4,4'-dibroMo-2,2'-dinitrobiphenyl
- Product Name
- 4,4'-dibroMo-2,2'-dinitrobiphenyl
- CAS No.
- 91371-12-9
- Chemical Name
- 4,4'-dibroMo-2,2'-dinitrobiphenyl
- Synonyms
- 4,4'-Dibrom-2,2'-dinitro-biphenyl;4,4'-dibroMo-2,2'-dinitrobiphenyl;4,4'-Dibromo-2,2'-dinitro-1,1'-biphenyl;1,1'-Biphenyl, 4,4'-dibroMo-2,2'-dinitro-;4-bromo-1-(4-bromo-2-nitrophenyl)-2-nitrobenzene
- CBNumber
- CB42657248
- Molecular Formula
- C12H6Br2N2O4
- Formula Weight
- 401.99
- MOL File
- 91371-12-9.mol
4,4'-dibroMo-2,2'-dinitrobiphenyl Property
- Melting point:
- 145-150°C
- Boiling point:
- 452.9±40.0 °C(Predicted)
- Density
- 1.907±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- Appearance
- Light yellow to yellow Solid
Safety
- Hazard Codes
- Xi,N
- Risk Statements
- 37/38-41-50
- Safety Statements
- 26-39-61
- RIDADR
- UN 3077 9 / PGIII
- WGK Germany
- 3
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
H400Very toxic to aquatic life
- Precautionary statements
-
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 755362
- Product name
- 4,4′-Dibromo-2,2′-dinitrobiphenyl
- Purity
- 97%
- Packaging
- 1g
- Price
- $94.81
- Updated
- 2025/07/31
- Product number
- D425438
- Product name
- 4,4-Dibromo-2,2-dinitrobiphenyl
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D425438
- Product name
- 4,4-Dibromo-2,2-dinitrobiphenyl
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 1111AQ
- Product name
- 4,4′-Dibromo-2,2′-dinitrobiphenyl
- Packaging
- 1g
- Price
- $161
- Updated
- 2021/12/16
- Product number
- HCH0365240
- Product name
- 4,4'-DIBROMO-2,2'-DINITRO-1,1'-BIPHENYL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.4
- Updated
- 2021/12/16
4,4'-dibroMo-2,2'-dinitrobiphenyl Chemical Properties,Usage,Production
Synthesis
3460-18-2
91371-12-9
(1) Under nitrogen protection, 2,5-dibromonitrobenzene (14.1 g, 50 mmol) was dissolved in 55 mL of N,N-dimethylformamide with copper powder (7.0 g, 109 mmol), and the reaction was stirred for 1 hour at 125°C. After completion of the reaction, the reaction was cooled to room temperature, the reaction mixture was filtered, and the solid residue was washed with an appropriate amount of toluene to ensure that the target product, 4,4'-dibromo-2,2'-dinitrobiphenyl, was dissolved in the filtrate. The filtrate was distilled under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography and separated under reduced pressure with petroleum ether and dichloromethane (4:1, v/v) as eluent to give a yellow solid product in 91% yield. The product was characterized by 1H NMR and confirmed to be 4,4'-dibromo-2,2'-dinitrobiphenyl.
References
[1] Journal of Materials Chemistry C, 2015, vol. 3, # 11, p. 2624 - 2631
[2] Journal of Materials Chemistry A, 2016, vol. 4, # 22, p. 8750 - 8754
[3] Patent: CN104311588, 2016, B. Location in patent: Paragraph 0026; 0027
[4] Journal of the American Chemical Society, 2005, vol. 127, # 21, p. 7662 - 7663
[5] Patent: CN103819455, 2016, B. Location in patent: Paragraph 0067; 0068; 0069
4,4'-dibroMo-2,2'-dinitrobiphenyl Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4,4'-dibroMo-2,2'-dinitrobiphenyl manufacturers
- Product
- 4,4'-Dibromo-2,2'-dinitrobiphenyl 91371-12-9
- Price
- US $1.10-9.90/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 100kg
- Release date
- 2025-08-18
- Product
- 4,4'-dibroMo-2,2'-dinitrobiphenyl 91371-12-9
- Price
- US $6.60/KG
- Min. Order
- 500g
- Purity
- 98%
- Supply Ability
- 1KG, 50KG, 100KG
- Release date
- 2019-12-25