Methyl 2-Methyl-6-quinolinecarboxylate

Product Name: Methyl 2-Methyl-6-quinolinecarboxylate
CAS No.: 108166-01-4
Chemical Name: Methyl 2-Methyl-6-quinolinecarboxylate
Synonyms: Methyl 2-Methylquinoline-6-carboxylate;Methyl 2-Methyl-6-quinolinecarboxylate;2-Methylquinoline-6-carboxylic acid methyl ester;2-Methyl-6-quinolinecarboxylic acid methyl ester;6-Quinolinecarboxylic acid, 2-methyl-, methyl ester
CBNumber: CB42653659
Molecular Formula: C12H11NO2
Formula Weight: 201.22
MOL File: 108166-01-4.mol

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Methyl 2-Methyl-6-quinolinecarboxylate Property

Melting point:: 103-105 °C
Boiling point:: 320.3±22.0 °C(Predicted)
Density: 1.177±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 4.90±0.43(Predicted)
color: Light grey
InChI: InChI=1S/C12H11NO2/c1-8-3-4-9-7-10(12(14)15-2)5-6-11(9)13-8/h3-7H,1-2H3
InChIKey: KGSIXOOGGCSYTB-UHFFFAOYSA-N
SMILES: N1C2C(=CC(C(OC)=O)=CC=2)C=CC=1C

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR52927
Product name: Methyl 2-methylquinoline-6-carboxylate
Purity: 98%
Packaging: 5g
Price: $104
Updated: 2021/12/16

AK Scientific

Product number: 6968AJ
Product name: Methyl2-methylquinoline-6-carboxylate
Packaging: 1g
Price: $84
Updated: 2021/12/16

Apolloscientific

Product number: OR52927
Product name: Methyl 2-methylquinoline-6-carboxylate
Purity: 98%
Packaging: 25g
Price: $361
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0294839
Product name: 2-METHYL-QUINOLINE-6-CARBOXYLIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 5MG
Price: $504.24
Updated: 2021/12/16

Matrix Scientific

Product number: 114700
Product name: Methyl 2-methylquinoline-6-carboxylate
Purity: 97%
Packaging: 1g
Price: $575
Updated: 2021/12/16

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Methyl 2-Methyl-6-quinolinecarboxylate Chemical Properties,Usage,Production

Synthesis

67-56-1

635-80-3

108166-01-4

Step 2: Synthesis of methyl 2-methylquinoline-6-carboxylate: 2-methyl-6-quinolinecarboxylic acid (3.0 g, 16.20 mmol) was dissolved in methanol (30 mL) at 0°C and concentrated sulfuric acid (3 mL) was added slowly and dropwise. Subsequently, the reaction mixture was warmed to 65°C and stirred continuously for 12 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure. The concentrated residue was extracted by adding dichloromethane and aqueous sodium carbonate to the concentrated residue. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford methyl 2-methylquinoline-6-carboxylate as a brown solid (1.9 g, 59% yield).

References

[1] Journal of Heterocyclic Chemistry, 1989, vol. 26, p. 929 - 931
[2] Angewandte Chemie - International Edition, 2016, vol. 55, # 40, p. 12224 - 12227
[3] Angew. Chem., 2016, vol. 128, # 40, p. 12412 - 12415,4
[4] Patent: WO2013/144737, 2013, A2. Location in patent: Paragraph 252
[5] Patent: US2015/57309, 2015, A1. Location in patent: Paragraph 0525

Methyl 2-Methyl-6-quinolinecarboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2-Methyl-6-quinolinecarboxylate Suppliers

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View Lastest Price from Methyl 2-Methyl-6-quinolinecarboxylate manufacturers

PNP Biotech Co. Ltd

Product: Methyl 2-methyl-6-quinolinecarboxylate 108166-01-4
Price: US $0.00/kg
Min. Order: 25kg
Purity: 98%
Supply Ability: Inquiry
Release date: 2023-07-04

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6-Quinolinecarboxylic acid, 2-methyl-, methyl ester

2-Methyl-6-quinolinecarboxylic acid methyl ester

108166-01-4