([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride

Product Name: ([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride
CAS No.: 848141-14-0
Chemical Name: ([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride
Synonyms: ([5-(METHYLSULFONYL)PYRIDIN-2-YL]METHYL)AMINE HCL;[5-(methanesulfonyl)pyridin-2-yl]methanaminium chloride;(5-(Methylsulfonyl)pyridin-2-yl)methanamine hydrochloride;([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride;1-[5-(methane sulfonyl)pyridin-2-yl]methanamine Hydrochloride;2-Pyridinemethanamine, 5-(methylsulfonyl)-, monohydrochloride;([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride(WX603194)
CBNumber: CB43143207
Molecular Formula: C7H11ClN2O2S
Formula Weight: 222.69244
MOL File: 848141-14-0.mol

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([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride Property

storage temp.: Inert atmosphere,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M354230
Product name: (5-(Methylsulfonyl)pyridin-2-yl)methanamineHydrochloride
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 4827AQ
Product name: (5-methylsulfonylpyridin-2-yl)methanamine;hydrochloride
Packaging: 1g
Price: $810.8
Updated: 2021/12/16

Ambeed

Product number: A492786
Product name: (5-(Methylsulfonyl)pyridin-2-yl)methanaminehydrochloride
Purity: 98%
Packaging: 5g
Price: $859
Updated: 2021/12/16

Alichem

Product number: 848141140
Product name: (5-(Methylsulfonyl)pyridin-2-yl)methanaminehydrochloride
Packaging: 5g
Price: $1393.6
Updated: 2021/12/16

Alichem

Product number: 848141140
Product name: (5-(Methylsulfonyl)pyridin-2-yl)methanaminehydrochloride
Packaging: 10g
Price: $2186.88
Updated: 2021/12/16

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([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride Chemical Properties,Usage,Production

Synthesis

848141-13-9

848141-14-0

The general procedure for the synthesis of (5-(methylsulfonyl)pyridin-2-yl)methanamine hydrochloride from 5-(methylsulfonyl)pyridine-2-carbonitrile was as follows: 5-(methylsulfonyl)pyridine-2-carbonitrile (2.15 g, 11.8 mmol) was dissolved in methanol (230 mL). 6 M hydrochloric acid (1 mL) and 10% palladium-carbon catalyst (234 mg) were added to the solution, followed by stirring the reaction mixture overnight under atmospheric hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration and the filtrate was concentrated under reduced pressure to remove the solvent. Water was added to the residue and the resulting solution was freeze-dried to afford (5-(methylsulfonyl)pyridin-2-yl)methylamine hydrochloride as a yellow powder (2.34 g, 89% yield). The product was characterized by 1H NMR (CD3OD): δ 9.10 (1H, d, J = 2.2 Hz); 8.36 (1H, dd, J = 8.2, 2.4 Hz); 7.68 (1H, d, J = 8.8 Hz); 4.29 (2H, s); 3.22 (3H, s).

References

[1] Patent: WO2005/26124, 2005, A1. Location in patent: Page/Page column 102
[2] Patent: WO2005/26123, 2005, A1. Location in patent: Page/Page column 86
[3] Patent: US2010/216843, 2010, A1. Location in patent: Page/Page column 22
[4] Patent: WO2018/30550, 2018, A1. Location in patent: Paragraph 0646
[5] Patent: WO2015/160654, 2015, A1

([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride Suppliers

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848141-14-0, ([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine HydrochlorideRelated Search:

([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride

(5-(Methylsulfonyl)pyridin-2-yl)methanamine hydrochloride

([5-(Methylsulfonyl)Pyridin-2-Yl]Methyl)Amine Hydrochloride(WX603194)

([5-(METHYLSULFONYL)PYRIDIN-2-YL]METHYL)AMINE HCL

2-Pyridinemethanamine, 5-(methylsulfonyl)-, monohydrochloride

1-[5-(methane sulfonyl)pyridin-2-yl]methanamine Hydrochloride

[5-(methanesulfonyl)pyridin-2-yl]methanaminium chloride

848141-14-0