2,3-DIMETHYL-4-METHOXYBENZOIC ACID
- Product Name
- 2,3-DIMETHYL-4-METHOXYBENZOIC ACID
- CAS No.
- 5628-61-5
- Chemical Name
- 2,3-DIMETHYL-4-METHOXYBENZOIC ACID
- Synonyms
- RARECHEM AL BE 0657;2,3-DIMETHYL-4-METHOXYBENZOIC ACID;4-Methoxy-2,3-diMethylbenzoic acid;Benzoic acid, 4-Methoxy-2,3-diMethyl-
- CBNumber
- CB4147972
- Molecular Formula
- C10H12O3
- Formula Weight
- 180.2
- MOL File
- Mol file
2,3-DIMETHYL-4-METHOXYBENZOIC ACID Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to light yellow Solid
Safety
- HazardClass
- IRRITANT
- HS Code
- 2918290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 2721-1-15
- Product name
- 2,3-Dimethyl-4-methoxybenzoic acid
- Purity
- 98%
- Packaging
- 1g
- Price
- $66
- Updated
- 2021/12/16
- Product number
- OR47850
- Product name
- 2,3-Dimethyl-4-methoxybenzoicacid
- Packaging
- 1g
- Price
- $73
- Updated
- 2021/12/16
- Product number
- CS-M2517
- Product name
- Benzoicacid,4-methoxy-2,3-dimethyl-
- Packaging
- 100mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- CS-M2517
- Product name
- Benzoicacid,4-methoxy-2,3-dimethyl-
- Packaging
- 250mg
- Price
- $142
- Updated
- 2021/12/16
- Product number
- 056852
- Product name
- 2,3-Dimethyl-4-methoxybenzoic acid
- Purity
- 98%
- Packaging
- 1g
- Price
- $210
- Updated
- 2021/12/16
2,3-DIMETHYL-4-METHOXYBENZOIC ACID Chemical Properties,Usage,Production
Synthesis
38998-17-3
5628-61-5
General procedure for the synthesis of 4-methoxy-2,3-dimethylbenzoic acid from 4-methoxy-2,3-dimethylbenzaldehyde: 60.0 g of 4-methoxy-2,3-dimethylbenzaldehyde was dissolved in 1.20 L of dimethyl sulfoxide. Subsequently, a solution prepared by dissolving 131.5 g of sodium dihydrogen phosphate and 132.2 g of sodium chlorite in 480 mL of water was added dropwise, during which the reaction temperature was controlled not to exceed 40 °C. After addition, the reaction mixture was continued to be stirred at room temperature for 2 hours. Upon completion of the reaction, the suspension was diluted with 2.0 L of water, the precipitate was collected by filtration, washed with water and dried under vacuum at 100 °C to afford 65.0 g of the target product 4-methoxy-2,3-dimethylbenzoic acid as a colorless solid with a melting point of 214 °C (MS: 181.2 [MH+]).
References
[1] Patent: US2011/60050, 2011, A1. Location in patent: Page/Page column 4
[2] Patent: US2011/224302, 2011, A1. Location in patent: Page/Page column 10; 15
[3] Bioorganic Chemistry, 1996, vol. 24, # 4, p. 386 - 400
[4] Patent: EP1666473, 2006, A1. Location in patent: Page/Page column 41
2,3-DIMETHYL-4-METHOXYBENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
2,3-DIMETHYL-4-METHOXYBENZOIC ACID Suppliers
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