ChemicalBook > CAS DataBase List > 4-METHOXY-2,6-DIMETHYLBENZALDEHYDE

4-METHOXY-2,6-DIMETHYLBENZALDEHYDE

Product Name
4-METHOXY-2,6-DIMETHYLBENZALDEHYDE
CAS No.
19447-00-8
Chemical Name
4-METHOXY-2,6-DIMETHYLBENZALDEHYDE
Synonyms
4-METHOXY-2,6-DIMETHYLBENZALDEHYDE;4-methoxy-2,6-dimethylbenzylaldehyde;Benzaldehyde, 4-methoxy-2,6-dimethyl-
CBNumber
CB4266844
Molecular Formula
C10H12O2
Formula Weight
164.2
MOL File
19447-00-8.mol
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4-METHOXY-2,6-DIMETHYLBENZALDEHYDE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
Off-white to yellow Solid
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
M219568
Product name
4-Methoxy-2,6-dimethylbenzaldehyde
Packaging
500mg
Price
$110
Updated
2021/12/16
Rieke Metals
Product number
AL0564
Product name
4-Methoxy-2,6-dimethyl-benzaldehyde
Packaging
1g
Price
$360
Updated
2021/12/16
Apolloscientific
Product number
OR310809
Product name
4-Methoxy-2,6-dimethylbenzaldehyde
Packaging
1g
Price
$421
Updated
2021/12/16
AK Scientific
Product number
Z0327
Product name
2,6-Dimethyl-4-methoxybenzaldehyde
Packaging
5g
Price
$451
Updated
2021/12/16
SynQuest Laboratories
Product number
2715-1-43
Product name
4-Methoxy-2,6-dimethylbenzaldehyde
Packaging
1g
Price
$464
Updated
2021/12/16
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4-METHOXY-2,6-DIMETHYLBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

874-63-5

51926-66-0

19447-00-8

3,5-Dimethylanisole was dispersed in 1 mL of iso-octane and slowly added dropwise over 20 minutes to a pre-prepared 3,5-dimethylanisole/iso-octane/TiCl4 mixed system. Sticky material was observed to precipitate during the reaction, and the reaction system was kept at -15 °C with continuous stirring for 4.5 hours. Upon completion of the reaction, the reaction was quenched with water and subsequently treated with NaOH solution. Subsequent operations were performed with reference to the standard post-treatment process of Example 1. Analysis of the product mixture by gas chromatography (GC) showed that it contained about 40% unreacted 3,5-dimethylanisole and about 53% of the target product, a mixture of 2-methoxy-4,6-dimethylbenzaldehyde and 4-methoxy-2,6-dimethylbenzaldehyde, in a total yield of about 53%.

References

[1] Patent: US5457239, 1995, A

4-METHOXY-2,6-DIMETHYLBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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