ChemicalBook > CAS DataBase List > 2-bromo-6-methoxy-aniline

2-bromo-6-methoxy-aniline

Product Name
2-bromo-6-methoxy-aniline
CAS No.
5473-01-8
Chemical Name
2-bromo-6-methoxy-aniline
Synonyms
Nsc29554;2-Amino-3-bromoanisole;2-Bromo-6-methoxyaniline97%;2-Bromo-6-methoxyaniline 97%;2-BroMo-6-Methoxy-phenylaMine;BenzenaMine, 2-broMo-6-Methoxy-;2-Amino-3-bromoanisole, 6-Bromo-o-anisidine
CBNumber
CB41480038
Molecular Formula
C7H8BrNO
Formula Weight
202.05
MOL File
5473-01-8.mol
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2-bromo-6-methoxy-aniline Property

Boiling point:
251.3±20.0 °C(Predicted)
Density 
1.531±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
2.48±0.10(Predicted)
form 
liquid
color 
Yellow
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Safety

HS Code 
2922290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
B711055
Product name
2-Bromo-6-methoxyaniline
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
B711055
Product name
2-Bromo-6-methoxyaniline
Packaging
100mg
Price
$60
Updated
2021/12/16
Oakwood
Product number
075303
Product name
2-Bromo-6-methoxyaniline
Purity
99%
Packaging
250mg
Price
$29
Updated
2021/12/16
Oakwood
Product number
075303
Product name
2-Bromo-6-methoxyaniline
Purity
99%
Packaging
1g
Price
$44
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-9-Y2
Product name
2-Bromo-6-methoxyaniline
Purity
97%
Packaging
1g
Price
$64
Updated
2021/12/16
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2-bromo-6-methoxy-aniline Chemical Properties,Usage,Production

Synthesis

90-04-0

5473-01-8

Step A: Synthesis of 6-bromo-2-anisidine. A solution of bromine (1.22 mL, 23.7 mmol) in acetic acid (10 mL) was slowly added dropwise to a cooled solution of o-methoxyaniline (2.7 mL, 23.7 mmol) in hexadecanecarboxylic acid (20 mL) for a controlled time period of 10 minutes at 10°C. The reaction mixture was then stirred for 10 minutes. After the dropwise addition was completed, the reaction mixture was continued to be stirred for 10 min. Upon completion of the reaction, the solvent was removed by rotary evaporation and the residue was dissolved in ethyl acetate. The solution was sequentially washed with saturated sodium bicarbonate solution and dried with anhydrous magnesium sulfate. After drying, the desiccant was removed by filtration and the filtrate was concentrated by rotary evaporation. The crude product was purified by fast column chromatography on silica gel, the eluent being a hexane solution of 45% dichloromethane, resulting in 3.44 g of 2-bromo-6-methoxyaniline in 72% yield.

References

[1] Patent: US6291511, 2001, B1

2-bromo-6-methoxy-aniline Preparation Products And Raw materials

Raw materials

Preparation Products

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5473-01-8, 2-bromo-6-methoxy-anilineRelated Search:

2,4-DIBROMO-6-(TRIFLUOROMETHOXY)ANILINE 6,7-Dibromo-8-nitro-2,3-dihydrobenzo[1,4]dioxine-5-carboxylic acid N-(3-AMINO-2,6-DIBROMO-4-METHOXYPHENYL)-2-FURAMIDE 2-(BENZYLOXY)-6-BROMO-4-NITROANILINE 2,4-DIBROMO-6-TRIFLUOROMETHOXYPHENYLISOTHIOCYANATE 3-(DIFLUOROMETHOXY)-2-NITRO-BROMOBENZENE 4-bromo-6-chlorobenzo[d]oxazol-2(3H)-one 2,4-DIBROMO-6-(DIFLUOROMETHOXY)ANILINE TERT-BUTYL (5-BROMO-1,3-BENZODIOXOL-4-YL)CARBAMATE 1-BROMO-3-METHOXY-2-NITROBENZENE 2-BROMO-6-METHOXY-4-NITROANILINE 3-(1,3-BENZOTHIAZOL-2-YL)-2,4-DIBROMO-6-METHOXYANILINE 2-bromo-6-methoxy-aniline 5-BROMO-1,3-BENZODIOXOL-4-AMINE

  • 2-Bromo-6-methoxyaniline97%
  • 2-Amino-3-bromoanisole
  • Nsc29554
  • 2-Bromo-6-methoxyaniline 97%
  • 2-Amino-3-bromoanisole, 6-Bromo-o-anisidine
  • BenzenaMine, 2-broMo-6-Methoxy-
  • 2-BroMo-6-Methoxy-phenylaMine
  • 5473-01-8
  • 5473/1/8