2-Pentylpyridine
- Product Name
- 2-Pentylpyridine
- CAS No.
- 2294-76-0
- Chemical Name
- 2-Pentylpyridine
- Synonyms
- FEMA 3383;2-amylpyridine;FEMA NUMBER 3383;2-pentyl-pyridin;2-PENTYLPYRIDINE;2-N-AMYLPYRIDINE;α-Pyridyl benzene;2-N-PENTYLPYRIDINE;2-Amylpyridine >Pyridine, 2-pentyl-
- CBNumber
- CB4156756
- Molecular Formula
- C10H15N
- Formula Weight
- 149.23
- MOL File
- 2294-76-0.mol
2-Pentylpyridine Property
- Boiling point:
- 102-107 °C (lit.)
- Density
- 0.897 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.488(lit.)
- FEMA
- 3383 | 2-PENTYLPYRIDINE
- Flash point:
- 175 °F
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- clear liquid
- pka
- 6.01±0.10(Predicted)
- Specific Gravity
- 0.902
- color
- Colorless to Light yellow
- Odor
- at 0.10 % in propylene glycol. fatty tallow green pepper mushroom herbal
- Odor Type
- fatty
- biological source
- synthetic
- JECFA Number
- 1313
- BRN
- 2772
- LogP
- 3.31
- CAS DataBase Reference
- 2294-76-0(CAS DataBase Reference)
- NIST Chemistry Reference
- Pyridine, 2-pentyl-(2294-76-0)
- EPA Substance Registry System
- 2-Pentylpyridine (2294-76-0)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H227Combustible liquid
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- A2278
- Product name
- 2-Amylpyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $47
- Updated
- 2025/07/31
- Product number
- P284960
- Product name
- 2-Pentylpyridine
- Packaging
- 2.5g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- P284960
- Product name
- 2-Pentylpyridine
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- JK173112
- Product name
- 2-Pentylpyridine
- Purity
- 98%
- Packaging
- 5g
- Price
- $73
- Updated
- 2021/12/16
- Product number
- S154
- Product name
- 2-n-Pentylpyridine
- Packaging
- 1g
- Price
- $74
- Updated
- 2021/12/16
2-Pentylpyridine Chemical Properties,Usage,Production
Chemical Properties
2-Pentylpyridine has a tallowy-like odor.
Occurrence
Reported as occurring in shallow-fried beef and as a steam-volatile component in roasted Spanish peanut. Also reported found in bell pepper, black sesame seeds, roast turkey, fried chicken, fried beef, cooked beef, mutton, lamb fat, roasted filberts, toasted oats and coriander seed.
Uses
flavors and fragrances
Definition
ChEBI: 2-Pentylpyridine is a member of pyridines.
Preparation
By alkylation of 2-pycollyl lithium; by hydrogenation of 2-pentenyl pyridine.
Aroma threshold values
Detection: 0.6 ppb. Aroma characteristics at 0.1%: strong fresh green vegetative, peppery, mushroom, herbal and oily.
Taste threshold values
Taste characteristics at 1 ppm: green pepper vegetative, mushroom-like, musty, oily, meaty and MSG-like.
Synthesis
109-09-1
6393-56-2
2294-76-0
GENERAL STEPS: A THF solution (3 mL) of MnCl2-(THF)1.6 (3 mol%, 3 mg, 0.012 mmol) was added to a 20 mL scintillation vial in an inert atmosphere glove box. Subsequently, 2-chloropyridine (0.41 mmol, 1 eq.) was added as an electrophilic reagent, as well as the internal standard homotrimethylbenzene (0.41 mmol, 1 eq.). After stirring for 5 minutes at room temperature, 1-pentylmagnesium chloride Grignard reagent solution (1.2-2.6 eq.) was slowly added dropwise and the reaction continued to be stirred at room temperature. Upon completion of the reaction, the mixture was removed from the glove box and the reaction was quenched with saturated K2CO3 solution (3 mL) and EtOAc (3 mL). The organic layer was separated and the aqueous phase was further extracted with EtOAc (3 x 3 mL). The combined organic phases were dried with MgSO4, filtered and concentrated. The crude product was purified by silica gel column chromatography to afford the target product 2-pentylpyridine.
Purification Methods
Dry it with NaOH for several days, then distil it from CaO under reduced pressure, taking the middle fraction and redistilling it. The picrate has m 72-72.8o (from EtOH). [Beilstein 20 III/IV 2835.] 3-n-Pentylpyridine, purified as the 2-isomer, has b 110-112o/20mm, 224-226o/748mm, and the picrate has m 79.5-80o(from EtOH). [Beilstein 20 III/IV 2835.]
References
[1] Synlett, 2018, vol. 29, # 13, p. 1700 - 1706
2-Pentylpyridine Preparation Products And Raw materials
Raw materials
Preparation Products
2-Pentylpyridine Suppliers
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View Lastest Price from 2-Pentylpyridine manufacturers
- Product
- 2-Pentylpyridine 2294-76-0
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-07-12
- Product
- 2-Pentylpyridine 2294-76-0
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10ton
- Release date
- 2024-07-22
- Product
- 2-Pentylpyridine 2294-76-0
- Price
- US $0.00-0.00/Kg
- Min. Order
- 100G
- Purity
- 99.0%+
- Supply Ability
- 100 tons
- Release date
- 2020-01-17