ChemicalBook > CAS DataBase List > 5-BROMO-3-CHLORO-2-FORMYLPYRIDINE

5-BROMO-3-CHLORO-2-FORMYLPYRIDINE

Product Name
5-BROMO-3-CHLORO-2-FORMYLPYRIDINE
CAS No.
885168-04-7
Chemical Name
5-BROMO-3-CHLORO-2-FORMYLPYRIDINE
Synonyms
KML-125;5-Bromo-3-chloropicolinaldehyde;5-BROMO-3-CHLORO-2-FORMYLPYRIDINE;5-bromo-3-chloropyridine-2-carbaldehyde;2-Pyridinecarboxaldehyde, 5-bromo-3-chloro-
CBNumber
CB4225173
Molecular Formula
C6H3BrClNO
Formula Weight
220.45
MOL File
Mol file
More
Less

5-BROMO-3-CHLORO-2-FORMYLPYRIDINE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
Light yellow to green yellow Solid
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TRC
Product number
B993980
Product name
5-Bromo-3-chloropicolinaldehyde
Packaging
100mg
Price
$110
Updated
2021/12/16
AK Scientific
Product number
8866BB
Product name
5-Bromo-3-chloropicolinaldehyde
Packaging
100mg
Price
$342
Updated
2021/12/16
AK Scientific
Product number
8866BB
Product name
5-Bromo-3-chloropicolinaldehyde
Packaging
250mg
Price
$372
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0355437
Product name
5-BROMO-3-CHLORO-2-FORMYLPYRIDINE
Purity
95.00%
Packaging
5MG
Price
$498.47
Updated
2021/12/16
Ambeed
Product number
A193811
Product name
5-Bromo-3-chloropicolinaldehyde
Purity
95%
Packaging
100mg
Price
$64
Updated
2021/12/16
More
Less

5-BROMO-3-CHLORO-2-FORMYLPYRIDINE Chemical Properties,Usage,Production

Synthesis

1383001-27-1

885168-04-7

To a solution of 5-bromo-3-chloro-N-methoxy-N-methylpyridinamide (9.0 g, 32.3 mmol, 1.0 equiv) in tetrahydrofuran (THF, 100 mL) was slowly added lithium aluminum hydride (LAH, 1 M in THF, 16.12 mL, 16.1 mmol, 0.5 equiv) at -70 °C. The reaction was continued at this temperature for 2 hours. Upon completion of the reaction (monitored by thin layer chromatography TLC), the reaction mixture was quenched with saturated sodium bicarbonate (NaHCO3) solution. Subsequently, it was extracted with ethyl acetate (EtOAc, 3 x 250 mL), the organic layers were combined and washed sequentially with distilled water (500 mL) and saturated saline (500 mL). The organic layer was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by rapid column chromatography (CC) to afford 5-bromo-3-chloropyridin-2-aldehyde (5.0 g, 71% yield) as a brown gel.

References

[1] Patent: WO2015/158427, 2015, A1. Location in patent: Page/Page column 68
[2] Patent: WO2012/81736, 2012, A1. Location in patent: Page/Page column 102-103

