7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone

Product Name: 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone
CAS No.: 1378388-19-2
Chemical Name: 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone
Synonyms: CL122;7-(2-bromo-5-chlorobenzyloxy)-1-naphthalenone;7-(2-bromo-5-chlorobenzyloxy)-3,4-dihydronaphthalene-1(2H)-one;7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one;7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone;1(2H)-Naphthalenone, 7-[(2-bromo-5-chlorophenyl)methoxy]-3,4-dihydro-
CBNumber: CB42717199
Molecular Formula: C17H14BrClO2
Formula Weight: 365.65
MOL File: 1378388-19-2.mol

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7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone Property

Boiling point:: 489.4±45.0 °C(Predicted)
Density: 1.488±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 0458DU
Product name: 7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging: 1g
Price: $87
Updated: 2021/12/16

AK Scientific

Product number: 0458DU
Product name: 7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one
Packaging: 25g
Price: $320
Updated: 2021/12/16

Ambeed

Product number: A163700
Product name: 7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one
Purity: 97%
Packaging: 100mg
Price: $8
Updated: 2021/12/16

Ambeed

Product number: A163700
Product name: 7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one
Purity: 97%
Packaging: 250mg
Price: $11
Updated: 2021/12/16

Ambeed

Product number: A163700
Product name: 7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one
Purity: 97%
Packaging: 1g
Price: $20
Updated: 2021/12/16

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7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone Chemical Properties,Usage,Production

Synthesis

66192-24-3

22009-38-7

1378388-19-2

The general procedure for the synthesis of 7-[(2-bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone from 2-bromo-5-chlorobenzyl bromide and 7-hydroxy-3,4-dihydronaphthalen-1(2H)-one was carried out in the following manner: under argon protection, 7-hydroxy-3,4-dihydronaphthalen-1(2H)-one (13.9 g, 85.7 mmol) and 2-bromo-5- chlorobenzyl bromide (25.6 g, 90.0 mmol) were dissolved in dimethylformamide (850 mL) and potassium carbonate (24 g, 172 mmol) was added. The reaction mixture was stirred at room temperature for 18 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (1 L) and washed sequentially with water three times and brine once. The organic layer was dried with magnesium sulfate, filtered and concentrated. Methanol (500 mL) was added to the oil obtained by concentration and stirred for 30 minutes. The solid product was collected by filtration to afford 7-[(2-bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone (27.8 g, 89% yield).

References

[1] Patent: WO2013/75029, 2013, A1. Location in patent: Page/Page column 53-55
[2] Patent: US2013/309196, 2013, A1. Location in patent: Paragraph 0205
[3] Patent: US2014/178336, 2014, A1. Location in patent: Paragraph 0234
[4] Patent: US2015/361073, 2015, A1. Location in patent: Paragraph 0433
[5] Patent: CN107540679, 2018, A. Location in patent: Paragraph 0031; 0032

7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone manufacturers

Capot Chemical Co.,Ltd.

Product: 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone 1378388-19-2
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: kgs
Release date: 2023-02-09

Zhuozhou Wenxi import and Export Co., Ltd

Product: 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone 1378388-19-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone 1378388-19-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

1378388-19-2, 7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenoneRelated Search:

7-[(2-Bromo-5-chlorophenyl)methoxy]-3,4-dihydro-1(2H)-naphthalenone

7-((2-Bromo-5-chlorobenzyl)oxy)-3,4-dihydronaphthalen-1(2H)-one

CL122

7-(2-bromo-5-chlorobenzyloxy)-3,4-dihydronaphthalene-1(2H)-one

1(2H)-Naphthalenone, 7-[(2-bromo-5-chlorophenyl)methoxy]-3,4-dihydro-

7-(2-bromo-5-chlorobenzyloxy)-1-naphthalenone

1378388-19-2

C17H14BrClO2