ChemicalBook > CAS DataBase List > 1,8-Dichloroisoquinoline

1,8-Dichloroisoquinoline

Product Name
1,8-Dichloroisoquinoline
CAS No.
848841-64-5
Chemical Name
1,8-Dichloroisoquinoline
Synonyms
1,8-Dichloroisoquinoline;Isoquinoline, 1,8-dichloro-;1,8-Dichloroisoquinoline ISO 9001：2015 REACH
CBNumber
CB42652793
Molecular Formula
C9H5Cl2N
Formula Weight
198.05
MOL File
848841-64-5.mol
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1,8-Dichloroisoquinoline Property

storage temp. 
Inert atmosphere,Room Temperature
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
D439810
Product name
1,8-Dichloroisoquinoline
Packaging
100mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142519
Product name
1,8-Dichloroisoquinoline
Packaging
250mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142519
Product name
1,8-Dichloroisoquinoline
Packaging
500mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142519
Product name
1,8-Dichloroisoquinoline
Packaging
1g
Price
$177
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142519
Product name
1,8-Dichloroisoquinoline
Packaging
2g
Price
$308
Updated
2021/12/16
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1,8-Dichloroisoquinoline Chemical Properties,Usage,Production

Synthesis

34784-07-1

848841-64-5

Procedure for the synthesis of 1,8-dichloroisoquinoline: To a solution of 8-chloroisoquinoline (11 g, 54 mmol) in dichloromethane (200 mL) was added m-chloroperoxybenzoic acid (MCPBA, 25 g, 112 mmol) in batches. The reaction mixture was stirred for 3 hours and then ether (400 mL) and hexane (1 L) were added. The mixture was stirred overnight and subsequently concentrated under vacuum. Ether (200 mL) and hexane (400 mL) were added to the concentrate and stirred again overnight. The precipitate was collected by filtration, air dried and mixed with silica gel (20 g) and toluene (150 mL). The mixture was heated to reflux for 3 hours and neutralized with sodium bicarbonate (NaHCO3) when the reaction was complete. The reaction mixture was extracted with dichloromethane (CH2Cl2) and the organic layer was dried over anhydrous sodium sulfate and concentrated in vacuum to give 1,8-dichloroisoquinoline (8 g, 72% yield). Mass spectrum (MS): 198.

References

[1] Patent: WO2005/28444, 2005, A1. Location in patent: Page/Page column 67-68

1,8-Dichloroisoquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

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848841-64-5, 1,8-DichloroisoquinolineRelated Search:

CHLOROETHANE 1,2,3,4-TETRAHYDRO-4-METHYLQUINOLINE

  • 1,8-Dichloroisoquinoline
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  • 1,8-Dichloroisoquinoline ISO 9001：2015 REACH
  • 848841-64-5
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