(3-Methoxy-5-methylphenyl)methanol

Product Name: (3-Methoxy-5-methylphenyl)methanol
CAS No.: 119650-44-1
Chemical Name: (3-Methoxy-5-methylphenyl)methanol
Synonyms: 3-Methoxy-5-methylbenzyl alcohol;3-methoxy-5-methylBenzenemethanol;Benzenemethanol, 3-methoxy-5-methyl-
CBNumber: CB43062919
Molecular Formula: C9H12O2
Formula Weight: 152.19
MOL File: 119650-44-1.mol

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(3-Methoxy-5-methylphenyl)methanol Property

storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M333203
Product name: (3-Methoxy-5-methylphenyl)methanol
Packaging: 100mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 3394AA
Product name: (3-Methoxy-5-methylphenyl)methanol
Packaging: 250mg
Price: $170
Updated: 2021/12/16

AK Scientific

Product number: 3394AA
Product name: (3-Methoxy-5-methylphenyl)methanol
Packaging: 1g
Price: $350
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0389252
Product name: (3-METHOXY-5-METHYLPHENYL)METHANOL
Purity: 95.00%
Packaging: 5MG
Price: $498.3
Updated: 2021/12/16

AK Scientific

Product number: 3394AA
Product name: (3-Methoxy-5-methylphenyl)methanol
Packaging: 5g
Price: $950
Updated: 2021/12/16

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(3-Methoxy-5-methylphenyl)methanol Chemical Properties,Usage,Production

Synthesis

106116-42-1

119650-44-1

General procedure for the synthesis of (3-methoxy-5-methylphenyl)methanol from 1-(bromomethyl)-3-methoxy-5-methylbenzene: To a solution of 1-(bromomethyl)-3-methoxy-5-methylbenzene (2.14 g) in acetone (80 mL) was added sodium bicarbonate (1.05 g) and water (50 mL), the mixture was heated and refluxed for 18 hours. Upon completion of the reaction, the reaction mixture was extracted with ethyl acetate, the organic layers were combined and washed with saturated sodium chloride solution. The organic layer was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography (eluent: ethyl acetate/hexane) to afford the target compound as a yellow oil (1.22 g).1H NMR (400 MHz, CDCl3) δ 2.35 (3H, s), 3.82 (3H, s), 4.64 (2H, s), 6.68 (1H, s), 6.75 (1H, s), 6.79 (1H, s).

References

[1] Journal of the American Chemical Society, 2012, vol. 134, # 30, p. 12402 - 12405
[2] Synthesis, 2007, # 1, p. 65 - 74
[3] Tetrahedron Letters, 2000, vol. 41, # 17, p. 3007 - 3010
[4] Journal of the American Chemical Society, 2011, vol. 133, # 39, p. 15686 - 15696
[5] RSC Advances, 2014, vol. 4, # 61, p. 32241 - 32248

(3-Methoxy-5-methylphenyl)methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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(3-Methoxy-5-methylphenyl)methanol Suppliers

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119650-44-1, (3-Methoxy-5-methylphenyl)methanolRelated Search:

3-methoxy-5-methylBenzenemethanol

Benzenemethanol, 3-methoxy-5-methyl-

3-Methoxy-5-methylbenzyl alcohol

119650-44-1