(9CI)
Synonyms: 3-methylbenzimidazol-5-amine;3-methyl-5-benzimidazolamine;6-Amino-1-methylbenzimidazole;(3-methylbenzimidazol-5-yl)amine;1-methyl-1H-benzimidazol-6-amine;1H-benzimidazol-6-amine, 1-methyl-;1-Methyl-1H-benzo[d]imidazol-6-amine;1H-Benzimidazol-6-amine,1-methyl-(9CI);1-methyl-1H-benzimidazol-6-amine(SALTDATA: FREE)
CBNumber: CB41286027
Molecular Formula: C8H9N3
Formula Weight: 147.18
MOL File: 26530-93-8.mol

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1H-Benzimidazol-6-amine,1-methyl-(9CI) Property

Melting point:: 160 °C
Boiling point:: 180-185 °C(Press: 4 Torr)
Density: 1.27±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 6.16±0.10(Predicted)
Appearance: Off-white to pink Solid

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Safety

Risk Statements: 41
Safety Statements: 26-39
HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H225Highly Flammable liquid and vapour

H318Causes serious eye damage

H320Causes eye irritation

H335May cause respiratory irritation

H336May cause drowsiness or dizziness

Precautionary statements

P242Use only non-sparking tools.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

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N-Bromosuccinimide Price

TRC

Product number: M782768
Product name: 1-methyl-1H-benzimidazol-6-amineDihydrochloride
Packaging: 50mg
Price: $155
Updated: 2021/12/16

Apolloscientific

Product number: OR942168
Product name: 1-Methyl-1H-benzimidazol-6-amine
Purity: 95%
Packaging: 250mg
Price: $120
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H30-1-PE
Product name: 1-Methyl-1H-benzimidazol-6-amine
Purity: 95%
Packaging: 250mg
Price: $192
Updated: 2021/12/16

Matrix Scientific

Product number: 063274
Product name: 1-Methyl-1H-benzimidazol-6-amine
Packaging: 500mg
Price: $195
Updated: 2021/12/16

Apolloscientific

Product number: OR942168
Product name: 1-Methyl-1H-benzimidazol-6-amine
Purity: 95%
Packaging: 1g
Price: $275
Updated: 2021/12/16

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1H-Benzimidazol-6-amine,1-methyl-(9CI) Chemical Properties,Usage,Production

Synthesis

5381-79-3

5381-78-2

10394-38-4

26530-93-8

General method: Step B: 1-methyl-6-nitro-1H-benzo[d]imidazole or 1-methyl-5-nitro-1H-benzo[d]imidazole is dissolved in methanol (or a solvent mixture of methanol and tetrahydrofuran), followed by the addition of 10% palladium/carbon catalyst. The reaction mixture was stirred at room temperature in a hydrogen atmosphere until thin layer chromatography (TLC) monitoring showed complete consumption of the feedstock. Upon completion of the reaction, the crude reaction solution was filtered through a diatomaceous earth pad and the filter cake was washed well with methanol. The filtrate was concentrated under reduced pressure and the resulting products, 1-methylbenzimidazol-5-amine or 1-methyl-1H-benzimidazol-6-amine, could be used directly in the subsequent reaction or further purified by silica gel column chromatography to obtain higher purity products.

References

[1] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 13, p. 3821 - 3830

1H-Benzimidazol-6-amine,1-methyl-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-Benzimidazol-6-amine,1-methyl-(9CI) Suppliers

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