5-BROMO-3-CHLORO-2-FORMYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

5-BROMO-3-CHLORO-2-FORMYLPYRIDINE Suppliers

China 45 India 1 United States 3 Global 49
Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
16077
Advantage
64
Cochemical Ltd.
Tel
029-86115547 17791676824
Fax
02151602123
Email
sales@cochemical.com
Country
China
ProdList
3014
Advantage
58
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Hangzhou Milestone Pharmtech Co., Ltd.
Tel
0571-82896630 18969958410
Email
sales_hz@milestonepharmtech.com
Country
China
ProdList
4895
Advantage
55
Yancheng KangdiSen Pharmaceutical Co., Ltd.
Tel
13812573443
Fax
-
Email
tongbenwan22@163.com
Country
China
ProdList
1980
Advantage
55
Suzhou JingTong Pharmaceutical Co., Ltd.
Tel
13675155016
Fax
18912765016
Email
tongtf110@sina.com
Country
China
ProdList
963
Advantage
55
Heze Development Zone chuangli Chemical Co., Ltd.
Tel
0530-+86-530-529 6766，+86-15666160102 15666160102
Fax
0530-529 6766
Email
info@chuangli-chem.com
Country
China
ProdList
836
Advantage
55
Suzhou Nuoouman Biological Technology Co., Ltd.
Tel
15026866316
Email
180642609@qq.com
Country
China
ProdList
4967
Advantage
58
Zhijiang City Zhou Yuan Yao Biological Technology Co., LTD
Tel
15671050515
Fax
-
Email
2267948566@qq.com
Country
China
ProdList
480
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
Email
3007523370@qq.com
Country
China
ProdList
52687
Advantage
58
Jiangsu aikang biomedical research and development co., LTD
Tel
025-58859352 13155353615
Email
qzhang@aikonchem.com
Country
China
ProdList
15525
Advantage
58
Career Henan Chemica Co
Tel
+86-0371-86658258 +8613203830695
Fax
0371-86658258
Email
laboratory@coreychem.com
Country
China
ProdList
30229
Advantage
58
Henan Weituxi Chemical Technology Co., Ltd.
Tel
0371-63284658 18135795563
Fax
QQ:2885349392
Email
2885349392@qq.com
Country
China
ProdList
9989
Advantage
58
Wuxi Donghe Pharmaceutical Technology Co., Ltd.
Tel
63313187 15358055255
Fax
QQ：63313187
Email
63313187@qq.com
Country
China
ProdList
1984
Advantage
58
Birdo (Shanghai) Medical Technology Co., Ltd.
Tel
021-58099077-8041 18601625411
Email
sales@birdotech.com
Country
China
ProdList
9764
Advantage
58
Taizhou Nanfeng Pharmaceutical Research Institute
Tel
nanfengdrug@163.com; 18616377689
Email
nanfengdrug@163.com
Country
China
ProdList
20009
Advantage
58
Energy Chemical
Tel
021-58432009 400-005-6266
Fax
021-58436166
Email
marketing@energy-chemical.com
Country
China
ProdList
44918
Advantage
58
Lingyuan Bebiansen Biological Technology Co., Ltd
Tel
18642120371
Email
2837458851@qq.com
Country
China
ProdList
7963
Advantage
58
Hubei Co-prosperity Medicine Technonlogy Co., Ltd
Tel
2383948258 19172820304
Email
2383948258@qq.com
Country
China
ProdList
12987
Advantage
58
Beijing Jin Ming Biotechnology Co., Ltd.
Tel
010-60605840 15801484223;
Email
psaitong@jm-bio.com
Country
China
ProdList
29757
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Shaanxi Yudingzhuo Medical Technology Co., Ltd.
Tel
18992018580 18165105898
Fax
QQ:1617857088
Email
13608210612@163.com
Country
China
ProdList
2984
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39653
Advantage
58
Qingzhou dafeng import and export Co. LTD
Tel
16773308882
Email
927608786@qq.com
Country
China
ProdList
3051
Advantage
58
BEIJING QIONGFENG TECHNOLOGICAL CO., LTD.
Tel
13552142508
Email
766912840@qq.com
Country
China
ProdList
188
Advantage
58
Shandong Mingde Biotechnology Co., Ltd
Tel
15553348166
Email
m15553348166@163.com
Country
China
ProdList
9967
Advantage
58
Shaanxi PharmaGHS Science Co., LTD
Tel
13279368192
Email
pharmaghs@126.com
Country
China
ProdList
2935
Advantage
58
Anhui Henuo Biotechnology Co., Ltd
Tel
18455579438
Country
China
ProdList
16684
Advantage
58
Beijing Solarbio Science & Tecnology Co., Ltd.
Tel
010-50973130 17801761073
Email
Gsiyu@solarbio.com
Country
China
ProdList
50464
Advantage
58
Zhuhai Aobokai Biomedical Technology Co., Ltd.
Tel
400-0628126 15697565236;
Email
sales-team@aobchem.com.cn
Country
China
ProdList
50000
Advantage
58
Shanghai Huasige Pharmaceutical Technology Co., LTD
Tel
13611612777
Email
3627377363@qq.com
Country
China
ProdList
4015
Advantage
58
Shanghai Jieshikai Biotechnology Co. , Ltd.
Tel
021-57520305 13795461237
Email
zhuruyan@jskchem.com
Country
China
ProdList
49234
Advantage
58
Lianhe Aigen Pharmatech Co.,Ltd.
Tel
18918657159
Email
sales-Aigen@lianhetech.com
Country
China
ProdList
3000
Advantage
58
Wuhan Acumen Bio-Technology Co.,ltd
Tel
027-027-16602739303 16602739303
Email
673003916@qq.com
Country
China
ProdList
2935
Advantage
58
Hefei Mokai Pharmaceutical Technology Co., Ltd
Tel
19355912709
Email
690231469@qq.com
Country
China
ProdList
7593
Advantage
58
Shanghai Aladdin Biochemical Technology Co.,Ltd.
Tel
400-6206333 13167063860
Email
anhua.mao@aladdin-e.com
Country
China
ProdList
48457
Advantage
58
Shaanxi Xihua Chemical Industry Co., Ltd
Tel
029-81136151 17392212881
Email
1095@dideu.com
Country
China
ProdList
9984
Advantage
58
Biosynth Biological Technology (Suzhou) Co Ltd
Tel
51288865780
Email
sales@biosynth.com
Country
China
ProdList
6051
Advantage
58
Ningbo Chaoming Biotechnology Co., Ltd
Tel
13301662590
Email
mandy@atkchemical.com
Country
China
ProdList
9343
Advantage
58
ATK CHEMICAL COMPANY LIMITED
Tel
+undefined-21-51877795
Fax
+86 21 5161 9052/ 5187 7796
Email
ivan@atkchemical.com
Country
China
ProdList
33024
Advantage
60
Qingdao Dexin Chemical Co., Ltd
Tel
+86-15553333686
Email
15553333686@qq.com
Country
China
ProdList
3113
Advantage
58
Cochemical Co. Ltd.
Tel
+86-029-86115547 +86-17791676824
Email
sales@cochemical.com
Country
China
ProdList
3952
Advantage
58
Guangzhou Weike Biotechnology Co., Ltd.
Tel
15902098758
Country
CHINA
ProdList
133
Advantage
58
VESINO INDUSTRIAL CO., LTD.
Tel
--
Fax
--
Email
info@vesino.com.cn
Country
China
ProdList
617
Advantage
38
Suzhou Rovathin Foreign Trade Co.,Ltd
Tel
--
Fax
--
Email
sales@rovathin.com
Country
China
ProdList
4395
Advantage
58

885168-04-7, 5-BROMO-3-CHLORO-2-FORMYLPYRIDINERelated Search:


  • 5-bromo-3-chloropyridine-2-carbaldehyde
  • 5-BROMO-3-CHLORO-2-FORMYLPYRIDINE
  • 5-Bromo-3-chloropicolinaldehyde
  • 2-Pyridinecarboxaldehyde, 5-bromo-3-chloro-
  • KML-125
  • 885168-04-7
  • Heterocyclic Compounds