2-aminocyclohexanone hydrochloride
- Product Name
- 2-aminocyclohexanone hydrochloride
- CAS No.
- 6946-05-0
- Chemical Name
- 2-aminocyclohexanone hydrochloride
- Synonyms
- 146315;2-Aminocyclohexanone hcl;Cyclohexanone, 2-amino-, HCl;2-aminocyclohexanone hydrochloride;2-Aminocyclohexan-1-one hydrochloride;Cyclohexanone,2-amino-, hydrochloride;Cyclohexanone, 2-amino-, hydrochloride (1:1)
- CBNumber
- CB42506070
- Molecular Formula
- C6H12ClNO
- Formula Weight
- 149.61858
- MOL File
- 6946-05-0.mol
2-aminocyclohexanone hydrochloride Property
- Melting point:
- 157-158 °C (decomp)
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C6H11NO.ClH/c7-5-3-1-2-4-6(5)8;/h5H,1-4,7H2;1H
- InChIKey
- HGHZKLDCXNJLJK-UHFFFAOYSA-N
- SMILES
- C1(=O)CCCCC1N.[H]Cl
Safety
- Hazard Codes
- Xn,N
- Risk Statements
- 22-41-51/53
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H318Causes serious eye damage
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P330Rinse mouth.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- A938145
- Product name
- 2-Aminocyclohexanonehydrochloride
- Packaging
- 100mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- 180197
- Product name
- 2-Aminocyclohexanone hydrochloride
- Packaging
- 500mg
- Price
- $480
- Updated
- 2021/12/16
- Product number
- CHM0388031
- Product name
- 2-AMINOCYCLOHEXANONE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.63
- Updated
- 2021/12/16
- Product number
- 180197
- Product name
- 2-Aminocyclohexanone hydrochloride
- Packaging
- 1g
- Price
- $600
- Updated
- 2021/12/16
- Product number
- 0726AC
- Product name
- 2-Aminocyclohexanonehydrochloride
- Packaging
- 500mg
- Price
- $692
- Updated
- 2021/12/16
2-aminocyclohexanone hydrochloride Chemical Properties,Usage,Production
Synthesis
4883-67-4
6946-05-0
General procedure for the synthesis of 2-aminocyclohexanone hydrochloride from 2-nitrocyclohexanone: 2-nitrocyclohexanone (7.0 g, 48.9 mmol), 5% carbon sulfide (500 mg), ethanol (120 mL), and concentrated hydrochloric acid (6 mL) were added to a pressure vessel under nitrogen protection. The vessel was pressurized to 50 psi with hydrogen and the reaction mixture was stirred for 3 hours. Upon completion of the reaction, the mixture was filtered through EPO Celite? The filter cake was washed sequentially with ethanol and dichloromethane (DCM) under nitrogen atmosphere. The filtrate was concentrated under reduced pressure. The concentrated residue was slurried in acetone (50 mL) and filtered. The solid was collected to afford the target product 2-aminocyclohexanone hydrochloride (2.2 g, 40% yield).
References
[1] Tetrahedron Letters, 1986, vol. 27, # 47, p. 5759 - 5762
[2] Patent: WO2007/28082, 2007, A1. Location in patent: Page/Page column 70-71
2-aminocyclohexanone hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
2-aminocyclohexanone hydrochloride Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 2-aminocyclohexanone hydrochloride manufacturers
- Product
- 2-aminocyclohexanone hydrochloride 6946-05-0
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-09