3-IODO-TETRAHYDRO-FURAN

Physical Form

Product Name: 3-IODO-TETRAHYDRO-FURAN
CAS No.: 121138-01-0
Chemical Name: 3-IODO-TETRAHYDRO-FURAN
Synonyms: 3-iodooxolane;3-IODO-TETRAHYDRO-FURAN;Furan, tetrahydro-3-iodo-;(RS)-3-iodotetrahydrofuran;Benzoicacid,8-hydroxy-,pentylester
CBNumber: CB42451930
Molecular Formula: C4H7IO
Formula Weight: 198
MOL File: 121138-01-0.mol

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3-IODO-TETRAHYDRO-FURAN Property

Boiling point:: 187.0±33.0 °C(Predicted)
Density: 1.93±0.1 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: liquid
color: Dark brown
InChI: InChI=1S/C4H7IO/c5-4-1-2-6-3-4/h4H,1-3H2
InChIKey: BKIQORJIKOPRCG-UHFFFAOYSA-N
SMILES: O1CCC(I)C1

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Safety

HS Code: 2932190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I737015
Product name: 3-Iodotetrahydrofuran
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Apolloscientific

Product number: OR52585
Product name: 3-Iodotetrahydrofuran
Packaging: 1g
Price: $176
Updated: 2021/12/16

Matrix Scientific

Product number: 068669
Product name: 3-Iodotetrahydrofuran
Purity: >95%
Packaging: 1g
Price: $123
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2H10-H-02
Product name: 3-Iodooxolane
Packaging: 1g
Price: $150
Updated: 2021/12/16

Matrix Scientific

Product number: 068669
Product name: 3-Iodotetrahydrofuran
Purity: >95%
Packaging: 5g
Price: $430
Updated: 2021/12/16

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3-IODO-TETRAHYDRO-FURAN Chemical Properties,Usage,Production

Physical Form

liquid

Uses

3-Iodotetrahydrofuran is used to study transition-metal-free Heck-type reaction between alkenes and alkyl iodides enabled by light in water.

Synthesis

453-20-3

121138-01-0

3-Hydroxytetrahydrofuran (8.8 g, 0.1 mol) was used as starting material and dissolved in dichloromethane (200 mL). Triphenylphosphine (52.4 g, 0.2 mol), imidazole (13.6 g, 0.2 mol) and iodine (50.7 g, 0.2 mol) were added sequentially to this solution. The reaction mixture was heated to reflux overnight under nitrogen protection. Upon completion of the reaction, 0.2 M sodium thiosulfate solution (30 mL) was added to quench the reaction. The organic layer was separated and the aqueous phase was extracted with dichloromethane. The organic phases were combined, dried over anhydrous magnesium sulfate, filtered and concentrated to give a wet yellow solid. The solid was dissolved in pentane (100 mL) and stirred for 2 h. The insoluble material was removed by filtration and the filtrate was concentrated to give the final 3-iodotetrahydrofuran (18.6 g, 94% yield).

References

[1] Patent: CN103965174, 2016, B. Location in patent: Paragraph 0171; 0173-0175
[2] Organic and Biomolecular Chemistry, 2015, vol. 13, # 22, p. 6170 - 6174
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 3, p. 933 - 937
[4] Angew. Chem., 2012, vol. 125, # 3, p. 967 - 971,5

3-IODO-TETRAHYDRO-FURAN Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODO-TETRAHYDRO-FURAN Suppliers

China 89 Germany 1 India 2 United Kingdom 1 United States 9 Global 102

Shanghai Sunmonth Technology Co., LTD

Tel: 15216675652
Email: xuanyuelj@163.com
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J & K SCIENTIFIC LTD.

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Tel: 18270980682
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Email: mlcheng@sunwaypharm.cn
Country: China
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Advantage: 57

Thermo Fisher Scientific

Tel: 800-810-5118
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Country: China
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Advantage: 75

NovoChemy Ltd.

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Country: Germany
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Shanghai Sheepchem Co., Ltd.

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Fax: +86 (21) 6715-7651
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View Lastest Price from 3-IODO-TETRAHYDRO-FURAN manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD

Product: 3-Iodotetrahydrofuran 121138-01-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 95%min
Supply Ability: 30tons/month
Release date: 2023-02-22

Career Henan Chemical Co

Product: 3-IODO-TETRAHYDRO-FURAN 121138-01-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 500kg
Release date: 2018-08-16

121138-01-0, 3-IODO-TETRAHYDRO-FURANRelated Search:

TETRAHYDROFURAN-3-CARBOXALDEHYDE 98 2'-IODO-ADENOSINE-5'-DIPHOSPHATE, SODIUM SALT 3-IODO-TETRAHYDRO-FURAN 2'-IODO-ADENOSINE-5'-[(BETA,GAMMA)-IMIDO]TRIPHOSPHATE, SODIUM SALT 3'-DEOXY-3'-IODOTHYMIDINE 2'-IODO-ADENOSINE-5'-TRIPHOSPHATE, SODIUM SALT 4,5-DIHYDRO-4-IODO-1'-METHYL-SPIRO[FURAN-2(3H),3'-[3H]INDOL]-2'(1'H)-ONE METHYL 3-DEOXY-3-IODO-5-O-BENZOYL-D-XYLOFURANOSE SPECS AK-823/41252400

3-IODO-TETRAHYDRO-FURAN

3-iodooxolane

Furan, tetrahydro-3-iodo-

(RS)-3-iodotetrahydrofuran

Benzoicacid,8-hydroxy-,pentylester

121138-01-0