Uses Application
ChemicalBook > CAS DataBase List > 4-(N-Boc-N-MethylaMino)cyclohexanol

4-(N-Boc-N-MethylaMino)cyclohexanol

Uses Application
Product Name
4-(N-Boc-N-MethylaMino)cyclohexanol
CAS No.
1256633-24-5
Chemical Name
4-(N-Boc-N-MethylaMino)cyclohexanol
Synonyms
4-(N-Boc-N-MethylaMino)cyclohexanol;Carbamic acid,N-(4-hydroxycyclohexyl)-N-methyl-, 1,1-dimethylethyl ester
CBNumber
CB42597140
Molecular Formula
C12H23NO3
Formula Weight
229.32
MOL File
1256633-24-5.mol
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4-(N-Boc-N-MethylaMino)cyclohexanol Property

Boiling point:
319.2±31.0 °C(Predicted)
Density 
1.05±0.1 g/cm3(Predicted)
pka
15.09±0.40(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

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N-Bromosuccinimide Price

AK Scientific
Product number
Y5983
Product name
tert-Butyl4-hydroxycyclohexyl(methyl)carbamate
Packaging
5g
Price
$458
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0096859
Product name
TERT-BUTYL-(4-HYDROXYCYCLOHEXYL)METHYLCARBAMATE
Purity
95.00%
Packaging
5MG
Price
$497.83
Updated
2021/12/16
Crysdot
Product number
CD13025151
Product name
4-(N-Boc-N-methylamino)cyclohexanol
Purity
95+%
Packaging
5g
Price
$327
Updated
2021/12/16
Chemenu
Product number
CM324211
Product name
4-(N-Boc-N-methylamino)cyclohexanol
Purity
95%
Packaging
10g
Price
$438
Updated
2021/12/16
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4-(N-Boc-N-MethylaMino)cyclohexanol Chemical Properties,Usage,Production

Uses

4-(N-BOC-N-methylamino)cyclohexanol can be used as a pharmaceutical synthesis intermediate.

Application

4-(N-BOC-N-methylamino)cyclohexanol (30 g, 149.1 mmol, 1 eq.), triethylamine (22.87 mL, 164 mmol, 1.1 eq.), and N,N-dimethylpyridine-4-amine (DMAP) (1.83 g, 14.98 mmol, 0.1 eq.) were dissolved in anhydrous dichloromethane (500 mL) and cooled to 0 °C in an ice bath. Methanesulfonyl chloride (12.12 mL, 156.6 mmol, 1.05 equivalents) was added dropwise. After the addition was complete, the reaction mixture was warmed to room temperature and stirred for 16 hours. The reaction mixture was washed with water (3 × 100 mL) and saturated sodium bicarbonate (3 × 100 mL). The combined washings were back-extracted with dichloromethane. The combined organic compounds were dried over Na2SO4 and concentrated to give 40.83 g (146.2 mmol) of 1-(tert-butyloxycarbonyl)piperidine-4-ylmethanesulfonate (compound 1013, 98% yield), which was a grayish-white solid and could be used without further processing.

4-(N-Boc-N-MethylaMino)cyclohexanol Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(N-Boc-N-MethylaMino)cyclohexanol Suppliers

China 16 India 1 United States 2 Global 19
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 4-(N-Boc-N-MethylaMino)cyclohexanol manufacturers

Career Henan Chemica Co
Product
4-(N-Boc-N-MethylaMino)cyclohexanol 1256633-24-5
Price
US $1.30/g
Min. Order
1g
Purity
98%
Supply Ability
1kg,10kg,100kg
Release date
2020-10-27

1256633-24-5, 4-(N-Boc-N-MethylaMino)cyclohexanolRelated Search:

N-CARBAMYL-L-GLUTAMIC ACID Ethylene glycol Carbamic acid, methyl(4-oxocyclohexyl)-, 1,1-dimethylethyl ester N-Acetyl-L-cysteine

  • 4-(N-Boc-N-MethylaMino)cyclohexanol
  • Carbamic acid,N-(4-hydroxycyclohexyl)-N-methyl-, 1,1-dimethylethyl ester
  • 1256633-24-5