2-BROMO-6-IODO-3-METHOXYPYRIDINE

Product Name: 2-BROMO-6-IODO-3-METHOXYPYRIDINE
CAS No.: 321535-37-9
Chemical Name: 2-BROMO-6-IODO-3-METHOXYPYRIDINE
Synonyms: 2-Bromo-3-methoxy-6-iodopyridine;2-BROMO-6-IODO-3-METHOXYPYRIDINE;Pyridine, 2-bromo-6-iodo-3-methoxy-
CBNumber: CB42452669
Molecular Formula: C6H5BrINO
Formula Weight: 313.92
MOL File: 321535-37-9.mol

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2-BROMO-6-IODO-3-METHOXYPYRIDINE Property

Boiling point:: 315.7±42.0 °C(Predicted)
Density: 2.166±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -6.51±0.10(Predicted)
form: solid
Appearance: White to yellow Solid
InChI: InChI=1S/C6H5BrINO/c1-10-4-2-3-5(8)9-6(4)7/h2-3H,1H3
InChIKey: LHDNVVCKJSWJKM-UHFFFAOYSA-N
SMILES: C1(Br)=NC(I)=CC=C1OC

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Safety

Hazard Codes: Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ADE000467
Product name: 2-Bromo-6-iodo-3-methoxypyridine
Purity: Aldrich
Packaging: 1g
Price: $817
Updated: 2025/07/31

TRC

Product number: B693553
Product name: 2-Bromo-6-iodo-3-methoxypyridine
Packaging: 250mg
Price: $55
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H07-S-X1
Product name: 2-Bromo-6-iodo-3-methoxypyridine
Packaging: 1g
Price: $192
Updated: 2021/12/16

AK Scientific

Product number: 0163AE
Product name: 2-Bromo-6-iodo-3-methoxypyridine
Packaging: 5g
Price: $250
Updated: 2021/12/16

Matrix Scientific

Product number: 035171
Product name: 2-Bromo-6-iodo-3-methoxypyridine
Packaging: 500mg
Price: $260
Updated: 2021/12/16

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2-BROMO-6-IODO-3-METHOXYPYRIDINE Chemical Properties,Usage,Production

Synthesis

129611-32-1

74-88-4

321535-37-9

Stage 1(b): synthesis of 2-bromo-6-iodo-3-methoxypyridine (3). Potassium carbonate (K2CO3, 6.22 g, 45.1 mmol) and iodomethane (CH3I, 24.6 g, 10.77 mL, 173.3 mmol) were sequentially added to a solution of N,N-dimethylformamide (DMF, 30 mL) in which 2-bromo-6-iodo-pyridin-3-ol (2, 14.9 g, 49.5 mmol) was dissolved. The reaction mixture was heated and stirred at 100 °C for 2 h and subsequently cooled to room temperature. Reaction termination was achieved by addition of water (H2O) and stirring was continued for 30 min. The precipitate formed was collected by filtration, washed with water and dried in air to give light brown solid product 3 (15.7 g, 100% yield). The product was characterized by the following data: 1H NMR (CDCl3) δ 7.61 (d, 1H, J = 8.4 Hz), 6.86 (d, 1H, J = 8.4 Hz), 3.93 (s, 3H); mass spectral observation m/z = 314 (M + 1), 315.

References

[1] Patent: US2008/45561, 2008, A1. Location in patent: Page/Page column 25; 22
[2] Organic Letters, 2000, vol. 2, # 26, p. 4201 - 4204
[3] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 21, p. 6435 - 6446
[4] Patent: WO2014/43252, 2014, A2. Location in patent: Page/Page column 45-46
[5] Patent: WO2007/88999, 2007, A1. Location in patent: Page/Page column 166

2-BROMO-6-IODO-3-METHOXYPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-6-IODO-3-METHOXYPYRIDINE Suppliers

China 91 India 2 United Kingdom 1 United States 12 Global 106

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View Lastest Price from 2-BROMO-6-IODO-3-METHOXYPYRIDINE manufacturers

Career Henan Chemical Co

Product: 2-Bromo-6-iodo-3-methoxypyridine 321535-37-9
Price: US $8.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 100kg
Release date: 2019-07-09

321535-37-9, 2-BROMO-6-IODO-3-METHOXYPYRIDINERelated Search:

Trimethoprim 2-BROMO-3-DIFLUOROMETHOXY-6-IODOPYRIDINE 2-IODO-5-METHOXYPYRIDINE 2-Bromo-6-iodopyridine 2-Bromo-3-hydroxy-6-iodopyridine 2-BROMO-6-IODO-3-METHOXYPYRIDINE

2-BROMO-6-IODO-3-METHOXYPYRIDINE

2-Bromo-3-methoxy-6-iodopyridine

Pyridine, 2-bromo-6-iodo-3-methoxy-

321535-37-9