METHYL 6-AMINO-2-METHYLNICOTINATE
- Product Name
- METHYL 6-AMINO-2-METHYLNICOTINATE
- CAS No.
- 872355-52-7
- Chemical Name
- METHYL 6-AMINO-2-METHYLNICOTINATE
- Synonyms
- METHYL 6-AMINO-2-METHYLNICOTINATE;methyl 6-amino-2-methyl-pyridine-3-carboxylate;3-Pyridinecarboxylic acid, 6-amino-2-methyl-, methyl ester
- CBNumber
- CB4304346
- Molecular Formula
- C8H10N2O2
- Formula Weight
- 166.18
- MOL File
- Mol file
METHYL 6-AMINO-2-METHYLNICOTINATE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- color
- Light yellow to yellow
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M878138
- Product name
- Methyl6-amino-2-methylnicotinate
- Packaging
- 10mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- CS-0061193
- Product name
- Methyl6-amino-2-methylnicotinate
- Purity
- 99.95%
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- CS-0061193
- Product name
- Methyl6-amino-2-methylnicotinate
- Purity
- 99.95%
- Packaging
- 250mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- CS-0061193
- Product name
- Methyl6-amino-2-methylnicotinate
- Purity
- 99.95%
- Packaging
- 1g
- Price
- $235
- Updated
- 2021/12/16
- Product number
- Y4417
- Product name
- Methyl6-amino-2-methylpyridine-3-carboxylate
- Packaging
- 1g
- Price
- $435.2
- Updated
- 2021/12/16
METHYL 6-AMINO-2-METHYLNICOTINATE Chemical Properties,Usage,Production
Synthesis
67-56-1
680208-82-6
872355-52-7
Preparative Example 36: Preparation of methyl 6-amino-2-methylnicotinate [0248] 6-Amino-2-methyl-3-pyridinecarboxylic acid (1.00 g) was suspended in methanol (15 mL) and concentrated sulfuric acid (0.5 mL) was added. The reaction mixture was heated and stirred under reflux conditions for 18 hours. Upon completion of the reaction, the reaction mixture was cooled, neutralized with sodium hydroxide solution and subsequently extracted with chloroform. The organic layer was washed with saturated sodium chloride solution, dried over anhydrous sodium sulfate and the solvent was concentrated under reduced pressure to give the target product methyl 6-amino-2-methylnicotinate (0.82 g). Mass spectrum (ESI) m/z: 167 (M + H)+.
References
[1] Patent: EP2565182, 2013, A1. Location in patent: Paragraph 0246; 0247; 0248
[2] Patent: WO2006/112828, 2006, A1. Location in patent: Page/Page column 74
METHYL 6-AMINO-2-METHYLNICOTINATE Preparation Products And Raw materials
Raw materials
Preparation Products
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