ETHYL 2,2-DIMETHOXYETHYLCARBAMATE
- Product Name
- ETHYL 2,2-DIMETHOXYETHYLCARBAMATE
- CAS No.
- 71545-60-3
- Chemical Name
- ETHYL 2,2-DIMETHOXYETHYLCARBAMATE
- Synonyms
- ETHYL 2,2-DIMETHOXYETHYLCARBAMATE;Carbamic acid, N-(2,2-dimethoxyethyl)-, ethyl ester
- CBNumber
- CB42453196
- Molecular Formula
- C7H15NO4
- Formula Weight
- 177.2
- MOL File
- 71545-60-3.mol
ETHYL 2,2-DIMETHOXYETHYLCARBAMATE Property
- Boiling point:
- 62-63 °C(Press: 0.2 Torr)
- Density
- 1.0823 g/cm3
- storage temp.
- 2-8°C, protect from light
- pka
- 12.61±0.46(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- E939955
- Product name
- Ethyl2,2-dimethoxyethylcarbamate
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CHM0384430
- Product name
- ETHYL-2,2-DIMETHOXYETHYLCARBAMATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.23
- Updated
- 2021/12/16
- Product number
- SC-74018
- Product name
- ETHYL2,2-DIMETHOXYETHYLCARBAMATE
- Purity
- 95
- Packaging
- 1.5kg
- Price
- $2700
- Updated
- 2021/12/16
- Product number
- CD13005832
- Product name
- Ethyl(2,2-dimethoxyethyl)carbamate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $120
- Updated
- 2021/12/16
- Product number
- CD13005832
- Product name
- Ethyl(2,2-dimethoxyethyl)carbamate
- Purity
- 95+%
- Packaging
- 10g
- Price
- $230
- Updated
- 2021/12/16
ETHYL 2,2-DIMETHOXYETHYLCARBAMATE Chemical Properties,Usage,Production
Synthesis
541-41-3
22483-09-6
71545-60-3
General procedure: Ethyl chloroformate (4.37 mL, 45.77 mmol) was slowly added dropwise to a dichloromethane/water (25/12 mL) mixture containing aminoacetaldehyde dimethyl acetal (5 mL, 45.77 mmol) and sodium hydroxide (2.05 g, 51.26 mmol) under ice bath cooling conditions, ensuring that the temperature in the reaction system was maintained at less than 10°C. The reaction was carried out at room temperature with vigorous stirring. After dropwise addition, cooling was stopped and the reaction mixture was stirred vigorously at room temperature. Upon completion of the reaction, the organic and aqueous phases were separated, and the organic phase was washed with saturated brine, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford ethyl 2,2-dimethoxyethylcarbamate as a colorless oil (8.1 g, quantitative yield). Mass spectrum (m/z): 178.1 [M+H]+.
References
[1] Patent: WO2017/21920, 2017, A1. Location in patent: Paragraph 0625; 0626
[2] Patent: WO2013/14448, 2013, A1. Location in patent: Page/Page column 99; 100
[3] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 17, p. 2491 - 2496
[4] Patent: US4990517, 1991, A
[5] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 11, p. 2891 - 2894
ETHYL 2,2-DIMETHOXYETHYLCARBAMATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from ETHYL 2,2-DIMETHOXYETHYLCARBAMATE manufacturers
- Product
- ETHYL 2,2-DIMETHOXYETHYLCARBAMATE 71545-60-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 97%-98%
- Supply Ability
- 200KG
- Release date
- 2019-09-03