ChemicalBook > CAS DataBase List > 7-chlorothiazolo[5,4-d]pyrimidine

7-chlorothiazolo[5,4-d]pyrimidine

Product Name
7-chlorothiazolo[5,4-d]pyrimidine
CAS No.
13316-12-6
Chemical Name
7-chlorothiazolo[5,4-d]pyrimidine
Synonyms
SKL426;7-chlorothiazolo[5,4-d]pyrimidine;Thiazolo[5,4-d]pyriMidine, 7-chloro-;7-chloro-[1,3]thiazolo[5,4-d]pyrimidine
CBNumber
CB42123963
Molecular Formula
C5H2ClN3S
Formula Weight
171.61
MOL File
13316-12-6.mol
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7-chlorothiazolo[5,4-d]pyrimidine Property

Melting point:
152-154℃
Boiling point:
295℃
Density 
1.639
Flash point:
132℃
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
solid
Appearance
Light yellow to brown Solid
InChI
InChI=1S/C5H2ClN3S/c6-4-3-5(8-1-7-4)10-2-9-3/h1-2H
InChIKey
HGYFXAHDBRHZGF-UHFFFAOYSA-N
SMILES
C1=NC(Cl)=C2N=CSC2=N1
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Safety

HS Code 
2934999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
C380633
Product name
7-Chlorothiazolo[5,4-d]pyrimidine
Packaging
100mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC140240
Product name
7-Chlorothiazolo[5,4-d]pyrimidine
Packaging
500mg
Price
$95
Updated
2021/12/16
Apolloscientific
Product number
OR903749
Product name
7-Chlorothiazolo[5,4-d]pyrimidine
Purity
95%
Packaging
250mg
Price
$153
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC140240
Product name
7-Chlorothiazolo[5,4-d]pyrimidine
Packaging
1g
Price
$164
Updated
2021/12/16
Matrix Scientific
Product number
090179
Product name
7-Chlorothiazolo[5,4-d]pyrimidine
Purity
95+%
Packaging
250mg
Price
$168
Updated
2021/12/16
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7-chlorothiazolo[5,4-d]pyrimidine Chemical Properties,Usage,Production

Synthesis

122-51-0

54851-35-3

13316-12-6

General procedure for the synthesis of 7-chlorothiazolo[5,4-d]pyrimidine from triethyl orthoformate and 5-amino-6-chloropyrimidine-4-thiol: 5-amino-6-chloropyrimidine-4-thiol (4 g, 24.75 mmol) was dissolved in triethyl orthoformate and heated and refluxed for 1 hour. Upon completion of the reaction, the reaction mixture was concentrated to 60% of the original volume and subsequently cooled in a refrigerator. The precipitated solid was collected by filtration and dried under vacuum to afford 7-chlorothiazolo[5,4-d]pyrimidine (2.8 g, 66.04% yield) as a brown solid.1H NMR (300 MHz, CDCl3): δ 9.22 (s, 1H), 8.97 (s, 1H).

References

[1] Patent: WO2010/14930, 2010, A2. Location in patent: Page/Page column 50
[2] Patent: WO2008/57402, 2008, A2. Location in patent: Page/Page column 61-62
[3] Chemical and pharmaceutical bulletin, 1968, vol. 16, # 4, p. 750 - 755
[4] Patent: US2012/122838, 2012, A1. Location in patent: Page/Page column 81
[5] Patent: WO2013/12918, 2013, A1. Location in patent: Paragraph 00533

7-chlorothiazolo[5,4-d]pyrimidine Preparation Products And Raw materials

Raw materials

Preparation Products

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7-chlorothiazolo[5,4-d]pyrimidine Suppliers

Shanghai Ruipu Medical Technology Co., Ltd
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15895968936
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qq 1018762393
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China
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PharmaBlock Sciences (Nanjing),Inc.
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ChangZhou SIDU chemical Co., Ltd.
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Nanjing Norris-Pharm Technology Co., Ltd
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China
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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
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025-66113011 17798518460
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View Lastest Price from 7-chlorothiazolo[5,4-d]pyrimidine manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
7-Chlorothiazolo[5,4-d]pyriMidine 13316-12-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2020-05-15