1-Acetyl-6-nitroindoline
- Product Name
- 1-Acetyl-6-nitroindoline
- CAS No.
- 22949-08-2
- Chemical Name
- 1-Acetyl-6-nitroindoline
- Synonyms
- 1-Acetyl-6-Nitroindole;1-(6-Nitroindolin-1-yl);1-Acetyl-6-nitroindoline;1-Acetyl-6-nitro-1h-indole;Indoline, 1-acetyl-6-nitro-;1-(6-Nitroindolin-1-yl)ethanone;1-(6-nitro-1-indolinyl)ethanone;1-Acetyl-2,3-dihydro-6-nitro-1H-indole;1H-Indole, 1-acetyl-2,3-dihydro-6-nitro-;1-(6-nitro-2,3-dihydro-1H-indol-1-yl)ethan-1-one
- CBNumber
- CB42275037
- Molecular Formula
- C10H10N2O3
- Formula Weight
- 206.2
- MOL File
- 22949-08-2.mol
1-Acetyl-6-nitroindoline Property
- storage temp.
- Sealed in dry,Room Temperature
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- S445606
- Product name
- 1-ACETYL-6-NITROINDOLINE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $113
- Updated
- 2025/07/31
- Product number
- S445606
- Product name
- 1-ACETYL-6-NITROINDOLINE
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $110
- Updated
- 2024/03/01
- Product number
- N498198
- Product name
- 1-(6-Nitroindolin-1-yl)ethanone
- Packaging
- 1g
- Price
- $175
- Updated
- 2021/12/16
- Product number
- N498198
- Product name
- 1-(6-Nitroindolin-1-yl)ethanone
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- N498198
- Product name
- 1-(6-Nitroindolin-1-yl)ethanone
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
1-Acetyl-6-nitroindoline Chemical Properties,Usage,Production
Synthesis
19727-83-4
22949-08-2
Step A: 6-Nitrodihydroindole (3.0 g, 18.3 mmol) was dissolved in tetrahydrofuran (THF, 45 mL) and triethylamine (Et3N, 3.4 mL, 24.4 mmol) at 0 °C. Acetyl chloride (1.5 mL, 21 mmol) was added dropwise. The reaction mixture was stirred at room temperature for 30 minutes. After completion of the reaction, the mixture was partitioned between ethyl acetate (EtOAc) and aqueous hydrochloric acid (HCl aq.). The organic layer was separated, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 1-acetyl-6-nitrodihydroindole (3.8 g, 100% yield) as a yellow solid.
References
[1] Patent: WO2006/19831, 2006, A1. Location in patent: Page/Page column 447
[2] Zhurnal Obshchei Khimii, 1959, vol. 29, p. 2541,2550; engl. Ausg. S. 2504, 2511
[3] Heterocycles, 1998, vol. 48, # 12, p. 2481 - 2484
1-Acetyl-6-nitroindoline Preparation Products And Raw materials
Raw materials
Preparation Products
1-Acetyl-6-nitroindoline Suppliers
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View Lastest Price from 1-Acetyl-6-nitroindoline manufacturers
- Product
- 1-Acetyl-2,3-dihydro-6-nitro-1H-indole 22949-08-2
- Price
- US $5.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12