2-amino-6-nitro-phenol
- Product Name
- 2-amino-6-nitro-phenol
- CAS No.
- 603-87-2
- Chemical Name
- 2-amino-6-nitro-phenol
- Synonyms
- NSC 87541;2-amino-6-nitro-phenol;Phenol, 2-amino-6-nitro-;tert-butyl (2-hydroxy-3-nitrophenyl)carbamate
- CBNumber
- CB41458464
- Molecular Formula
- C6H6N2O3
- Formula Weight
- 154.12
- MOL File
- 603-87-2.mol
2-amino-6-nitro-phenol Property
- Melting point:
- >280 °C
- Boiling point:
- 280.3±25.0 °C(Predicted)
- Density
- 1.511±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 6.85±0.24(Predicted)
- Appearance
- Brown to reddish brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
H341Suspected of causing genetic defects
- Precautionary statements
-
P201Obtain special instructions before use.
P202Do not handle until all safety precautions have been read and understood.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P281Use personal protective equipment as required.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P308+P313IF exposed or concerned: Get medical advice/attention.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- A619845
- Product name
- 2-Amino-6-nitrophenol
- Packaging
- 25mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- FA141984
- Product name
- 2-Amino-6-nitrophenol
- Packaging
- 250mg
- Price
- $160
- Updated
- 2021/12/16
- Product number
- Y9591
- Product name
- 2-Amino-6-nitrophenol
- Packaging
- 250mg
- Price
- $266
- Updated
- 2021/12/16
- Product number
- FA141984
- Product name
- 2-Amino-6-nitrophenol
- Packaging
- 500mg
- Price
- $275
- Updated
- 2021/12/16
- Product number
- Y9591
- Product name
- 2-Amino-6-nitrophenol
- Packaging
- 500mg
- Price
- $421
- Updated
- 2021/12/16
2-amino-6-nitro-phenol Chemical Properties,Usage,Production
Synthesis
573-56-8
603-87-2
The general procedure for the synthesis of 2-amino-6-nitrophenol from 2,6-dinitrophenol was as follows: a suspension of 2,6-dinitrophenol (5.0 g, 27 mmol), ammonium hydroxide (3 ml) and ammonium chloride (14 g) was mixed with 30 ml of water. To the mixture was added an aqueous solution of sodium sulfide hydrate nine (24.19 g, 100 mmol), followed by heating the reaction system to 70°C and stirring for 2 hours. After completion of the reaction, the mixture was cooled to room temperature, acidified to pH 3.2 with 2N HCl and filtered to collect the brown precipitate. The filtrate was extracted with chloroform (6 x 75 ml) and after combining the organic extract with the precipitate, the solvent was removed by vacuum evaporation to afford the dark brown solid product 2-amino-6-nitrophenol (2.5 g, 60% yield). The structure of the product was confirmed by 1H NMR (CDCl3): δ 4.09 (s, 2H), 6.78 (t, 1H, J = 8.2 Hz), 6.95 (d, 1H, J = 7.8 Hz), 7.47 (d, 1H, J = 8.6 Hz), 10.73 (s, 3H).
References
[1] Patent: WO2005/28445, 2005, A2. Location in patent: Page/Page column 38
[2] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 15, p. 3521 - 3525
[3] Journal of Medicinal Chemistry, 2004, vol. 47, # 6, p. 1319 - 1321
[4] Patent: WO2005/44793, 2005, A2. Location in patent: Page/Page column 135
[5] Patent: US2014/309208, 2014, A1. Location in patent: Paragraph 0237; 0238
2-amino-6-nitro-phenol Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-amino-6-nitro-phenol manufacturers
- Product
- 2-Amino-6-nitro-phenol 603-87-2
- Price
- US $0.00-0.00/G
- Min. Order
- 1G
- Purity
- 99%
- Supply Ability
- 2000tons
- Release date
- 2025-08-15