1-(3-Ethoxy-4-Methoxyphenyl)ethanone

Product Name: 1-(3-Ethoxy-4-Methoxyphenyl)ethanone
CAS No.: 31526-71-3
Chemical Name: 1-(3-Ethoxy-4-Methoxyphenyl)ethanone
Synonyms: 1-(3-Ethoxy-4-methoxyphenyl);3''-Ethoxy-4''-methoxyacetophenone;1-(3-Ethoxy-4-Methoxyphenyl)ethanone;1-(3-ethoxy-4-methoxyphenyl)ethan-1-one;Ethanone, 1-(3-ethoxy-4-methoxyphenyl)-
CBNumber: CB42651983
Molecular Formula: C11H14O3
Formula Weight: 194.23
MOL File: 31526-71-3.mol

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1-(3-Ethoxy-4-Methoxyphenyl)ethanone Property

Melting point:: 66-67 °C(Solv: isopropanol (67-63-0))
Boiling point:: 295.2±20.0 °C(Predicted)
Density: 1.047±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature

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Safety

HS Code: 2914500090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 0955CU
Product name: 1-(3-Ethoxy-4-methoxyphenyl)ethanone
Packaging: 100mg
Price: $70
Updated: 2021/12/16

AK Scientific

Product number: 0955CU
Product name: 1-(3-Ethoxy-4-methoxyphenyl)ethanone
Packaging: 250mg
Price: $81
Updated: 2021/12/16

Rieke Metals

Product number: NV04396
Product name: 1-(3-ETHOXY-4-METHOXYPHENYL)ETHAN-1-ONE
Packaging: 1g
Price: $809
Updated: 2021/12/16

Rieke Metals

Product number: NV04396
Product name: 1-(3-ETHOXY-4-METHOXYPHENYL)ETHAN-1-ONE
Packaging: 5g
Price: $1943
Updated: 2021/12/16

Alichem

Product number: 31526713
Product name: 1-(3-Ethoxy-4-methoxyphenyl)ethanone
Packaging: 100g
Price: $441
Updated: 2021/12/16

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1-(3-Ethoxy-4-Methoxyphenyl)ethanone Chemical Properties,Usage,Production

Synthesis

74-96-4

6100-74-9

31526-71-3

Purified 4-methoxy-3-hydroxyacetophenone (24.9 g; 0.15 mol) was dissolved in dimethylformamide (80 ml) at room temperature. Potassium carbonate (27.6 g; 0.20 mol) was added to the reaction system, followed by the slow dropwise addition of ethyl bromide (18.0 g; 0.165 mol) at a temperature not exceeding 35 °C with simultaneous stirring and cooling to control the reaction temperature. The reaction mixture was stirred continuously at 30-35 °C for 5 h. Upon completion of the reaction, the system was cooled to below 10 °C, diluted with deionized water (240 ml) and stirring was continued at 0-10 °C for 2 h to promote product precipitation. The solid product was collected by filtration, washed with deionized water (2 x 100 ml) to remove residual inorganic salts and solvent, and finally dried under vacuum at 40 °C to constant weight to afford 1-(3-ethoxy-4-methoxyphenyl)ethanone (26.32 g; yield 90.4%; HPLC purity: 99.8%).

References

[1] Patent: WO2017/59040, 2017, A1. Location in patent: Paragraph 0078
[2] European Journal of Organic Chemistry, 2006, # 17, p. 4044 - 4054
[3] Organic Letters, 2017, vol. 19, # 11, p. 2877 - 2880
[4] Patent: CN105622380, 2016, A. Location in patent: Paragraph 0044; 0045; 0046; 0047
[5] Patent: US2007/259868, 2007, A1. Location in patent: Page/Page column 16

1-(3-Ethoxy-4-Methoxyphenyl)ethanone Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(3-Ethoxy-4-Methoxyphenyl)ethanone manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 1-(3-Ethoxy-4-Methoxyphenyl)ethanone 31526-71-3
Price: US $1.00/Kg
Min. Order: 1Kg
Purity: 98%
Supply Ability: 20T
Release date: 2024-07-20

31526-71-3, 1-(3-Ethoxy-4-Methoxyphenyl)ethanoneRelated Search:

1-(3-Ethoxy-4-Methoxyphenyl)ethanone

1-(3-Ethoxy-4-methoxyphenyl)

Ethanone, 1-(3-ethoxy-4-methoxyphenyl)-

3''-Ethoxy-4''-methoxyacetophenone

1-(3-ethoxy-4-methoxyphenyl)ethan-1-one

31526-71-3