[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER
- Product Name
- [4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER
- CAS No.
- 457631-44-6
- Chemical Name
- [4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER
- Synonyms
- 4-(2-Aminoethyl)-N-Boc-aniline;tert-Butyl (4-(2-aminoethyl)phenyl)carbamate;[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER;Carbamic acid, N-[4-(2-aminoethyl)phenyl]-, 1,1-dimethylethyl ester
- CBNumber
- CB42460370
- Molecular Formula
- C13H20N2O2
- Formula Weight
- 236.31
- MOL File
- 457631-44-6.mol
[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER Property
- Melting point:
- 89-91 °C
- Boiling point:
- 315.9±25.0 °C(Predicted)
- Density
- 1.099±0.06 g/cm3(Predicted)
- storage temp.
- Store at Room Tem.
- pka
- 13.79±0.70(Predicted)
- Appearance
- white to off-white solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- CHM0125011
- Product name
- (4-(2-AMINO-ETHYL)-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER
- Purity
- 96.00%
- Packaging
- 1G
- Price
- $1070.84
- Updated
- 2021/12/16
- Product number
- 4658AJ
- Product name
- tert-ButylN-[4-(2-aminoethyl)phenyl]carbamate
- Packaging
- 2.5g
- Price
- $1451
- Updated
- 2021/12/16
- Product number
- CHM0125011
- Product name
- (4-(2-AMINO-ETHYL)-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER
- Purity
- 96.00%
- Packaging
- 2.5G
- Price
- $1635.3
- Updated
- 2021/12/16
- Product number
- CHM0125011
- Product name
- (4-(2-AMINO-ETHYL)-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER
- Purity
- 96.00%
- Packaging
- 5G
- Price
- $2181.31
- Updated
- 2021/12/16
- Product number
- 20R0424
- Product name
- [4-(2-Amino-ethyl)-phenyl]-carbamicacidtert-butylester
- Purity
- 96%
- Packaging
- 5g
- Price
- $1590
- Updated
- 2021/12/16
[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER Chemical Properties,Usage,Production
Synthesis
[4-(2-Amino-ethyl)-phenyl]-carbamic acid tert-butyl ester is synthesised using 4-tert-butoxycarbonylaminophenylacetonitrile as a raw material by chemical reaction. The specific synthesis steps are as follows:
To a solution of (300 gm, 1.29 moles) N-BOC-4-aminophenylacetonitrile in 3000 ml of methanol, 25% aq. ammonia solution (480 ml) and Raney nickel (45 gm) were added at 25 -30°C. Reaction mixture was subjected to hydrogenation at 50-60 PSI for 4 hrs. After completion of reaction, as indicated from TLC, reaction mixture was filtered and washed with (2 X 25 ml) methanol. Filtrate was concentrated under vacuum and resulting residue was treated with (1500 ml) 1M aq. hydrochloric acid at 25-30°C. Reaction mixture was stirred for 15 minutes and filtered to remove insoluble impurities. Filtrate was basified to pH 10-12 with 50% aq. NaOH solution below 25°C. Precipitated 4-(2-aminoethyl)-N-(tert-butoxycarbonyl) phenylamine was filtered and washed with (2 X 100 ml) water. Solid was dried under vacuum at 55- 60°C for 8-10 hrs. Dry weight: 240 gm (79%). 1H NMR (CDC13 and 400 MHz): δ 1.11 (2H, s), 1.51 (9H, s), 2.68 (2H, t), 2.93 (2H, t), 6.72 (1H, s), 7.10 (2H, d), 7.28 (2H, d).
[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
[4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER Suppliers
- Tel
- 021-58930698 15921516558
- Fax
- 86-021-58933679
- zhangyichao84@126.com
- Country
- China
- ProdList
- 981
- Advantage
- 55
- Tel
- 021-64340559 13651849907;
- Fax
- 021- 64345308
- xinyu_shi@jwypharmlab.com.cn
- Country
- China
- ProdList
- 12000
- Advantage
- 58
- Tel
- 400-685-9117
- Fax
- 021-51816740
- market@bepharm.com
- Country
- China
- ProdList
- 15081
- Advantage
- 60
- Tel
- 0512-56316828
- Fax
- 0512-56316826
- info@amateksci.com
- Country
- China
- ProdList
- 28785
- Advantage
- 58
- Tel
- 0551-66336380 18956014586
- Fax
- 055166336380
- 983438788@qq.com
- Country
- China
- ProdList
- 2297
- Advantage
- 58
- Tel
- zhiqianbio@126.com
- Country
- China
- ProdList
- 19778
- Advantage
- 58
- Tel
- +86-27-50766799 +8618062016861
- contact@labnetwork.com
- Country
- China
- ProdList
- 19987
- Advantage
- 58
- Tel
- 021-58461859 15821823057
- service@aiviche.com
- Country
- China
- ProdList
- 49312
- Advantage
- 58
- Tel
- 18721109360
- 306685371@qq.com
- Country
- China
- ProdList
- 1944
- Advantage
- 58
- Tel
- 025-025-66113011 18626450290
- cb5@aikonchem.com
- Country
- China
- ProdList
- 10358
- Advantage
- 58
View Lastest Price from [4-(2-AMINO-ETHYL)-PHENYL]-CARBAMIC ACID TERT-BUTYL ESTER manufacturers
- Product
- tert-Butyl (4-(2-aminoethyl)phenyl)carbamate 457631-44-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 0.1kg
- Purity
- 97% Min.
- Supply Ability
- 500kg
- Release date
- 2024-01-18