methyl 3-(methylamino)propanoate

Product Name: methyl 3-(methylamino)propanoate
CAS No.: 24549-12-0
Chemical Name: methyl 3-(methylamino)propanoate
Synonyms: Methyl N-methyl-beta-alaninate;Imbandronate sodium impurity 22;methyl 3-(methylamino)propanoate;β-Alanine, N-methyl-, methyl ester
CBNumber: CB41546936
Molecular Formula: C5H11NO2
Formula Weight: 117.15
MOL File: 24549-12-0.mol

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methyl 3-(methylamino)propanoate Property

Boiling point:: 50 °C(Press: 11 Torr)
Density: 0.949±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Store in freezer, under -20°C
pka: 9.39±0.10(Predicted)
Appearance: Colorless to light yellow Liquid
InChI: InChI=1S/C5H11NO2/c1-6-4-3-5(7)8-2/h6H,3-4H2,1-2H3
InChIKey: NGNUXOCKVMKGQL-UHFFFAOYSA-N
SMILES: C(OC)(=O)CCNC

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Safety

HS Code: 2922498590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H226Flammable liquid and vapour

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: M219900
Product name: Methyl3-(Methylamino)propanoate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M219900
Product name: Methyl3-(Methylamino)propanoate
Packaging: 500mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 1857AB
Product name: Methyl3-(methylamino)propanoate
Packaging: 5g
Price: $269
Updated: 2021/12/16

AK Scientific

Product number: 1857AB
Product name: Methyl3-(methylamino)propanoate
Packaging: 1g
Price: $141
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0122389
Product name: METHYL 3-(METHYLAMINO)PROPANOATE
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

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methyl 3-(methylamino)propanoate Chemical Properties,Usage,Production

Synthesis

292638-85-8

74-89-5

24549-12-0

Example 38: General procedure for the synthesis of methyl 3-(methylamino)propionate: methyl acrylate (10 g, 116 mmol) was dissolved in methanol (20 mL) and the solution was cooled to -20 °C. Methylamine solution (2M, dissolved in tetrahydrofuran, 90mL, 180mmol) was added slowly through the addition funnel, keeping the reaction mixture stirred at -20°C for 2 hours. After completion of the reaction, the solvent was removed under vacuum. The residue was distilled under reduced pressure (45 °C, 5 Torr) to give methyl 3-(methylamino)propionate as a colorless liquid (3.5 g, 28% yield). The product was characterized by 1H NMR (CDCl3): δ 2.44 (s, 3H), 2.52 (t, 2H, J=6.31Hz), 2.86 (t, 2H, J=6.31Hz), 3.69 (s, 3H).

References

[1] Phosphorus, Sulfur and Silicon and Related Elements, 1998, vol. 134-135, p. 231 - 254
[2] Kinetics and Catalysis, 2010, vol. 51, # 5, p. 653 - 656
[3] Organic and Biomolecular Chemistry, 2013, vol. 11, # 12, p. 1929 - 1932
[4] Patent: WO2009/118292, 2009, A1. Location in patent: Page/Page column 74-75
[5] Monatshefte fuer Chemie, 1933, vol. 63, p. 224,230,234

methyl 3-(methylamino)propanoate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl 3-(methylamino)propanoate Suppliers

China 52 India 3 United States 6 Global 61

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Accela ChemBio Inc.

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View Lastest Price from methyl 3-(methylamino)propanoate manufacturers

Honest Joy Holdings Limited

Product: Methyl 3-(methylamino)propanoate 24549-12-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.2%
Supply Ability: 100 tons
Release date: 2022-01-26

Career Henan Chemical Co

Product: methyl 3-(methylamino)propanoate 24549-12-0
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 1kg；10kg; 25kg
Release date: 2020-01-07

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Imbandronate sodium impurity 22

24549-12-0