ChemicalBook > CAS DataBase List > 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole

9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole

Product Name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
CAS No.
618442-57-2
Chemical Name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
Synonyms
3,6-Bis(4,4,5,5-tetramethyl-1,3,2;9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborol;9-Phenyl-9H-carbazole-3,6-diboronic Acid Bis(pinacol) Ester;9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole;3,6-Bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9-phenylcarbazole;9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole;3,6-Bis(4,4,5,5-tetramethyl-1,3,2- dioxaborolan-2-yl)-9-phenyl-9H-carbazole;9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborolan- 2-yl)-9H-carbazol;9H-Carbazole, 9-phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
CBNumber
CB42655325
Molecular Formula
C30H35B2NO4
Formula Weight
495.23
MOL File
618442-57-2.mol
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9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Property

Melting point:
238.0 to 242.0 °C
Boiling point:
587.8±43.0 °C(Predicted)
Density 
1.11±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
powder to crystal
color 
White to Light yellow
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Safety

HS Code 
2934.99.4400
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
P2350
Product name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
Purity
>98.0%(HPLC)(N)
Packaging
200mg
Price
$50
Updated
2025/07/31
TCI Chemical
Product number
P2350
Product name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
Purity
>98.0%(HPLC)(N)
Packaging
1g
Price
$149
Updated
2025/07/31
Ark Pharm
Product number
AK202330
Product name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
Purity
97%
Packaging
250mg
Price
$16
Updated
2021/12/16
Ark Pharm
Product number
AK202330
Product name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
Purity
97%
Packaging
1g
Price
$39
Updated
2021/12/16
AK Scientific
Product number
6971AL
Product name
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
Packaging
10g
Price
$319
Updated
2021/12/16
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9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Chemical Properties,Usage,Production

Synthesis

73183-34-3

57103-20-5

618442-57-2

3,6-Dibromo-9-phenylcarbazole (0.075 mol) and pinacol ester of bisboronic acid (0.164 mol) were dissolved in 300 mL of dioxane and potassium acetate (0.375 mol) and tetrakis(triphenylphosphine)palladium (0.00075 mol) were added sequentially. The reaction mixture was heated to reflux for 5 hours. Upon completion of the reaction, the reaction was quenched with dichloromethane and water. The organic phase was separated and filtered through a silica gel funnel. Subsequently, the organic phase was concentrated under reduced pressure to remove the solvent. Finally, the resulting solid was purified by column chromatography to afford the target product 9-phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole (45% yield).

References

[1] Patent: CN106928237, 2017, A. Location in patent: Paragraph 0212; 0213; 0214

9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole Suppliers

TOKYO CHEMICAL INDUSTRY CO., LTD.
Tel
03-36680489
Fax
03-3668-0520
Email
Sales-JP@TCIchemicals.com
Country
Japan
ProdList
28387
Advantage
80
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View Lastest Price from 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
Price
US $2.20-8.80/kg
Min. Order
1kg
Purity
99%min
Supply Ability
100kg
Release date
2025-06-17
Shanghai Daken Advanced Materials Co.,Ltd
Product
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
Price
US $0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
150KG /month
Release date
2021-11-12
Shanghai UCHEM Inc.
Product
9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole 618442-57-2
Price
US $15.00-250.00/g
Min. Order
5g
Purity
0.98
Supply Ability
100kg
Release date
2024-10-25

618442-57-2, 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazoleRelated Search:


  • 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)carbazole
  • 9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborolan- 2-yl)-9H-carbazol
  • 9-Phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
  • 3,6-Bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9-phenylcarbazole
  • 3,6-Bis(4,4,5,5-tetramethyl-1,3,2
  • 9-Phenyl-3,6-bis(4,4,5,5- tetraMethyl-1,3,2-dioxaborol
  • 9H-Carbazole, 9-phenyl-3,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
  • 9-Phenyl-9H-carbazole-3,6-diboronic Acid Bis(pinacol) Ester
  • 3,6-Bis(4,4,5,5-tetramethyl-1,3,2- dioxaborolan-2-yl)-9-phenyl-9H-carbazole
  • 618442-57-2
  • C30H35B2NO4