3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL

Product Name: 3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL
CAS No.: 726185-54-2
Chemical Name: 3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL
Synonyms: Methyl 3-(4-Piperidyl)benzoate Hydrochloride;3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL;METHYL 3-(PIPERIDIN-4-YL)BENZOATE HYDROCHLORIDE;4-(3-METHOXYCARBONYLPHENYL) PIPERIDINE HYDROCHLORIDE;Benzoic acid, 3-(4-piperidinyl)-, methyl ester, hydrochloride
CBNumber: CB4180203
Molecular Formula: C13H18ClNO2
Formula Weight: 255.74
MOL File: Mol file

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3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

ChemScene

Product number: CS-M3503
Product name: Benzoicacid,3-(4-piperidinyl)-,methylester,hydrochloride
Packaging: 100mg
Price: $117
Updated: 2021/12/16

ChemScene

Product number: CS-M3503
Product name: Benzoicacid,3-(4-piperidinyl)-,methylester,hydrochloride
Packaging: 250mg
Price: $185
Updated: 2021/12/16

AK Scientific

Product number: 6998AJ
Product name: Methyl3-(piperidin-4-yl)benzoatehydrochloride
Packaging: 250mg
Price: $266
Updated: 2021/12/16

ChemScene

Product number: CS-M3503
Product name: Benzoicacid,3-(4-piperidinyl)-,methylester,hydrochloride
Packaging: 1g
Price: $466
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0117810
Product name: 3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HYDROCHLORIDE
Purity: 95.00%
Packaging: 5MG
Price: $497
Updated: 2021/12/16

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3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL Chemical Properties,Usage,Production

Synthesis

67-56-1

726185-55-3

726185-54-2

General procedure for the synthesis of methyl 3-(piperidin-4-yl)benzoate hydrochloride from methanol and the compound (CAS: 726185-55-3): 500 mg (2.069 mmol) of 3-(4-piperidinyl)benzoate hydrochloride was mixed with 10 mL of saturated HCl methanol solution and the reaction was stirred at room temperature overnight. After completion of the reaction, the reaction mixture was concentrated by distillation under reduced pressure. The concentrated residue was mixed with 3 mL of isopropanol and stirred, followed by filtration. The filter cake was washed with ether and dried at 60 °C in a recirculating air dryer. A final 390 mg (74% yield) of colorless crystalline product was obtained, and thin layer chromatography (TLC) showed an Rf value of 0.34 (unfolding agent: EI D). Infrared spectra (IR, KBr press method) of the product showed a characteristic absorption peak of carbonyl (C=O) at 1728 cm-1 . Electrospray ionization mass spectrometry (ESI-MS) analysis showed a molecular ion peak (M+H)+ of 220, as well as peaks of (M+Cl+HCl) of 290/292/294 (corresponding to Cl2 isotope pattern).

References

[1] Patent: US2004/192729, 2004, A1. Location in patent: Page 32

3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCL Suppliers

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726185-54-2, 3-PIPERIDIN-4-YL-BENZOIC ACID METHYL ESTER HCLRelated Search:

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METHYL 3-(PIPERIDIN-4-YL)BENZOATE HYDROCHLORIDE

Benzoic acid, 3-(4-piperidinyl)-, methyl ester, hydrochloride

Methyl 3-(4-Piperidyl)benzoate Hydrochloride

726185-54-2

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