o-Mesitylenesulfonyl HydroxylaMine
- Product Name
- o-Mesitylenesulfonyl HydroxylaMine
- CAS No.
- 58042-39-0
- Chemical Name
- o-Mesitylenesulfonyl HydroxylaMine
- Synonyms
- SKL560;Mesitylenesulfonylhydroxylamine;Benzenesulfonamide, N-hydroxy-2,4,6-trimethyl-
- CBNumber
- CB42546108
- Molecular Formula
- C9H13NO3S
- Formula Weight
- 215.27
- MOL File
- 58042-39-0.mol
o-Mesitylenesulfonyl HydroxylaMine Property
- Boiling point:
- 381.0±52.0 °C(Predicted)
- Density
- 1.267±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 6.37±0.69(Predicted)
- Appearance
- White to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- H852900
- Product name
- N-Hydroxy-2,4,6-trimethylbenzenesulfonamide
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 7276AJ
- Product name
- N-Hydroxy-2,4,6-trimethylbenzenesulfonamide
- Packaging
- 1g
- Price
- $173
- Updated
- 2021/12/16
- Product number
- A230128
- Product name
- N-Hydroxy-2,4,6-trimethylbenzenesulfonamide
- Purity
- 95+%
- Packaging
- 5g
- Price
- $307
- Updated
- 2021/12/16
- Product number
- CM253787
- Product name
- N-Hydroxy-2,4,6-trimethylbenzenesulfonamide
- Purity
- 95%
- Packaging
- 5g
- Price
- $393
- Updated
- 2021/12/16
- Product number
- CD12058934
- Product name
- N-Hydroxy-2,4,6-trimethylbenzenesulfonamide
- Purity
- 95+%
- Packaging
- 5g
- Price
- $416
- Updated
- 2021/12/16
o-Mesitylenesulfonyl HydroxylaMine Chemical Properties,Usage,Production
Synthesis
773-64-8
58042-39-0
GENERAL METHOD: Hydroxylamine hydrochloride (2 eq.) and DMAP (2 eq.) were dissolved in pyridine (20 mL) in an ice bath and 2,4,6-trimethylbenzenesulfonyl chloride (1 eq.) was slowly added. The reaction mixture was stirred at room temperature for 5 minutes. The resulting suspension was poured into a mixture of ethyl acetate (100 mL) and 1N aqueous hydrochloric acid (100 mL). The organic layer (ethyl acetate layer) was separated, washed with saturated brine (100 mL), dried over anhydrous sodium sulfate, filtered and concentrated. The crude product was purified by fast column chromatography under the following gradient conditions and recrystallized from a mixed ether/hexane solvent to give N-hydroxy-2,4,6-trimethylbenzenesulfonamide.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 8, p. 2340 - 2343
o-Mesitylenesulfonyl HydroxylaMine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from o-Mesitylenesulfonyl HydroxylaMine manufacturers
- Product
- o-Mesitylenesulfonyl HydroxylaMine 58042-39-0
- Price
- US $0.01/KG
- Min. Order
- 500g
- Purity
- 98%; 99%
- Supply Ability
- 500g;1kg; 10kg; 25kg
- Release date
- 2020-01-08