4-CHLORO-2,6-DIPHENYLPYRIMIDINE
- Product Name
- 4-CHLORO-2,6-DIPHENYLPYRIMIDINE
- CAS No.
- 29509-91-9
- Chemical Name
- 4-CHLORO-2,6-DIPHENYLPYRIMIDINE
- Synonyms
- Pyrimidine, 4-chloro-2,6-diphenyl-;4-CDPP;6-CHLORO-2,4-DIPHENYLPYRIMIDINE;4-CHLORO-2,6-DIPHENYLPYRIMIDINE;2,6-diphenylpyrimidine-4-chloride;4-CHLORO-2,6-DIPHENYLPYRIMIDINE ISO 9001:2015 REACH
- CBNumber
- CB4153250
- Molecular Formula
- C16H11ClN2
- Formula Weight
- 266.72
- MOL File
- 29509-91-9.mol
4-CHLORO-2,6-DIPHENYLPYRIMIDINE Property
- Melting point:
- 104-105℃
- Boiling point:
- 339.2±35.0 °C(Predicted)
- Density
- 1.221
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- -0.99±0.30(Predicted)
- color
- White to Almost white
Safety
- HS Code
- 2933.59.8000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- C3016
- Product name
- 4-Chloro-2,6-diphenylpyrimidine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $43
- Updated
- 2025/07/31
- Product number
- C3016
- Product name
- 4-Chloro-2,6-diphenylpyrimidine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $216
- Updated
- 2025/07/31
- Product number
- C370175
- Product name
- 4-Chloro-2,6-diphenylpyrimidine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 3008AB
- Product name
- 4-Chloro-2,6-diphenylpyrimidine
- Packaging
- 25g
- Price
- $290
- Updated
- 2021/12/16
- Product number
- 095796
- Product name
- 4-Chloro-2,6-diphenylpyrimidine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $341
- Updated
- 2021/12/16
4-CHLORO-2,6-DIPHENYLPYRIMIDINE Chemical Properties,Usage,Production
Chemical Properties
White solid
Synthesis Reference(s)
Journal of Medicinal Chemistry, 47, p. 6529, 2004 DOI: 10.1021/jm049448r
Synthesis
3764-01-0
24388-23-6
29509-91-9
Using 2,4,6-trichloropyrimidine (10 g, 54.5 mmol) and (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene (22.3 g, 109 mmol) as raw material, catalyzed by tetrakis(triphenylphosphine)palladium (3.8 g, 3.27 mmol) in a mixed solvent of THF (240 mL) and water (120 mL). Potassium carbonate (45.2 g) was added and the reaction was stirred at 90 °C. Upon completion of the reaction, extraction was carried out with dichloromethane and water. The organic layer was dried with anhydrous magnesium sulfate and concentrated. Purified by silica gel column chromatography and recrystallization, 9.5 g of 4-chloro-2,6-diphenylpyrimidine was obtained in 65% yield.
References
[1] Patent: KR2017/127593, 2017, A. Location in patent: Paragraph 0400-0402
[2] Patent: KR2017/120233, 2017, A. Location in patent: Paragraph 0511; 0512
[3] Patent: US2018/251473, 2018, A1. Location in patent: Paragraph 0253; 0254
[4] Patent: US2018/282276, 2018, A1. Location in patent: Paragraph 0222; 0223
4-CHLORO-2,6-DIPHENYLPYRIMIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-CHLORO-2,6-DIPHENYLPYRIMIDINE manufacturers
- Product
- 4-CHLORO-2,6-DIPHENYLPYRIMIDINE 29509-91-9
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 ton
- Release date
- 2024-11-13
- Product
- 4-CHLORO-2,6-DIPHENYLPYRIMIDINE 29509-91-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-27
- Product
- 4-chloro-2,6-diphenylpyrimidine 29509-91-9
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-18