4-Chloro-N-Methoxy-N-MethylbutyraMide
- Product Name
- 4-Chloro-N-Methoxy-N-MethylbutyraMide
- CAS No.
- 64214-66-0
- Chemical Name
- 4-Chloro-N-Methoxy-N-MethylbutyraMide
- Synonyms
- 4- Chloro-N-methoxy-N-methyl butyl;N-Methyl-N-methoxy-4-chlorobutanamide;4-Chloro-N-methoxy-N-methylbutanamide;4-Chloro-N-Methoxy-N-MethylbutyraMide;N-methoxy-N-methyl-4-chloroprene amide;3-N-Methoxy-N-methyl-4-chlorobutyramide;Butanamide, 4-chloro-N-methoxy-N-methyl-;2- Chloro - N - Methoxy - N - Methylbutyramide
- CBNumber
- CB42657495
- Molecular Formula
- C6H12ClNO2
- Formula Weight
- 165.62
- MOL File
- 64214-66-0.mol
4-Chloro-N-Methoxy-N-MethylbutyraMide Property
- Boiling point:
- 199.1±42.0 °C(Predicted)
- Density
- 1.106±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- Appearance
- Colorless to light yellow Liquid
N-Bromosuccinimide Price
- Product number
- C381975
- Product name
- 4-Chloro-N-methoxy-N-methylbutanamide
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- CS-0046358
- Product name
- 4-Chloro-N-methoxy-N-methylbutanamide
- Packaging
- 5g
- Price
- $302
- Updated
- 2021/12/16
- Product number
- 2564AQ
- Product name
- 4-CHLORO-N-METHOXY-N-METHYLBUTANAMIDE
- Packaging
- 5g
- Price
- $425.6
- Updated
- 2021/12/16
- Product number
- CS-0046358
- Product name
- 4-Chloro-N-methoxy-N-methylbutanamide
- Packaging
- 250mg
- Price
- $51
- Updated
- 2021/12/16
- Product number
- CS-0046358
- Product name
- 4-Chloro-N-methoxy-N-methylbutanamide
- Packaging
- 1g
- Price
- $101
- Updated
- 2021/12/16
4-Chloro-N-Methoxy-N-MethylbutyraMide Chemical Properties,Usage,Production
Synthesis
6638-79-5
4635-59-0
64214-66-0
To a solution of 4-chlorobutanoyl chloride (50.0 g, 355 mmol) and N-methoxy-N-methylamine hydrochloride (34.6 g, 355 mmol) in dichloromethane (DCM, 709 mL) was slowly added triethylamine (TEA, 109 mL, 780 mmol) at 0 °C, the addition process lasted 30 min. The reaction mixture was continued to be stirred at 0 °C for 3 hours. Upon completion of the reaction, it was quenched by the addition of water (250 mL). The organic layer was separated, washed with saturated brine, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to afford 4-chloro-N-methoxy-N-methylbutyramide (55.0 g, 94% yield) as a yellow oil, which could be used for the subsequent reaction without further purification.1H-NMR (CDCl3, Varian, 400 MHz) δ: 2.12 ( 2H, quintuple peak, J = 6.4 Hz), 2.63 (2H, triple peak, J = 7.2 Hz), 3.19 (3H, single peak), 3.64 (2H, triple peak, J = 6.4 Hz), 3.71 (3H, single peak).
References
[1] Patent: CN104672121, 2017, B. Location in patent: Paragraph 0038-0040
[2] Patent: WO2005/37197, 2005, A2. Location in patent: Page/Page column 104
[3] Patent: US2016/168156, 2016, A1. Location in patent: Paragraph 0195; 0197; 0198
[4] European Journal of Medicinal Chemistry, 2018, vol. 158, p. 353 - 370
4-Chloro-N-Methoxy-N-MethylbutyraMide Preparation Products And Raw materials
Raw materials
Preparation Products
4-Chloro-N-Methoxy-N-MethylbutyraMide Suppliers
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View Lastest Price from 4-Chloro-N-Methoxy-N-MethylbutyraMide manufacturers
- Product
- 4-Chloro-N-Methoxy-N-Methylbutyramide 64214-66-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 4-Chloro-N-Methoxy-N-Methylbutyramide 64214-66-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09
- Product
- 4-Chloro-N-Methoxy-N-MethylbutyraMide 64214-66-0
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99.99
- Supply Ability
- 10Ton
- Release date
- 2020-09-27