3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol
- Product Name
- 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol
- CAS No.
- 221352-10-9
- Chemical Name
- 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol
- Synonyms
- 3,3-Dimethylbenzo[c][1,2]oxaborol-1(3H);1-hydroxy-3,3-dimethyl-2,1-benzoxaborole;3,3-DIMETHYL-3H-BENZO[C][1,2]OXABOROL-1-OL;3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol;3,3-dimethyl-1,3-dihydro-2,1-benzoxaborol-1-ol;1,3-Dihydro-1-hydroxy-3,3-diMethyl-2,1-benzoxaborole;3,3-DIMETHYLBENZO[C][1,2]OXABOROL-1(3H)-OL(WXC01846);3,3-Dimethyl-1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborole
- CBNumber
- CB42594235
- Molecular Formula
- C9H11BO2
- Formula Weight
- 161.99
- MOL File
- 221352-10-9.mol
3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol Property
- Boiling point:
- 242.5±43.0 °C(Predicted)
- Density
- 1.10±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 7.04±0.40(Predicted)
Safety
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 097912
- Product name
- 3,3-Dimethylbenzo[c][1,2]oxaborol-1(3H)-ol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $492
- Updated
- 2021/12/16
- Product number
- 097912
- Product name
- 3,3-Dimethylbenzo[c][1,2]oxaborol-1(3H)-ol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $1092
- Updated
- 2021/12/16
- Product number
- BOR0002245
- Product name
- 1,3-DIHYDRO-1-HYDROXY-3,3-DIMETHYL-2,1-BENZOXABOROLE
- Purity
- 95.00%
- Packaging
- 10G
- Price
- $1334.03
- Updated
- 2021/12/16
- Product number
- BOR0002245
- Product name
- 1,3-DIHYDRO-1-HYDROXY-3,3-DIMETHYL-2,1-BENZOXABOROLE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1980.3
- Updated
- 2021/12/16
- Product number
- 221352109
- Product name
- 3,3-Dimethylbenzo[c][1,2]oxaborol-1(3H)-ol
- Packaging
- 500g
- Price
- $11698.2
- Updated
- 2021/12/16
3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol Chemical Properties,Usage,Production
Synthesis
To a solution of 2-(2-bromo-phenyl)-propane-2-ol (4.0 g, 18.6 mmol) in anhydrous THF (60 mL) under argon was slowly added n-butyl lithium (15 mL, 2.5 M). The mixture was stirred at -78° C for 2 h, and then triisopropylborate (5.5 mL, 24.2 mmol) was added to the mixture. The mixture was heated to room temperature and stirred for 12 h and then cooled to 0° C. Hydrochloric acid (10 mL, 1N) was added to the mixture until pH<5. The reaction system was then stirred at RT for 1 h. Until the solution was separated, the aqueous layer was extracted twice with ethyl acetate. The organic layers were combined, dried with anhydrous sodium sulfate, and filtered. The filtrate was concentrated under reduced pressure to afford a yellow oil. The oil was purified by chromatography (silica, EtOAc: hexanes,1:3) to afford 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol which is a white solid.
3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol Preparation Products And Raw materials
Raw materials
Preparation Products
3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol Suppliers
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
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- 6100
- Advantage
- 58
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- enquiry@sldrugs.com
- Country
- India
- ProdList
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View Lastest Price from 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol manufacturers
- Product
- 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol 221352-10-9
- Price
- US $6.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg, 5kg, 50kg
- Release date
- 2020-01-09