ChemicalBook > CAS DataBase List > 3-PHENYLBENZENESULFONYL CHLORIDE

3-PHENYLBENZENESULFONYL CHLORIDE

Product Name: 3-PHENYLBENZENESULFONYL CHLORIDE
CAS No.: 65685-01-0
Chemical Name: 3-PHENYLBENZENESULFONYL CHLORIDE
Synonyms: BIPHENYL-3-SULFONYL CHLORIDE;Biphenyl-3-sulphonyl chloride;3-PHENYLBENZENESULFONYL CHLORIDE;3-PHENYLBENZENESULPHONYL CHLORIDE;1,1'-biphenyl-3-sulfonyl chloride;1,1'-Biphenyl]-3-sulfonyl chloride;3-phenylbenzene-1-sulfonyl chloride;1,1'-Biphenyl]-3-sulfonyl chloride (9CI, ACI);3-PHENYLBENZENESULFONYL CHLORIDE ISO 9001：2015 REACH;3-Phenylbenzenesulphonyl chloride, 3-(Chlorosulphonyl)biphenyl
CBNumber: CB4338606
Molecular Formula: C12H9ClO2S
Formula Weight: 252.72
MOL File: 65685-01-0.mol

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3-PHENYLBENZENESULFONYL CHLORIDE Property

Melting point:: 38-40 °C
Boiling point:: 397.8±21.0 °C(Predicted)
Density: 1.320±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
form: viscous liquid
color: Clear, yellow

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Safety

Hazard Codes: C,Xi
Risk Statements: 36
Safety Statements: 26
RIDADR: UN3261
Hazard Note: Corrosive
HazardClass: 8
HS Code: 2904990090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR12582
Product name: Biphenyl-3-sulphonylchloride
Packaging: 100mg
Price: $31
Updated: 2021/12/16

Apolloscientific

Product number: OR12582
Product name: Biphenyl-3-sulphonylchloride
Packaging: 250mg
Price: $63
Updated: 2021/12/16

Oakwood

Product number: 014900
Product name: Biphenyl-3-sulfonylchloride
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: OR12582
Product name: Biphenyl-3-sulphonylchloride
Packaging: 1g
Price: $224
Updated: 2021/12/16

AK Scientific

Product number: 5375AH
Product name: 3-Phenylbenzenesulfonylchloride
Packaging: 1g
Price: $325
Updated: 2021/12/16

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3-PHENYLBENZENESULFONYL CHLORIDE Chemical Properties,Usage,Production

Synthesis

94306-39-5

65685-01-0

[1,1'-Biphenyl]-3-yl(benzyl)thiolane (450 mg, 1.63 mmol) was used as a raw material to synthesize [1,1'-biphenyl]-3-sulfonyl chloride according to General Method J. The synthesis was carried out by using a mixture of acetic acid/water (3:1, v/v; 0.1 mmol/mL) and N-chlorobutanediyl chloride (3:1, v/v; 0.1 mmol/mL). The procedure was as follows: the raw material was dissolved in a mixed solvent of acetic acid/water (3:1, v/v; 0.1 mmol/mL) at room temperature, and N-chlorosuccinimide (NCS, 6 equiv) was added. The reaction mixture was stirred at the same temperature for 3-6 h. The reaction progress was monitored by HPLC. After completion of the reaction, the solvent was removed by concentration under reduced pressure, saturated aqueous sodium bicarbonate was added and extracted with ethyl acetate (EtOAc). The organic layers were combined, washed with saturated brine and dried over anhydrous sodium sulfate. After filtration, the crude product was concentrated under reduced pressure and purified by Combifiash silica gel column chromatography (100% hexane as eluent) to afford [1,1'-biphenyl]-3-sulfonyl chloride 250 mg (5.9% yield) as a colorless solid. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 8.28-8.24 (m, 1H), 8.05-8.01 (m, 1H), 7.98-7.95 (m, 1H), 7.74-7.68 (m, 1H), 7.66-7.61 (m, 2H), 7.56-7.49 (m, 2H), 7.49- 7.43 (m, 1H).

References

[1] ChemMedChem, 2016, vol. 11, # 23, p. 2607 - 2620
[2] Patent: WO2018/52903, 2018, A1. Location in patent: Page/Page column 22-23; 58

3-PHENYLBENZENESULFONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-PHENYLBENZENESULFONYL CHLORIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Biphenyl-3-sulphonyl chloride 65685-01-0
Price: US $0.00-0.00/Kg
Min. Order: 1KG
Purity: 99.0%+
Supply Ability: 100 tons
Release date: 2020-01-06

65685-01-0, 3-PHENYLBENZENESULFONYL CHLORIDERelated Search:

[3-(4-FLUOROPHENYL)PHENYL]SULFONYL CHLORIDE 4-PHENYLBENZENESULFONYL CHLORIDE [3-(4-CHLOROPHENYL)PHENYL]SULFONYL CHLORIDE (3-[4-(TRIFLUOROMETHYL)PHENYL]PHENYL)SULFONYLCHLORIDE 2'-FLUORO-BIPHENYL-3-SULFONYL CHLORIDE 2',4'-DIMETHOXY-BIPHENYL-3-SULFONYL CHLORIDE 3'-FLUORO-BIPHENYL-3-SULFONYL CHLORIDE [3-[3,5-BIS(TRIFLUOROMETHYL)PHENYL]PHENYL]SULFONYL CHLORIDE 3-PHENYLBENZENESULFONYL CHLORIDE [3-(4-METHYLPHENYL)PHENYL]SULFONYL CHLORIDE 3',4'-DIMETHOXY-BIPHENYL-3-SULFONYL CHLORIDE [3-(3,4-DICHLOROPHENYL)PHENYL]SULFONYL CHLORIDE [3-(4-METHOXYPHENYL)PHENYL]SULFONYL CHLORIDE 3'-METHOXY-BIPHENYL-3-SULFONYL CHLORIDE [3-(3,5-DICHLOROPHENYL)PHENYL]SULFONYL CHLORIDE 2-PHENYLBENZENESULFONYL CHLORIDE 3'-METHYL-BIPHENYL-3-SULFONYL CHLORIDE 3'-CHLORO-BIPHENYL-3-SULFONYL CHLORIDE

1,1'-biphenyl-3-sulfonyl chloride

3-Phenylbenzenesulphonyl chloride, 3-(Chlorosulphonyl)biphenyl

3-PHENYLBENZENESULFONYL CHLORIDE

3-PHENYLBENZENESULPHONYL CHLORIDE

Biphenyl-3-sulphonyl chloride

BIPHENYL-3-SULFONYL CHLORIDE

3-phenylbenzene-1-sulfonyl chloride

3-PHENYLBENZENESULFONYL CHLORIDE ISO 9001：2015 REACH

1,1'-Biphenyl]-3-sulfonyl chloride (9CI, ACI)

1,1'-Biphenyl]-3-sulfonyl chloride

65685-01-0

SULFONYL CHLORIDE