ChemicalBook > CAS DataBase List > 4-Acetyl-4'-bromobiphenyl
4-Acetyl-4'-bromobiphenyl
- Product Name
- 4-Acetyl-4'-bromobiphenyl
- CAS No.
- 5731-01-1
- Chemical Name
- 4-Acetyl-4'-bromobiphenyl
- Synonyms
- AKOS BAR-2458;Acetylbromodiphenyl;TIMTEC-BB SBB005889;4-ACETYL-4'-BROMODIPHENYL;4-Acetyl-4'-bromobiphenyl;4-bromo-4'-acetylbiphenyl;4-Acetyl-4'-bromobiphenyl;4-(4-BROMOPHENYL)ACETOPHENONE;4-Acetyl-4'-bromobiphenyl 90%;4-Acetyl-4'-bromobiphenyl >
- CBNumber
- CB4266556
- Molecular Formula
- C14H11BrO
- Formula Weight
- 275.14
- MOL File
- 5731-01-1.mol
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4-Acetyl-4'-bromobiphenyl Property
- Melting point:
- 129-133 °C(lit.)
- Boiling point:
- 372.1±17.0 °C(Predicted)
- Density
- 1.359±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Orange to Green
- BRN
- 2048590
- InChI
- InChI=1S/C14H11BrO/c1-10(16)11-2-4-12(5-3-11)13-6-8-14(15)9-7-13/h2-9H,1H3
- InChIKey
- UUVKNCRMWPNBNM-UHFFFAOYSA-N
- SMILES
- C(=O)(C1=CC=C(C2=CC=C(Br)C=C2)C=C1)C
- CAS DataBase Reference
- 5731-01-1(CAS DataBase Reference)
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Safety
- Hazard Codes
- Xi,N
- Risk Statements
- 36-51/53
- Safety Statements
- 26-36-61-24/25-22
- RIDADR
- UN 3077 9/PG 3
- WGK Germany
- 3
- HS Code
- 2914790090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H319Causes serious eye irritation
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P273Avoid release to the environment.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 640468
- Product name
- 4′-(4-Bromophenyl)acetophenone
- Purity
- 97%
- Packaging
- 25g
- Price
- $60.69
- Updated
- 2025/07/31
Sigma-Aldrich
- Product number
- 640468
- Product name
- 4′-(4-Bromophenyl)acetophenone
- Purity
- 97%
- Packaging
- 100g
- Price
- $221
- Updated
- 2025/07/31
TCI Chemical
- Product number
- A1410
- Product name
- 4-Acetyl-4'-bromobiphenyl
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $128
- Updated
- 2025/07/31
TRC
- Product number
- B807830
- Product name
- 4-(4-Bromophenyl)acetophenone
- Packaging
- 2.5g
- Price
- $75
- Updated
- 2021/12/16
AK Scientific
- Product number
- J51458
- Product name
- 4-Acetyl-4'-bromobiphenyl
- Packaging
- 5g
- Price
- $17.6
- Updated
- 2021/12/16
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4-Acetyl-4'-bromobiphenyl Chemical Properties,Usage,Production
Chemical Properties
White or pale brown solid
Uses
4-Acetyl-4'-bromobiphenyl is mainly used as a reagent for experimental organic synthesis or reactions, including substitution reactions or the synthesis and polymerisation of biphenyl derivatives.
Synthesis
Dichloromethane was added to Aluminium chloride. The mixture was stirred and cooled to 5 °C in a salt/ice bath. Acetyl chloride was quickly added through a dropping funnel and cooled to ? 3 °C to give a transparent yellow solution. Solid 4-bromobiphenyl was added in small amounts and stirred; wait for ? an hour, then add more. The mixture was stirred for ten hours, rising to 15 °C. The mixture was poured into a bucket of ice /37 percent HCl to destroy the aluminum chloride, then transferred to a separatory funnel and extracted into DCM. Then, the mixture was washed twice with water to destroy HCl. Again, it was washed with 10 percent NaOH and water. The collected DCM layer was dried over magnesium sulfate, mostly filtered by gravity. The solvent was removed in vacuo, and the residue was re-crystallized through ethanol to yield 4-Acetyl-4'-bromobiphen
References
[1] Journal of Molecular Liquids, 2012, vol. 175, p. 72 - 84
[2] Macromolecules, 2004, vol. 37, # 7, p. 2442 - 2449
[3] Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1992, vol. 213, p. 187 - 206
[4] Journal of the Chemical Society, 1934, p. 869,871
[5] Journal of the Chemical Society [Section] C: Organic, 1966, p. 840 - 845
4-Acetyl-4'-bromobiphenyl Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Acetyl-4'-bromobiphenyl manufacturers
Career Henan Chemical Co
- Product
- 4-ACETYL-4'-BROMOBIPHENYL 5731-01-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-02
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