3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE
- Product Name
- 3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE
- CAS No.
- 51642-03-6
- Chemical Name
- 3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE
- Synonyms
- Tetrahydro-3-thiophenaMine 1;3-Aminosulfolane hydrochloride;3-AMINOTHIOLANE-1,1-DIONE, HYDROCHLORIDE;1,1-Dioxidotetrahydrothien-3-ylaMine, HCl;Tetrahydro-3-thiophenaMine 1,1-dioxide HCl;3-AMINOTETRAHYDROTHIOPHENE 1,1-DIOXIDE HCL;3-amino-1λ-thiolane-1,1-dione hydrochloride;TETRAHYDROTHIOPHEN-3-AMINIUM 1,1-DIOXIDE CHLORIDE;1,1-DIOXIDOTETRAHYDROTHIEN-3-YLAMINE HYDROCHLORIDE;3-Aminotetrahydrothiopene 1,1-dioxide hydrochloride
- CBNumber
- CB4193151
- Molecular Formula
- C4H10ClNO2S
- Formula Weight
- 171.65
- MOL File
- 51642-03-6.mol
3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE Property
- Melting point:
- 208 °C
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- D462590
- Product name
- 1,1-Dioxidotetrahydrothien-3-ylaminehydrochloride
- Packaging
- 250mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 8H70-5-X9
- Product name
- 3-Aminotetrahydrothiophene 1,1-dioxide hydrochloride
- Packaging
- 250mg
- Price
- $84
- Updated
- 2021/12/16
- Product number
- FD115428
- Product name
- 1,1-Dioxidotetrahydrothien-3-ylamine hydrochloride
- Packaging
- 250mg
- Price
- $115
- Updated
- 2021/12/16
- Product number
- W6650
- Product name
- 3-Aminotetrahydrothiophene1,1-dioxidehydrochloride
- Packaging
- 500mg
- Price
- $120
- Updated
- 2021/12/16
- Product number
- FD115428
- Product name
- 1,1-Dioxidotetrahydrothien-3-ylamine hydrochloride
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE Chemical Properties,Usage,Production
Uses
1,1-Dioxidotetrahydrothien-3-ylamine, HCl
Synthesis
77-79-2
51642-03-6
1. Preparation of 1,1-dioxo-tetrahydro-thiophen-3-ylamine hydrochloride: 3-cyclobutylsulfone (compound 10a, 0.5 g, 4.2 mmol) was dissolved in 10 mL of 26% ammonia (NH4OH) in a sealed reaction tube and heated to react for 4 hours at 80°C. The reaction was carried out under reduced pressure. After completion of the reaction, the mixture was concentrated under reduced pressure to give a yellow oil. The oily material was dissolved in 3 mL of ethanol (EtOH) and acidified by slowly adding 1 mL of concentrated hydrochloric acid (HCl). The acidified mixture was stirred for 0.5 h. Subsequently, ether was added to promote crystallization of the hydrochloride. The solid product was collected by filtration, washed with ether and finally dried under vacuum to afford 1,1-dioxo-tetrahydro-thiophen-3-ylamine hydrochloride (Compound 10b, 0.533 g, 74% yield).
References
[1] Patent: WO2008/33562, 2008, A2. Location in patent: Page/Page column 42
[2] Patent: US2009/76005, 2009, A1. Location in patent: Page/Page column 17
3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE Suppliers
- Tel
- --
- Fax
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- Country
- Belgium
- ProdList
- 6293
- Advantage
- 73
View Lastest Price from 3-AMINOTETRAHYDRO-1H-1LAMBDA6-THIOPHENE-1,1-DIONE HYDROCHLORIDE manufacturers
- Product
- 3-Aminotetrahydrothiophene 1,1-dioxide hydrochloride 51642-03-6
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- Min98%HPLC
- Supply Ability
- g/kg/ton
- Release date
- 2020-01-09