N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine
- Product Name
- N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine
- CAS No.
- 204580-28-9
- Chemical Name
- N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine
- Synonyms
- DK658;DK205;[2-[(tert-Butyldimethylsilyl)oxy]ethyl]methylamine;N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine;[2-(tert-Butyldimethylsilanyloxy)ethyl]methylamine;2-[(tert-Butyldimethylsilyl)oxy]-N-methylethanamine;N-[2-(tert-Butyldimethylsilyloxy)ethyl]-N-methylamine;2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]-N-methylethanamine;Ethanamine, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N-methyl-
- CBNumber
- CB42710958
- Molecular Formula
- C9H23NOSi
- Formula Weight
- 189.37
- MOL File
- 204580-28-9.mol
N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine Property
- Boiling point:
- 193.8±23.0 °C(Predicted)
- Density
- 0.830±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 9.55±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2931900090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H227Combustible liquid
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B943458
- Product name
- N-[2-(tert-Butyldimethylsilyloxy)ethyl]methylamine
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- ORS0005316
- Product name
- N-[2-(TERT-BUTYLDIMETHYLSILYLOXY)ETHYL]METHYLAMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.5
- Updated
- 2021/12/16
- Product number
- J95293
- Product name
- N-[2-(tert-Butyldimethylsilyloxy)ethyl]methylamine
- Packaging
- 10g
- Price
- $300
- Updated
- 2021/12/16
- Product number
- A166317
- Product name
- N-[2-(tert-Butyldimethylsilyloxy)ethyl]methylamine
- Purity
- 97%
- Packaging
- 10g
- Price
- $310
- Updated
- 2021/12/16
- Product number
- A166317
- Product name
- N-[2-(tert-Butyldimethylsilyloxy)ethyl]methylamine
- Purity
- 97%
- Packaging
- 1g
- Price
- $57
- Updated
- 2021/12/16
N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine Chemical Properties,Usage,Production
Synthesis
109-83-1
18162-48-6
204580-28-9
GENERAL STEPS: To a stirred solution of N-methyl-2-hydroxyethylamine (10 g, 133.13 mmol) in dichloromethane (200 mL) was added diisopropylethylamine (30.8 mL, 186.39 mmol) and tert-butyldimethylchlorosilane (20.06 g, 133.13 mmol) sequentially at room temperature. The reaction mixture was stirred for 16 hours. After the reaction was completed, water was added and the mixture was extracted with dichloromethane. The organic phase was separated, washed with water, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give N-[2-(tert-butyldimethylsilyloxy)ethyl]methylamine (18 g, 71.39%) as a yellow liquid.
References
[1] Organic and Biomolecular Chemistry, 2009, vol. 7, # 4, p. 655 - 659
[2] Patent: US2014/194431, 2014, A1. Location in patent: Paragraph 0160-0161
[3] Organic Letters, 2016, vol. 18, # 15, p. 3878 - 3881
[4] Patent: WO2015/57938, 2015, A1. Location in patent: Page/Page column 119-120
[5] Chemical and Pharmaceutical Bulletin, 2007, vol. 55, # 2, p. 328 - 333
N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine manufacturers
- Product
- N-[2-(tert-ButyldiMethylsilyloxy)ethyl]MethylaMine 204580-28-9
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 1000KG /month
- Release date
- 2021-11-24